• Title/Summary/Keyword: Dry sample

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Preparation of High Permeability Mn-Zn Ferrites by the Wet Method (습식법에 의한 고투자율 Mn-Zn Ferrite의 제조에 관한 연구)

  • 이경희;이병하;허원도;황우연
    • Journal of the Korean Ceramic Society
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    • v.31 no.1
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    • pp.55-61
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    • 1994
  • Mn-Zn ferrite powder was obtained by wet method that was to be coprecipitated the metal ions of Fe2+, Mn2+ and Zn2+ with alkali solution. The target composition of the ferrite powder was 52 mol% Fe2O3, 24 mol% MnO, and 24 mol% ZnO, that was based on the region of high permeability. And the other ferrite powder was prepared by the dry method that was to be mixed the metal oxides as the above chemical composition. The wet method was compared with dry method for the powder properties and the electromagnetic characteristics of sintered cores. The synthesized powder by wet method was smaller particle size, narrower particle distribution, and higher purity than that of dry method. The initial permeability of sintered sample prepared by the wet method was 14000~28000, on the other side, 9000~15500 in case of the dry method.

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Study on the Soil Compaction (흙의 다짐에 관한 연구(I))

  • 강문묵
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.11 no.4
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    • pp.1783-1790
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    • 1969
  • It is one of the most economical method of soil stabilization works to compact soil, which increases soil density artificially. Compaction effort is to lessen void of soils, and consequently its aim is to enlarge friction and cohesion force, and reduce permeability of soil. Factors in compaction effort are moisture content, grain size, grain size distribution, physical properties, compaction method and temperature of soils etc. The results obtained in this study on the effects that grain size, gradation and physical properties influence upon compaction effort for 20 samples under the constant compaction method, are summarized as follows: 1. The bigger the maximum dry density is, the smaller the optimum moisture content is, on the other hand, the smaller the maximum dry densityis, the bigger the optimum moisture content is, ingeneral. 2. The coarser the grain size is, the bigger the maximum dry density is, and the optimum moisture content becomes small, and dry density-moisture content curve has the sharp peak, generally. Also, the finer the grain size is the smaller the maximum dry density is, and the optimum moisture content shows the big value, and dry density-moisture content curve has the dull peak. 3. The maximum dry density shows the biggest value on the sample to be about 15% of particles finer than No. 200 sieve. The more the percent passing of No. 10 sieve increase, the smaller the maximum dry density is. Soils which have uniformity coefficient less than 5 in particles larger than 0.074mm hardly show dry density-moisture content curve. 4. There is a relation which is ramax=2.3948-0.0376 Wopt between the maximum dry density and the optimum moisture content, namely, the maximum dry density is increased in proportion to decrease of the optimum moisture content. 5. There are relations to be the straight lines which the maximum dry density decrease, on the other hand, the optimum moisture content increase in accordance with enlargement of Atterberg Limit(LL, PL, PL) in compacted soils.

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Studies on the Calculating Method of Conditioned Weight by dry Weight after Boiling-off in Raw Silk (생사정량산정에 있어서 연감후 무수량의 도입에 관한 연구)

  • 김수현;이상근;김영진
    • Journal of Sericultural and Entomological Science
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    • v.13 no.1
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    • pp.73-78
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    • 1971
  • The purpose of this study is to find out the method of conditioned weight test by which the dealing weight of raw silk can be calculated from true fiber in order to do the fair trading. The results of this study were as follows. 1. It is more reasonable than the current test that conditioned weight as a dealing weigh can be calculated by boil-off and moisture regain which is a percentage of boil-on and moisture regain to net weight. Because the boil-off and moisture regain can show directly the amount of true fiber and reproductibility in raw silk. In this study the boil-off and moisture regain is to take dry weight after boiling-off from net weight. 2. To calculate the conditioned weight from boil-of and moisture regain it would be proper that the standard additional ratio is 44 per cent of dry weight after boiling-off. 3. Boil-of percent of the sizing sample skein used in the size test did not show a statistical significance comparing with the boil-off percent of sample skeins (24 skeins) which may represent that of a lot. To observe this result boil-off percent of the sizing sample skein may represent that of a lot. 4. In Korea if conditioned weight test substitute for test of boil-off and moisture regain, we make a profit of two billion won in a year at the current market-price.

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Verification of the adequacy of domestic low-level radioactive waste grouping analysis using statistical methods

  • Lee, Dong-Ju;Woo, Hyunjong;Hong, Dae-Seok;Kim, Gi Yong;Oh, Sang-Hee;Seong, Wonjun;Im, Junhyuck;Yang, Jae Hwan
    • Nuclear Engineering and Technology
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    • v.54 no.7
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    • pp.2418-2426
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    • 2022
  • The grouping analysis is a method guided by the Korea Radioactive Waste Agency for efficient analysis of radioactive waste for disposal. In this study, experiments to verify the adequacy of grouping analysis were conducted with radioactive soil, concrete, and dry active waste in similar environments. First, analysis results of the major radionuclide concentrations in individual waste samples were reviewed to evaluate whether wastes from similar environments correspond to a single waste stream. As a result, the soil and concrete waste were identified as a single waste stream because the distribution range of radionuclide concentrations was "within a factor of 10", the range that meet the criterion of the U.S. Nuclear Regulatory Commission for a single waste stream. On the other hand, the dry active waste was judged to correspond to distinct waste streams. Second, after analyzing the composite samples prepared by grouping the individual samples, the population means of the values of "composite sample analysis results/individual sample analysis results" were estimated at a 95% confidence level. The results showed that all evaluation values for soil and concrete waste were within the set reference values (0.1-10) when five-package and ten-package grouping analyses were conducted, verifying the adequacy of the grouping analysis.

Study on the Effect of the ABC Dry Chemical on Wood in Pyrolysis (ABC 분말소화약제의 열분해 시 목재에 미치는 영향에 관한 연구)

  • Ko, Wang-Youl;In, Se-Jin
    • Fire Science and Engineering
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    • v.32 no.3
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    • pp.1-7
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    • 2018
  • This study the effect of pyrolysis products ABC dry chemical and of monoammonium phosphate on wood surface. When the pyrolysis product was removed from the wood surface, monoammonium phosphate was removed due to the high viscosity of the transparent pyrolysis product, but the ABC dry chemical was removed in a lump form. Thermal analysis showed that the pyrolysis characteristics of each sample were similar but the weight of pyrolysis residue was 55.9% for ABC dry chemical and 25.2% for monoammonium phosphate. The additives added to the ABC dry chemical also affect the weight of the pyrolysis residue and the fire protection effect of metaphosphoric acid.

Effect of Dry Grinding of Laterite on the Extraction of Nickel and Cobalt (라테라이트광의 건식분쇄가 니켈 및 코발트의 침출에 미치는 영향)

  • Kim, Wan-Tae;Choi, Do-Young;Kim, Sang-Bae
    • Journal of the Mineralogical Society of Korea
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    • v.23 no.3
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    • pp.227-234
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    • 2010
  • We investigated the effect of dry grinding of laterite on the extraction of nickel and cobalt. The major chemical compositions of the sample for this work were $SiO_2$, $Fe_2O_3$ and MgO. The sample contained 0.81% Ni and 0.02% Co. The major minerals of the sample were lizardite and quartz with minor amounts of forsterite and enstatite. The mean particle size, specific surface area and density of the ground sample decreased with increasing grinding time, while the amorphization of lizardite increased as identified by XRD analysis. The grinding enabled the extraction ratio of Ni and Co to increase by the breakdown of Mg-OH bonding in the lizardite structure. However, physical properties of quartz were not changed by grinding. The extraction ratio of Ni and Co increased with increasing grinding time. Approximately 80% of Ni and Co were extracted regardless of the kind of acid solutions when the sample was ground for 60 minutes.

DETERMINATION OF MOISTURE AND NITROGEN ON UNDRIED FORAGES BY NEAR INFRARED REFLECTANCE SPECTROSCOPY(NIRS)

  • Cozzolino, D.;Labandera, M.;Inia La Estanzuela
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1620-1620
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    • 2001
  • Forages, both grazed and conserved, provide the basis of ruminant production systems throughout the world. More than 90 per cent of the feed energy consumed by herbivorous animals world - wide were provided by forages. With such world - wide dependence on forages, the economic and nutritional necessity of been able to characterize them in a meaningful way is vital. The characterization of forages for productive animals is becoming important for several reasons. Relative to conventional laboratory procedures, Near Infrared Reflectance Spectroscopy (NIRS) offers advantages of simplicity, speed, reduced chemical waste, and more cost-effective prediction of product functionality. NIR spectroscopy represents a radical departure from conventional analytical methods, in that entire sample of forage is characterized in terms of its absorption properties in the near infrared region, rather than separate subsamples being treated with various chemicals to isolate specific components. This forces the analyst to abandon his/her traditional narrow focus on the sample (one analyte at a time) and to take a broader view of the relationship between components within the sample and between the sample and the population from which it comes. forage is usually analysed by NIRS in dry and ground presentation. Initial success of NIRS analysis of coarse forages suggest a need to better understand the potential for analysis of minimally processed samples. Preparation costs and possible compositional alterations could be reduced by samples presented to the instrument in undried and unground conditions. NIRS has gained widespread acceptance for the analysis of forage quality constituents on dry material, however little attention has been given to the use of NIRS for chemical determinations on undried and unground forages. Relatively few works reported the use of NIRS to determine quality parameters on undried materials, most of them on both grass and corn silage. Only two works have been found on the determination of quality parameters on fresh forages. The objectives of this paper were (1) to evaluate the use of NIRS for determination of nitrogen and moisture on undried and unground forage samples and (2) to explore two mathematical treatments and two NIR regions to predict chemical parameters on fresh forage. Four hundred forage samples (n: 400) were analysed in a NIRS 6500 instrument (NIR Systems, PA, USA) in reflectance mode. Two mathematical treatments were applied: 1,4,4,1 and 2,5,5,2. Predictive equations were developed using modified partial least squares (MPLS) with internal cross - validation. Coefficient of determination in calibration (${R^2}_{CAL}$) and standard error in cross-validation (SECV) for moisture were 0.92 (12.4) and 0.92 (12.4) for 1,4,4,1 and 2,5,5,2 respectively, on g $kg^{-1}$ dry weight. For crude protein NIRS calibration statistics yield a (${R^2}_{CAL}$) and (SECV) of 0.85 (19.8) and 0.85 (19.6) for 1,4,4,1 and 2,5,5,2 respectively, on a dry weight. It was concluded that NIRS is a suitable method to predict moisture and nitrogen on fresh forage without samples preparation.

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Changes in Moisture Content and Quality of Oriental Hybrid Lily (Lilium oriental cv. Siberia) Cut Flowers during Storage at Cold and Dry Condition and Subsequent Exposure to Ambient Temperature (오리엔탈 나리 '시베리아' 절화의 포장내 건식저장 기간별 수분함량과 품질 변화)

  • Lee, Jung-Soo;Rhee, JuHee;Kang, Yun-Im;Choi, Ji Weon
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.23 no.1
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    • pp.27-36
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    • 2017
  • In order to determine the relationship between water content and flower qualities of oriental hybrid lily cv. 'Siberia' cut flower, flowers were subjected to dry and cold storage at $5^{\circ}C$ for 3, 6, and 12 days and subsequently exposed to ambient temperature ($26^{\circ}C$) in bottles with water for up to 16 days. Flowers stored at $22^{\circ}C$ in dry condition for 3 days were used as the control. Changes in fresh weight, moisture content, water balance, flowering stages, osmolality and vase life of cut flowers were observed. Flowers treated with cold and dry storage had higher moisture content compared to control sample. However, this trend was evident only for 3-day cold and dry stored sample during the whole storage period. The fresh weight of cut flowers increased gradually when the samples were transferred to ambient temperature in water bottles and then declined steadily before reaching the peak in between 6-8 days of vase life. However, the changes of fresh weight of control sample were substantially faster than samples pre-treated with cold and dry storage. This was also correlated with the water balance of cut flower as it reached the minus (-) value in 6-8 days of vase life at ambient temperature. Cut lily flowers showed high osmolality values corresponding with the duration of dry storage regardless of low or higher temperature. However, osmolality had no effect on vase life since flower stem absorbed water rapidly at the end of dry storage period. Our vase life results suggest that cold and dry storage of lily cut flowers for a certain period could ensure longer vase life at ambient temperature. It was observed that prolonging the storage period at cold and dry condition for more than a week significantly increased bud abortion, reduced longevity of flowers and reduced the vase life of cut flowers. On the other hand, the shorter cold and dry storage treatment delayed the bud opening and senescence of the flowers, thus, slowering the normal maturation and aging. Results indicated that dry and cold storage at $5^{\circ}C$ for 3 days was effective in maintaining and preserving overall quality and vase life at ambient condition of oriental hybrid lily cut flowers.

COMPARISON OF SHADE CHANGES ACCORDING TO DRY/WET CONDITION OF TEETH USING INTRA-ORAL COLORIMETER

  • Lee, Dong-Hwan;Han, Jung-Suk;Yang, Jae-Ho;Lee, Jai-Bong
    • The Journal of Korean Academy of Prosthodontics
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    • v.43 no.3
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    • pp.314-321
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    • 2005
  • Objectives. The purpose of this study was to compare the shade changes in wet and dry conditions of natural teeth using two different intra-oral colorimeters. Materials and methods. Twenty volunteer subjects have no restorations and fillings in the maxillary central incisors were involved in this clinical study. The color of tooth was measured by two different instruments that were a Shade $Scan^{TM}$ System and a VITA $Easyshade^{(R)}$, Five times consecutive measurements were done for each subject with both instruments. Groups of measurement are an initial wet condition as control, dry in 5 minutes, 15 seconds after re-wetting with saliva, re-wetting after 5minutes and re-wetting after 30 minutes. Using ShadeScan $System^{TM}$, tooth image was captured and converted to the mapping image of Vitapan 3D master. Three main shades were chosen from each subject and calculated the area in Global Lab Image software. Data were analyzed using paired T-Test and Wilcoxon Signed Ranked Test. Using VITA $Easyshade^{(R)}$, color differences($\Delta$E) between measurements were analyzed with one sample T-test. Results. Using ShadeScan $System^{TM}$, there were significant differences between control group and dry(P=.023), dry and re-wetting 15 seconds, 5 minutes, 30 minutes as well(P=.021, P=.017, P=.030) in comparison of primary shade. However, comparing three main shades, there was no significant difference between control and dry(P=.105). Using VITA $Easyshade^{(R)}$, color differences($\Delta$E) between control and dry, dry and re-wetting 30 minutes were statistically different(P=.002, P=.022). Conclusion. Primary shade could be changed in dry and wetting procedure in time, however there was no significant shade changes in overall.

Measurement of Atmospheric Dry Deposition and Size Distribution of Particulate PCBs in 1999 at Seoul

  • Park, Seong-Suk;Shin, Hye-Joung;Yi, Seung-Muk;Kim, Yong-Pyo
    • Journal of Korean Society for Atmospheric Environment
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    • v.22 no.E1
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    • pp.35-43
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    • 2006
  • Ambient particle size distributions of PCBs and their dry deposition fluxes were measured at a site in Seoul to quantify dry deposition fluxes of PCBs and size characteristics of PCBs in the air, and to estimate ambient concentrations of gaseous PCBs and dry deposition fluxes. The dry deposition plate was used to measure dry deposition fluxes of particulate mass and PCBs and a cascade impactor and rotary impactor were used to measure ambient particle size distributions for small ($D_p<9{\mu}m$) and large ($D_p>9{\mu}m$) particles, respectively. Six sample sets were collected from April to July 1999. The fluxes of particulate total PCBs (the sum of 43 congeners) ranged from 160 to $607ng\;m^{-2}day^{-1}$. The size distribution of total PCBs was bimodal with two peaks in small particle size ($D_p{\sim}0.6\;and\;6{\mu}m$, respectively) and, thus, mass concentration being dominant in small particles. The mean particulate PCBs concentration was $6.9{\mu}g$ PCBs/g. The concentrations of PCB homologues in the gas phase were estimated based on the particle/gas partition coefficient ($K_p$) with the measured values of particulate PCBs in this study and they were comparable to those observed in other previous studies. Dry deposition fluxes were estimated by calculating dry deposition velocities.