• Title/Summary/Keyword: Double extraction process

Search Result 18, Processing Time 0.024 seconds

Preparation by the double extraction process with preliminary neutron irradiation of yttria or calcia stabilised cubic zirconium dioxide microspheres

  • Brykala, Marcin;Walczak, Rafal;Wawszczak, Danuta;Kilim, Stanislaw;Rogowski, Marcin;Strugalska-Gola, Elzbieta;Olczak, Tadeusz;Smolinski, Tomasz;Szuta, Marcin
    • Nuclear Engineering and Technology
    • /
    • v.53 no.1
    • /
    • pp.188-198
    • /
    • 2021
  • A modern approach to nuclear energy involves reprocessing like transmutations of spent nuclear fuel products to reduce their radiotoxicity and time needed for their storage. For this purpose, they are immobilized in inert matrices made of zirconia and can be "burned" in fast neutron reactor or Accelerator Driven System. These matrices in spherical form can be obtained by sol-gel process. The paper presents a method of microspheres fabrication based on the combined Complex Sol-Gel Process and double extraction process consisting in the preparation of zirconium-ascorbate sol and simultaneous extraction of water and nitrates. The procedure allows obtaining gel microspheres with a diameter of 50 ㎛, which after heat treatment are processed into the final product. The synthesis of zirconia microspheres with Yttrium by internal gelation process is well known for over a decade now. However, the explanation and characterization of synthesis of such material by extraction of water process is rarely found. Parameters such as: pH, viscosity, shape, sphericity and crystal structure have been determined for synthesized products and semi-products. In addition, preliminary research consisting in irradiation of the obtained materials in fast and thermal neutron flux was carried out. The obtained results are presented and described in this work.

Tobacco Retail License Recognition Based on Dual Attention Mechanism

  • Shan, Yuxiang;Ren, Qin;Wang, Cheng;Wang, Xiuhui
    • Journal of Information Processing Systems
    • /
    • v.18 no.4
    • /
    • pp.480-488
    • /
    • 2022
  • Images of tobacco retail licenses have complex unstructured characteristics, which is an urgent technical problem in the robot process automation of tobacco marketing. In this paper, a novel recognition approach using a double attention mechanism is presented to realize the automatic recognition and information extraction from such images. First, we utilized a DenseNet network to extract the license information from the input tobacco retail license data. Second, bi-directional long short-term memory was used for coding and decoding using a continuous decoder integrating dual attention to realize the recognition and information extraction of tobacco retail license images without segmentation. Finally, several performance experiments were conducted using a largescale dataset of tobacco retail licenses. The experimental results show that the proposed approach achieves a correction accuracy of 98.36% on the ZY-LQ dataset, outperforming most existing methods.

Optimized Design of Dioxin Analysis for Water Sample

  • Choi, Jaewon;Lee, Jaehee;Kim, Kyoungsim;Kim, Sunheong;Bae, Kyunghee
    • Journal of Korean Society on Water Environment
    • /
    • v.21 no.3
    • /
    • pp.219-229
    • /
    • 2005
  • The analytical methods for dioxins in water sample from wastewater to tap water were reviewed. For extraction method, liquid-liquid extraction (LLE) has been widely used, however, this process needs too much time and man power. New approach including solid phase extraction (SPE) is now applicable to large volume of water sample with high extraction efficiency. Column clean up in classical analytical methods were very complex and time consuming procedures during decade. Modifications were tried to decrease solvent and reagents volume. Moreover, use of column connection method has been demonstrated in the environmental matrices. Instrumental configurations also have been improved, in which GC/MS/MS with large volume injection approach can analyze picogram levels. Absolute sensitivities of HRMS increased compared to old versions of double focusing sector type mass spectrometers. Based on these analytical evolutions during last 10 years, we tried to optimize the analytical method for dioxins in water sample from sample extraction to instrumental analysis.

Alveolar ridge preservation with an open-healing approach using single-layer or double-layer coverage with collagen membranes

  • Choi, Ho-Keun;Cho, Hag-Yeon;Lee, Sung-Jo;Cho, In-Woo;Shin, Hyun-Seung;Koo, Ki-Tae;Lim, Hyun-Chang;Park, Jung-Chul
    • Journal of Periodontal and Implant Science
    • /
    • v.47 no.6
    • /
    • pp.372-380
    • /
    • 2017
  • Purpose: The aim of this prospective pilot study was to compare alveolar ridge preservation (ARP) procedures with open-healing approach using a single-layer and a double-layer coverage with collagen membranes using radiographic and clinical analyses. Methods: Eleven molars from 9 healthy patients requiring extraction of the maxillary or mandibular posterior teeth were included and allocated into 2 groups. After tooth extraction, deproteinized bovine bone mineral mixed with 10% collagen was grafted into the socket and covered either with a double-layer of resorbable non-cross-linked collagen membranes (DL group, n=6) or with a single-layer (SL group, n=5). Primary closure was not obtained. Cone-beam computed tomography images were taken immediately after the ARP procedure and after a healing period of 4 months before implant placement. Radiographic measurements were made of the width and height changes of the alveolar ridge. Results: All sites healed without any complications, and dental implants were placed at all operated sites with acceptable initial stability. The measurements showed that the reductions in width at the level 1 mm apical from the alveolar crest (including the bone graft) were $-1.7{\pm}0.5mm$ in the SL group and $-1.8{\pm}0.4mm$ in the DL group, and the horizontal changes in the other areas were also similar in the DL and SL groups. The reductions in height were also comparable between groups. Conclusions: Within the limitations of this study, single-layer and double-layer coverage with collagen membranes after ARP failed to show substantial differences in the preservation of horizontal or vertical dimensions or in clinical healing. Thus, both approaches seem to be suitable for open-healing ridge preservation procedures.

The hidden X suture: a technical note on a novel suture technique for alveolar ridge preservation

  • Park, Jung-Chul;Koo, Ki-Tae;Lim, Hyun-Chang
    • Journal of Periodontal and Implant Science
    • /
    • v.46 no.6
    • /
    • pp.415-425
    • /
    • 2016
  • Purpose: The present study investigated the impact of 2 different suture techniques, the conventional crossed mattress suture (X suture) and the novel hidden X suture, for alveolar ridge preservation (ARP) with an open healing approach. Methods: This study was a prospective randomized controlled clinical trial. Fourteen patients requiring extraction of the maxillary or mandibular posterior teeth were enrolled and allocated into 2 groups. After extraction, demineralized bovine bone matrix mixed with 10% collagen (DBBM-C) was grafted and the socket was covered by porcine collagen membrane in a double-layer fashion. No attempt to obtain primary closure was made. The hidden X suture and conventional X suture techniques were performed in the test and control groups, respectively. Cone-beam computed tomographic (CBCT) images were taken immediately after the graft procedure and before implant surgery 4 months later. Additionally, the change in the mucogingival junction (MGJ) position was measured and was compared after extraction, after suturing, and 4 months after the operation. Results: All sites healed without any complications. Clinical evaluations showed that the MGJ line shifted to the lingual side immediately after the application of the X suture by $1.56{\pm}0.90mm$ in the control group, while the application of the hidden X suture rather pushed the MGJ line slightly to the buccal side by $0.25{\pm}0.66mm$. It was demonstrated that the amount of keratinized tissue (KT) preserved on the buccal side was significantly greater in the hidden X suture group 4 months after the procedure (P<0.05). Radiographic analysis showed that the hidden X suture had a significant effect in preserving horizontal width and minimizing vertical reduction in comparison to X suture (P<0.05). Conclusions: Our study provided clinical and radiographic verification of the efficacy of the hidden X suture in preserving the width of KT and the dimensions of the alveolar ridge after ARP.

The comparative study of two extraction methods for ancient DNA: silica suspension method and ultracentrifugal concentrator method (고대 유전자에 대한 두 종류의 DNA 분리 방법의 비교 연구: 실리카 현탁액 방법 및 초원심분리 농축 방법)

  • Lee, Eun-jung;Maixner, Frank;Zink, Albert
    • Analytical Science and Technology
    • /
    • v.31 no.2
    • /
    • pp.65-70
    • /
    • 2018
  • This study compared two methods for preparing ancient DNA (aDNA) for the construction of successful shotgun libraries that may be applied to massive parallel sequencing. For the comparative analysis, the DNA of prehistoric rib samples from Hungary was extracted using either a manually prepared silica suspension or the Amicon Ultracel-15 10K ultracentrifugal device (Millipore). After the extraction of the same amount of bone powder (about 150 mg) from three samples by each method, the amount of extracted double-stranded DNA and the subsequent degree of construction of the shotgun library were analyzed. The Amicon device method was rapid and easier to perform and resulted in an approximately 11-fold higher DNA recovery than that obtained using the silica suspension. The shotgun library constructed using DNA templates prepared by the Amicon device was more successful than that constructed from templates isolated using the silica suspension. The comparative study of these two aDNA extraction methods showed that the Amicon device has the advantages of saving time, process simplicity, and high efficiency.

A Study on Image Pattern Recognition using Attributed Relational Graph (Attributed Relational Graph를 이용한 영상 패턴의 인식에 관한 연구)

  • Lee, Kwang-Kee;Jeon, Joong-Nam;Lee, Chang-Han;Lie, Han-Wook;Park, Kyu-Tae
    • Proceedings of the KIEE Conference
    • /
    • 1988.07a
    • /
    • pp.687-690
    • /
    • 1988
  • Algorithms that represent given pattern in the form of an ARG (Attributed relational graph) using not only structural relations but also symbolic or numerical attributes, and then recognize that pattern by graph matching process are presented in this paper. Based on definitions of pattern deformational models, algorithms that can find GPECI(Graph preserved error correcting isomorphism). SGECI(subgraph ECI) and DSECI(Double subgraph ECI) are proposed and comparisons among these algorithms are described. To be useful in performig practical tasks, efficient schemes for extraction of ARG representation fron raw image are needed. In this study, given patterns are restricted within objects having distinct skeleton, and then the information which is necessary for recognition and analysis is successfully extracted.

  • PDF

Physical Property and Extraction of Squalene and Alkoxyglycerol from Shark Liver Oil (상어간유에서 스쿠알렌과 알콕시글리세롤의 물성 및 추출)

  • Lee, Su Il;Heo, Hyo Jung;Row, Kyung Ho
    • Korean Chemical Engineering Research
    • /
    • v.49 no.5
    • /
    • pp.617-622
    • /
    • 2011
  • A simple method has been successfully applied to extract squalene and its byproducts alkoxyglycerol from deep-sea shark liver oil. GC-MS was used to determine the extraction amount of the squalene and alkoxyglycerol, and the content of them in rough product and refined product were compared. The physical property of squalene was identified by measuring the pH value, peroxide value and iodine value. Under optimum extraction conditions, the amount of squalene and alkoxyglycerol increased 35.0% and 21.9%, respectively, while the amount of fatty acid decreased from 61% to 4%, especially, the amount of palmitic acid and oleic acid remarkably decreased. Large amount of peroxide and acid were removed from shark liver oil after refining process. Because squalene contains lots of double bond, so the value of iodine is much higher than squalane.

An Evaluation of Changes in the Allergenicity of Kochujang upon Preparation Using Aloe Extract

  • Son, Bo-Kyung;Huh, Yoon-Ee;Kim, Jung-Yun;Noh, Geon-Woong;Lee, Sang-Sun
    • Nutritional Sciences
    • /
    • v.9 no.4
    • /
    • pp.317-322
    • /
    • 2006
  • Soybeans are well-known as allergenic foods. Koreans consume large amounts of soybean foods, such as kochujang, which have gone through the fermentation process. To lower the allergenicity of these foods, we prepared hypo allergenic kochujang with aloe extract (AK). A sensory evaluation was conducted along with a clinical evaluation that used a double-blind, placebo-controlled food challenge (DBPCFC) test These tests were designed to evaluate the acceptability of the fermented foods. In comparison to normal kochujang (NK), AK elicited a higher sensory test score, and the rate of positive reactions in atopic dermatitis patients during the DBPCFC test was reduced. Methods of protein extraction, protein quantitation with sodium dodecyl sulphate polyacrylamide gel electrophoresis (SDS-PAGE), and protein identification using two-dimensional (2D) gel electrophoresis were performed for both NK and AK to compare the functional factors. We found a reduction in the levels of high molecular proteins even though the bands of the proteins had not entirely disappeared, indicating that the boiling and fermentation process changed the soybean protein patterns. The rate of the reduction of high molecular proteins was more effective in the AK. In conclusion, AK can be recognized as a food with hypoallergenic effect.

A Study on the Cartographic Generalization of Stream Networks by Rule-based Modelling (규칙기반 모델링에 의한 하계망 일반화에 관한 연구)

  • Kim Nam-Shin
    • Journal of the Korean Geographical Society
    • /
    • v.39 no.4
    • /
    • pp.633-642
    • /
    • 2004
  • This study tries to generalize the stream network by constructing rule-based modelling. A study on the map generalization tends to be concentrated on development of algorithms for modification of linear features and evaluations to the limited cartographic elements. Rule-based modelling can help to improve previous algorithms by application of generalization process with the results that analyzing mapping principles and spatial distribution patterns of geographical phenomena. Rule-based modelling can be applied to generalize various cartographic elements, and make an effective on multi-scaling mapping in the digital environments. In this research, nile-based modelling for stream network is composed of generalization rule, algorithm for centerline extraction and linear features. Before generalization, drainage pattern was analyzed by the connectivity with lake to minimize logical errors. As a result, 17 streams with centerline are extracted from 108 double-lined streams. Total length of stream networks is reduced as 17% in 1:25,000 scale, and as 29% in 1:50,000. Simoo algorithm, which is developed to generalize linear features, is compared to Douglas-Peucker(D-P) algorithm. D-P made linear features rough due to the increase of data point distance and widening of external angle. But in Simoo, linear features are smoothed with the decrease of scale.