• 제목/요약/키워드: Dry sample

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Taurine Content in Korean Foods of Plant Origin (한국인 상용 식물성 식품의 타우린함량 조사)

  • 박태선;박정은;장준성;손미원;손경희
    • Journal of the Korean Society of Food Science and Nutrition
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    • 제27권5호
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    • pp.801-807
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    • 1998
  • Taurine content in Korean foods of plant origin was determined for 118 commonly used food items including cereals, potatoes, pulses, nuts, seeds, vegetables and fruits. Taurine concentration in food sample was analyzed using an automated amino acid analyzer(Biochrom 20, Pharmacia LKB) based on ion-exchange chromatography. Taurine was frequently detected in plant kingdom in much lower concentrations(1/100~1/1000) than those found in marine lifes and mammals. Glutinous rice, glutinous millent and sorghum did not contain taurine, while 0.7~3.9mg taurine/100g dry wt were detected in rice, barley and their products. Potatoes and sweet potatoes contained 0.3~1.2mg taurine/100g wet wt, and seasame seeds, perilla seeds, almonds, walnuts and gigko nuts contained 0.7~3.0mg taurine/100g wt. Taurine concentration was undetectable in most of the pulses, and in a large number of vegetables. Garlic bulbs, eggplants, green peppers, lotus roots, and cabbages have a relatively high level of taurine(around 1mg taurine/100g wet wt) among vegetables. Taurine was absent or found in very low levels(<1mg taurine/100g wet wt) in most of the commonly used fruits.

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Analysis of ultra-low radionuclide concentrations in water samples with baromembrane method

  • Vasyanovich, Maxim;Ekidin, Aleksey;Trapeznikov, Alexander;Plataev, Anatoly
    • Nuclear Engineering and Technology
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    • 제53권1호
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    • pp.253-257
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    • 2021
  • This work demonstrates the use of baromembrane method based on reverse osmosis (RO) process. The method is realized on mobile complex, which allows to concentrate and determine ultra-low activity of radionuclides in water cooling ponds of Russian nuclear fuel cycle enterprises. The existence level of radionuclide background creates difficult conditions for identification the contribution of liquid discharges enterprise, as standard monitoring methods have a very high detection level for radionuclides. Traditional methods for determining the background radionuclides concentrations require the selection of at least 500 liters (l) of water, followed by their evaporation to form a dry residue. This procedure with RO membranes requires at least 5 days. It is possible to reduce the time and energy spent on evaporation of hundreds of water liters by pre-concentrating radionuclides in a smaller sample volume with baromembrane method. This approach allows preliminary concentration of water samples from 500 l volume till 20 l volume during several hours. This approach is universal for the concentration of dissolved salts of any heavy metals, other organic compounds and allows the preparation of water countable samples in much shorter time compared to the traditional evaporation method.

Simple Fabrication of Green Emission and Water-Resistant CsPbBr3 Encapsulation Using Commercial Glass Frits (상업용 유리프릿의 소결 공정을 이용한 내수성을 갖는 CsPbBr3/Glass 세라믹 복합체의 제작)

  • Mun, Na-eun;Kim, Sunghoon
    • Korean Journal of Materials Research
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    • 제31권1호
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    • pp.54-59
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    • 2021
  • In this work, narrow-band green-emitting CsPbBr3 particles are embedded in commercialized glass composites by a facile dry process. By optimizing the method through sintering in glass frit (GF) composites including CsBr and PbBr2, used as precursors, the encapsulation of CsPbBr3 particles made them waterproof with green fluorescence. To improve the fluorescent properties by reducing aggregation of CsPbBr3, fumed silica (FS) is additionally used to help particles avoid bulking up in the glass matrix. The CsPbBr3 perovskite/glass composites are characterized using scanning electron microscopy (SEM) images and energy-dispersive X-ray spectroscopy (EDS) maps, which support the existence of CsPbBr3 particles in the glass matrix. The photoluminescence (PL) properties demonstrate that the emission spectrum peak, full width at half maximum (FWHM), and photoluminescence quantum yield (PLQY) values are 519 nm, 17 nm, and 17.7 %. We also confirm the water-resistant properties. To enhance water/moisture stability, the composite sample is put directly into water, with its PLQY monitored periodically under UV light.

A Study on the Subjectivity about Nursing Student's Attitude after Hand Washing Education (간호학과 학생들의 손씻기 교육 후 태도 유형에 관한 주관성 연구)

  • Kim, Yun-Jeong
    • Journal of Digital Convergence
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    • 제11권12호
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    • pp.621-630
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    • 2013
  • This study, after education for nursing students through texts on hand washing, PPT materials and practices, will investigated the types of the subjects' attitude toward hand washing and attempt to provide basic data needed for nursing education and nursing practice program. As the methods of this research, Q methodology was applied, and 20 sophomores in the Department of Nursing Science as P-sample from October 8, 2012 to October 15, 2012 were asked to distribute Q-sample of 9-point Q-sample distribution, and the collected data were processed with principal factor analysis method by the PC QUANL program. As a result of the research, their attitude toward hand washing was classified into 3 types. The three factors extracted all had eigenvalues greater than 1.0 and explained approximately 56.67% of the variation in responses 40.41%, 10.14% and 6.11% respectively. Type 1 was the ones with the increased number of hand washing; Type 2 was the ones who recognize the need of hand washing education; and Type 3 was the ones who dry hands after washing. In conclusion, the significance of the classification of the types of the attitude after the hand washing education is that with the development of programmes of nursing education and nursing practice, individualized intervention strategies should be differently provided.

Biomass Expansion Factors, Allometric Equations and Stand Biomass of Pinus thunbergii in Southern Korea (전남 여수지역 곰솔의 현존량 확장계수, 상대생장식 및 임분 현존량)

  • Park, In-Hyeop;Kim, So-Dam
    • Korean Journal of Environment and Ecology
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    • 제32권5호
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    • pp.507-512
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    • 2018
  • Three natural Pinus thunbergii stands in southern Korea were studied to investigate stem density, biomass expansion factors, allometric equations and stand biomass. Stand ages of stand 1, 2 and 3 were 15, 29 and 45 years old, respectively. Three $10m{\times}10m$ plots were set up, five sample trees were cut and roots of three sample trees were excavated for dimension analysis in each stand. Stem density of stand 1, 2 and 3 were $0.450g/cm^3$, $0.440/cm^3$ and $0.457g/cm^3$, respectively, and there was no significant difference among the three stands. Biomass expansion factors of above-ground and total tree decreased with increasing stand age. Above-ground biomass expansion factor of stand 1 was significantly higher than those of stand 2 and 3, and total tree biomass expansion factor of stand 1 was significantly higher than that of stand 3. Allometric equations were developed for the 15 sample trees of the three stands based on D or $D^2H$. Above-ground biomass of stand 1, 2 and 3 were 50.72t/ha, 89.92t/ha, 194.07t/ha, respectively, and total tree biomass of stand 1, 2 and 3 were 61.62t/ha, 113.12t/ha, 248.36t/ha, respetively.

A Study for Influence of Salt on Stabilized Marin Clay with Lime and Cement (해성점토의 석회 및 시멘트 안정처리에 미치는 염분의 영향)

  • 정두영;이병석
    • Geotechnical Engineering
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    • 제7권4호
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    • pp.49-64
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    • 1991
  • Abstract The stabilization by lime or Portland cement has long been the most commonly used methods for clay soil. But it wart the purpose of this reserch to define the effectiveness malt content on unconfined compressive strength of limeflay mixture and cementrlay mixture. From result of a laboratary investigation, saInt content in sample soil was not concernd with variation of PH value. PH value of lime 10% mixture and of cement 10% mixture were near 12.4, 11.6 respectively. In case of more than 7 curing days, PH value and Ca++ion concentration were decreased with increasing curing time. Also the result of X-ray difflection analysib for stabilized soil by admixture 10% in 90 curing days showed that the diffrection intensity of Tobermorite and Ettringite and other reaction products was smaller in the case of addition of salt 8% than malt 0% in stabilized soil. When lime-soil mixture and cement-boil mixture were cured in 2$0^{\circ}C$ and 5$^{\circ}C$, 2$0^{\circ}C$ cured mizture produced significantly higher compressive strength than 5t cured mixture and air dry curing sample produced higher than cured sample in water. The addition of salt 2~4% in conjuntion with lime or cement may accelerate strenth gain or not prevent front However, the addition of salt 8% prevent from strength gams.

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Effects of Combined Treatments of Lactic Acid Bacteria and Cell Wall Degrading Enzymes on Fermentation and Composition of Italian Ryegrass (Lolium multiflorum Lam.) Silage

  • Ridla, M.;Uchida, S.
    • Asian-Australasian Journal of Animal Sciences
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    • 제11권3호
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    • pp.277-284
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    • 1998
  • This experiment was carried out to study the effects of lactic acid bacteria (LAB) inoculation and addition of cell wall degrading enzymes on the fermentation characteristics and chemical compositions of Italian ryegrass silage. An inoculant LAB with or without a cell wall degrading enzyme of Acremoniumcellulase (A), or Meicellulase (M) or a mixture of both (AM), was applied to 1 kg of fresh Italian ryegrass sample. The treatments were control untreated, LAB-treated (application rate $10^5$ cfu/g fresh sample), LAB+A 0.005%, LAB + A 0.01%, LAB+A 0.02%, LAB + M 0.005%, LAB + M 0.01%, LAB + M 0.02%, LAB+AM 0.005%, LAB + AM 0.01% and LAB+AM 0.02%. The sample was ensiled into 2-L vinyl bottle silo, with 9 silages of each treatment were made (a total of 99 silages). Three silages of each treatment were incubated at 20, 30 and $40{^{\circ}C}$ for an approximately 2-months storage period. All silages were well preserved as evidenced by their low pH values (3.79-4.20) and high lactic acid concentrations (7.71-11.34% DM). The fermentation quality and chemical composition of the control untreated and the LAB-treated silages were similar, except that for volatile basic nitrogen (VBN) content was lower (p < 0.05) in the LAB-treated silages. LAB + cellulase treatments improved the fermentation quality of silages by decreasing (p < 0.01) pH values and increasing (p<0.01) lactic acid concentrations, in all of cellulase types and incubation temperatures. Increasing amount of cellulase addition resulted in further decrease (p < 0.01) of pH value and increases (p < 0.01) of lactic acid and residual water soluble carbohydrate (WSC) concentrations. LAB + cellulase treatments reduced (p<0.01) NDF, ADF, hemicellulose and cellulose contents of silages compared with both the control untreated and LAB-treated silages. LAB + cellulase treatments did not affect the silage digestibility due to fact of in vitro dry matter digestibility (IVDMD) was similar in all silages. The silages treated with cellulase A resulted in a better fermentation quality and a higher rate of cell wall reduction losses than those of the silages treated with cellulases M and AM. Incubation temperature of $30{^{\circ}C}$ seemed to be more suitable for the fermentation of Italian ryegrass silages than those of 20 and $40{^{\circ}C}$.

Separation of chlorine in a uranium compound by pyrohydrolysis and steam distillation, and its determination by ion chromatography (열가수분해 및 수증기증류에 의한 우라늄 화합물 중 염소 분리 및 이온크로마토그래피 정량)

  • Kim, Jung-Suk;Lee, Chang-Hun;Park, Soon-Dal;Han, Sun-Ho;Song, Kyu-Seok
    • Analytical Science and Technology
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    • 제23권1호
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    • pp.45-53
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    • 2010
  • For the determination of chlorine in uranium compound, analytical methods by using a steam distillation and a pyrohydrolysis have been developed. The steam distillation apparatus was composed of steam generator, distilling flask and condenser etc. The samples were prepared with an aliquot of LiCl standard solution and a simulated spent nuclear fuel. A sample aliquot was mixed with a solution containing 0.2 M ferrous ammonium sulfate-0.5 M sulfamic acid 3 mL, phosphoric acid 6 mL and sulfuric acid 15 mL. The chloride was then distilled by steam at the temperature of $140^{\circ}C$ until a volume of $90{\pm}5\;mL$ is collected. The pyrohydrolysis equipment was composed of air introduction system, water supply, quartz reaction tube, combustion tube furnace, combustion boat and absorption vessel. The chloride was separated from powdered sample which is added with $U_3O_8$ accelerator, by pyrohydrolysis at the temperature of $950^{\circ}C$ for 1 hour in a quartz tube with a stream of air of 1 mL/min supplied from the water reservoir at $80^{\circ}C$. The chlorides collected in each absorption solution by two methods was diluted to 100 mL and measured with ion chromatography to determine the recovery yield. For the ion chromatographic determination of chlorine in molten salt retained in a metal ingot, the chlorine was separated by means of pyrohydrolysis after air and dry oxidation, and grinding for the sample.

Behavior of Shear Strength of Coarse Grained Materials Based on Large Scale Direct Shear Test (I) (대형직접전단시험을 이용한 조립재료의 전단거동 특성 (I))

  • Lee Dae-Soo;Kim Kyoung-Yul;Hong Sung-Yun;Jo Hwa-Kyung;Whang Sung-Chun
    • Journal of the Korean Geotechnical Society
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    • 제21권6호
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    • pp.81-91
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    • 2005
  • 'Coarse grained material' refers to crushed stones or gravels, and the behaviour of soil containing coarse grained material is not easily defined using the conventional soil mechanics theory due to the influences of large particles, therefore large scale test is essential to investigate their effects. Previous studies have identified the major factors affecting the properties of coarse grained materials by using large scale shear testing apparatus, such as maximum particle size, water content, density and uniformity coefficients. In this paper, the effect of variation of maximum particle size and water content on shear strength was analyzed from the results of large scale shear test. In addition, the fiction coefficient at critical state per vertical load was estimated using the equation proposed by Wood (1998). The sample for the test was obtained from the local quarry sites. Tests results show that the shear strength for 50.8 m maximum particle size is relatively larger than that of 76.3 m and air-dry sample has larger shear strength than saturated sample. In the meantime, the friction coefficient at critical state shows $1.0\sim1.6$ according to the test conditions.

Microwave Vacuum Drying of Brown Rice Koji as an Enzymic Health Food (효소식품으로서 현미코오지의 마이크로파 진공건조)

  • Kim, Suk-Shin;Roh, Hoe-Jin;Kim, Sang-Yong
    • Korean Journal of Food Science and Technology
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    • 제31권3호
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    • pp.625-630
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    • 1999
  • This work was to study drying characteristics of the brown rice koji, an enzymic health food, using microwave under vacuum. Cooked brown rice was inoculated with Aspergillus oryzae and incubated at $32^{\circ}C$ for 6 days. The brown rice koji was dried by different drying methods: microwave vacuum drying, hot air drying, vacuum drying and freeze drying. Each drier except freeze drier was set to maintain the sample temperature at $40^{\circ}C$. During microwave vacuum drying, the sample reached $40^{\circ}C$ much faster (within $5{\sim}10\;min$) and was dried much faster (2 hrs) than the other drying methods. The initial drying rate of microwave vacuum drying was ten times faster than that of hot air drying. The microwave vacuum drying produced a dry sample of the highly retained enzymic activity, followed by freeze drying, vacuum drying, and hot air drying.

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