• Title/Summary/Keyword: Dry sample

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A Study on the Spontaneous Ignition Possibility of Shredded Waste Thermoplastic Elastomer (폐 열가소성 플라스틱 탄성체 분쇄물의 자연발화가능성에 관한 연구)

  • Park, Young Ju;Lee, Hae Pyeong;Goh, Kyoung Chun;Eom, Young Sup
    • Journal of the Korean Society of Safety
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    • v.31 no.1
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    • pp.61-65
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    • 2016
  • In this study, we considered the ignition possibility for the shredded thermoplastic elastomer at the fire ground loaded the waste TPE. The average moisture content of the TPE sample was almost 0.33 wt.% at $110^{\circ}C$ and the range of ignition point was $461.9{\sim}491.9^{\circ}C$ approximately. In addition, we analyzed the change of weight and calorie the TPE sample according to temperature variations using the TG-DTA analyzer. As a result, the weight loss occurred twice in $250{\sim}420^{\circ}C$ and $420{\sim}473^{\circ}C$, and we found the second weight loss temperature range was the ignition point of TPE. Also, we conducted the spontaneous ignition tests of TPE for the wet and dry samples and we confirmed that the possibility of spontaneous ignition of TPE was very low. The elapsed time and humidity had little influence on the spontaneous ignition of TPE in this experimental conditions. In conclusion, the spontaneous of the shredded waste TPE in this study.

The study of Phellodendron amurense Rupr. Dyeing (황벽의 염색성에 관한연구)

  • 소황옥
    • Journal of the Korean Society of Costume
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    • v.27
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    • pp.121-132
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    • 1996
  • This study showed the proper pigment extract in the Phe. Dyeing which is the basic dye of the natural plants dyeing,. Also it compared and examined the K/S the promotion of the color fastness and the effect of color difference change were attended by mordants and method of mordanting. 1. The most absorbance of Phellodendron. sol-ution is 330nm berberine is 430nm. 2. The best and proper temperature to extrat Phe,. was 80 and dyeing solution for 24 hours. 3. The pH effect was stable in the absorbances and color differences change. 4. Mordanted group increased the absorbances compared to non-mordanted sample. In case depth the most absorbance of Al. Sn. K. Cu and C. A solution were in 3% Fe and Cr were in 5%. In the color difference change they became dark reduced greenish and increased yellowish when their absorbances were in 3% 5. K./S was recoginzed by tainnin and fe, K/S was more increased pre-mordants than post-mordants. 6. Fe is the unchangable mordant in the color difference change and pre-mordants is more stable than post-mordants in the difference color. 7. Generally light C. F indicated more than grade 2 and light C. F, was much improved in post-mordanted by alumium potassium potass-ium dichromate. Washing C.F was improved in mordanted by tainnin and ferrous suulfate mordanted group was better than non-mordanted sample. Perspir-ation C,F was more stable in acid than alkali. Dry cleaning C.F indicated more than grade. 4.

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Development of Diagnostic kit for Hepatitis B Susrface Antigen using Immunochromatographic Assay Method (면역크로마토그래피법을 이용한 B형간염 진단용 kit의 개발)

  • 신형순;신광순;정홍근;허태련
    • KSBB Journal
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    • v.15 no.2
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    • pp.214-218
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    • 2000
  • A hepatitis B Surface Antigen(HBsAg)-screening kit using immunochromatographic assay(ICA) method was developed by e employing two kinds of antibodies. One is mouse monoclonal anti-HBs for tracer antibody and the other is goat p이yclonal a anti-HBs for capture antibody. This capture antibody was immobilized on the surface of nitroceliulose(NC) membrane and the t tracer antibody was conjugated with g미d particles. When serum sample was added to the sample well, the $\infty$njugates d deposited in a dry state on the surface of glass fiber filter were reconstituted and then combined with HBsAg in serum. In 5 5 min after adding, the assay result was visible through the window, that is, the complexes composed of HBsAg and the c conjugates appeared as maroon line on the lower part of the NC membrane. The detection limit of the ICA kit was 2 ng/ml w when being tested with the reference HBsAg.

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Ion Beam Assisted Deposition System의 제작 및 자동화

  • 손영호
    • Proceedings of the Korean Vacuum Society Conference
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    • 1998.02a
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    • pp.27-27
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    • 1998
  • 진공기술의 응용과 진공환경의 이용은 더 이상 논하지 않더라도 산업 전반에 그 충요성이 점점 더 커가고 있다. 이러한 여건에도 불구하고 진공율 이용하는 system 개밟의 국산화는 수 입하는 system으$\mid$ 수에 비하여 절대적으로 부족하며, 또한 개발하는 system의 자동화는 거의 이 루어지지 않고 있으며, 자동화된 진공판련 system은 거의 대부분 수입에 의흔하고 있다. 실험 실 규모에서부터 System올 하나하나 개밭하고, 이톨 자동화하는 노력과 일이 진행됨다면 산업 응용에 있어서도 자연스럽게 자동화된 system으$\mid$ 개발이 이루어 질 것이다 .. system 자동화는 상 품수명의 단축과 이에 따른 다품종 소량을 요구하는 시장수요에 대응하고, 인력절감과 고풀짙 화로 생산성 향상의 요구에 대응하기 위하여 필요하다. 본 연 구에 서 는 e-beam evaporator로 evaporation하면 서 ion beam으로 assist하여 thin film율 제 작하는 IBAD vacuum system율 싫 계 및 제 작하고[1,2], PLC[3,떼톨 이 용하여 system 자동화톨 하였다 .. thin film 제작 process는 먼저 기본 진공상태로 만뚫고 난 뒤, e-beam evaporator로 e evaporation하면서 ion beam source로 assist하여 substrate 011 thin film율 제조한다 226;. thin film올 제 조하면서 thickness monitor로 sample의 thickness rate톨 control 하고, sample의 균얼성과 밀착 성을 고려하여 substrate톨 rotation 및 heating 할 수 있도록 싫계, 제작하였다. 양질의 박막올 제조하기 위해서 진공환경이 좋은 상태로 제공되어야 한다. 이톨 위하여 oil free operation 0 I 가 능한 dry pump와 turbo molecular pump로 고진공 배기 하였다. 진공도의 흑점은 thermal effect 툴 고려하여 cold cathode ion gauge률 사용하였고, intro chamber와 main chamber 사이에는 g gate valve톨 설치하여 벌도로 운용되도록 하였다. 이러한 process를 박막의 두께, 진공도, 시 간, 온도, 공정 동의 조건올 기훈으로 자동화한 것이다. 또한 정전과 단수에 대한 interlock 기능 도 고려하였다.하였다.

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Coloration Conditions of Clay Minerals on Cotton Fabrics and Analysis of Components (면포에 대한 점토광물의 착색조건과 착색성분 분석)

  • Jung, Jong Sun;Song, Kyung Hun
    • Journal of the Korean Society of Clothing and Textiles
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    • v.38 no.5
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    • pp.665-674
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    • 2014
  • An analysis of the components of clay mineral before and after coloration (XRF) showed that the elements involved in coloration are Fe, Cr, and Ni. Fe accounts for 65% of coloring components on dyed fabric; in addition, Cr and Ni also affect coloring. The optimal coloration condition was to repeat the process of immersing the cotton fabric in $80^{\circ}C$ slurry of 8g of clay mineral to 1g cotton for 60 minutes, dry it for 24 hours and rinse three times. Especially, as the repetition of coloration increased, the $(K/S)_{440}$ value of sample A increased from 1.0 to 2.5, and sample B increased from 1.0 to 1.6. The effect of the repeated process on coloration was significant; consequently, the rinsing and drying process were important to decrease the coloration level. It also showed excellent results in regard to color fastness to washing, light, rubbing, perspiration, and antibiotic effect.

Preparation of Carbon Nanomaterial from the Microbial Cellulose (미생물 셀룰로오스로부터 탄소 나노물질의 제조)

  • Kim Bong Gyun;Sohng Jae Kyung;Liou Kwangkyoung;Lee Hei Chan
    • KSBB Journal
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    • v.20 no.1 s.90
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    • pp.50-54
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    • 2005
  • Tar is often produced during the carbonization of cellulose that limits the formation fibrous structure of the carbonized sample. This problem was reduced by applying a high temperature $(up\;to\;800{\circ}C)$ during carbonization process. Alternatively, dry cellulose was immersed in toluene and ultrasonicated prior to carbonization. In both cases, complete fibrous structures were not achieved. The formation of tar was reduced by the heat treatment of cellulose in the presence of HCI vapor before carbonization process. Such treatment before carbonization yielded mostly the fibrous structures of the carbonized sample as evident from SEM analysis. Similar results were found when the cellulose was subjected to a heat treatment in an inert condition followed by the removal of tar by the oxidation process prior to the carbonization.

An Experimental Study on the Compressive Strength of Ultra High Strength Concrete with Vacuum Water Absorbing Curing (진공포수양생을 적용한 초고강도 페이스트의 압축강도 발현에 관한 실험적 연구)

  • Jang, Jong-Min;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2019.11a
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    • pp.27-28
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    • 2019
  • In this study, the characteristics of compressive strength of ultra high strength concrete supplied with moisture from outside by vacuum water absorbing curing method were investigated. Specimens were prepared by replacing the binder(Silifa fume and GGBS) by 25 wt% with respect to the weight of cement at W/B 0.16. Each specimen was subjected to water Vacuum absorbing curing time 0 min, 30 min, 60 min, 90 min and 120 minutes immediately after the demolding. Curing was performed at $20^{\circ}C$ Air-dry curing, $90^{\circ}C$ steam curing, $90^{\circ}C$ steam curing and $180^{\circ}C$ autoclave curing. Experimental results showed that water absorbing degree increased with increasing water absorbing curing time, and BS25 sample had higher water absorbing degree than SF25 sample at same time. Compressive strength tended to increase up to about 40% in water absorbing degree, but compressive strength decreased again in water absorbing more than 40%.

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Distribution of Nonylphenol in Gwangyang Bay and the Surrounding Streams (광양만 및 주변 하천에서의 노닐페놀 화합물 분포)

  • 이동호;김민선;심원준;임운혁;홍상희;오재룡
    • Korean Journal of Environmental Biology
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    • v.22
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    • pp.71-77
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    • 2004
  • Alkylphenols (8), chlorophenols (2), bisphenol A, eoprostanols (2) and cholesterol compounds were analyzed in the surface water and surface sediment taken from Gwangyang Bay and surrounding streams in 2001. Among the target analytes, nonylphenol and dihydrocholesteyol compounds were detected with high concentration and high frequency. t-Octylphenol, bisphenol A and coprostanols were detected only in some sediment samples from the stream. The highest concentration of nonylphenol was determined in stream sample, and concentrations of nonylphenol in the inner part of Gwangyang Bay were higher than those in the out part. Nonylphenol concentrations in the surface seawater and surface sediment samples ranged from 4.0 to 74.0 ng l$\^$-1/ and from 3.1 to 74.3 ng g$\^$-1/ dry wt., respectively. Partition coefficient (LogK$\_$oc/) of nonylphenol between sediment and water was 4.8. Nonylphenol nnd dihydrocholesteol concentrations in the stream surface sediment samples ranged from 4.6 to 808.6 and from 78.4 to 1133.6 ng g$\^$-1/ dry wt., respectively. Relatively high concentrations of nonylphenol were found in the stream samples which aye flowing through industrial complex area, while dihydrocholesterol concentration was relatively high in the stream samples which are flowing through only municipal area. Seaward decreasing tyend in nonylphenol concentration was observed from the Seomjin River estuary to the Gwanyang Bay. Such trend was best supported by the strong correlation between nonylphenol concentration and salinity in water samples.

Quality Characteristics of Backsulgi with Dextrinized Rice (호정화에 의한 백설기의 품질특성)

  • Doo, Hwa-Jin;Lee, Eun-Suk;Kim, Yong-Ro;Shim, Jae-Yong
    • Food Engineering Progress
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    • v.13 no.4
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    • pp.289-296
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    • 2009
  • The purpose of this study was to investigate the effect of dextrinization methods (dry oven and roaster) and the ratio of dextrinized rice on the quality of Backsulgi during storage. The moisture content significantly increased with increasing the amount of dextrinized rice regardless of dextrinization methods. As the ratio of dextrinized rice increased, the L value of the Backsulgi decreased, but the a and b values increased. The a and b values of dry oven method were higher than those of roaster method due to their thermal denaturalization. However, there were no significant pattern's change in sample's colors during storage. In the texture profiles, the hardness, cohesiveness, gumminess and chewiness significantly decreased with increasing the amount of dextrinized rice depending on the dextrinization methods and the ratios. The time constant (1/k) of the Backsulgi with dextrinized rice comparatively higher than that of control and appeared to be the highest in the Backsulgi formulated by 100% of dextrinized rice. In the sensory evaluation, Backsulgi with dextrinized rice over 30% after 1day storage showed higher value in overall quality and lower value in hardness than control. The addition of 30% dextrinized rice made by roaster showed the most effective on the quality and retrogradation of Backsulgi.

Measurement of lipid content of compost fermentation using near-infrared spectroscopy

  • Daisuke Masui;Suehara, Ken-ichiro;Yasuhisa Nakano;Takuo Yano
    • Near Infrared Analysis
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    • v.2 no.1
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    • pp.37-42
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    • 2001
  • Near infrared spectroscopy (NIRS) was applied to determination of the lipid content of the compost during the compost fermentation of tofu (soybean0curd) refuse. The absorption of lipid observed at 5 wavelengths, 1208, 1712, 1772, 2312 and 2352 nm on the second derivative spectra. To formulated a calibration equation, a multiple linear regression analysis was carried out between the near-infrared spectral data and on the lipid content in the calibration sample set (sample number, n=60) obtained using Soxhlet extraction method. The value of the multiple correlation coefficient (R) was 0.975 when using the wavelengths of 1208 and 1712 nm were used in the calibration equation. To validate the calibration equation obtained, the lipid content in the validation sample set (n=35) not used for formulating the calibration equation was calculated using the calibration equation, and compared with the value obtained using the Soxhlet extraction method. Good agreement was observed between the results of the Soxhlet extraction method and those values of the NIRS method. The simple correlation coefficient (r) and standard error of prediction (SEP) were 0.964 and 0.815 %, respectively. suitability of the lipid content as an indicator of the compost fermentation of tofu refuse was also studied. The decrease of the lipid content in the compost corresponded to the decrease of the total dry weight of the compost in the composter. The lipid content was a significant indicator of the compost fermentation. The NIRS method was applied to measure the time course of the lipid content in the compost fermentation and good results were obtained. The study indicates that NIRS is a useful method for process management of the compost fermentation of tofu refuse.