• Title/Summary/Keyword: Distillation temperature

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Development of 3th Effects Evaporative desalination system for Solar Desalination System (태양에너지 해수담수화를 위한 3중 효용 증발식 담수기 개발)

  • Hwang, In-Seon;Joo, Hong-Jin;Yun, Eung-Sang;Kwak, Hee-Youl
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.06a
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    • pp.201-201
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    • 2010
  • The evaporative desalination system with solar energy would be the efficient and attractive method to get fresh water. This study was described the development of Multi Effect Distillation(MED) with solar energy desalination system. The system was designed and manufactured Multi effect distillation on the capacity of $3m^3$/day. The experimental apparatus consists mainly of ejector pump, Hot water pump, flow meter, demister, cooler, evaporator and condenser. Evaporator and condenser were made Shell&Tube Heat Exchanger type with corrugated tube. The experimental variables were chosen $75^{\circ}C$ for hot water inlet temperature, 40, 60 and $80{\ell}$/min for hot water inlet volume flow rate, 6.0 and $8.0{\ell}$/min for evaporator feed seawater flow rate, $18^{\circ}C$ for sea water inlet temperature to cover the average sea water temperature and the salinity of sea water is measured about 33,000 PPM (parts per million). for a year in Korea. This study was analyzed the results of thermal performance of Multi Effect Distillation. The results are as follows, The experimental Multi effect distillation is required about 40 kW heat source for production of $3m^3$/day fresh water. Various operating flow rate was confirm in the experiments to get the optimum design data and the results showed that the optimum total flow was $8.0{\ell}$/min. Comparison of Single Effect Distillation with Multi Effect Distillation showed MED is at least more than double of SED.

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Process Optimization Using Regression Analysis of Distillation Processes for the Recovery of Propylene Glycol Monomethyl Ether Acetate (PGMEA) Containing Waste Organic Solvent (폐액 중 프로필 글리콜 모노메틸 에테르 아세테이트(PGMEA) 회수하는 증류공정에서 회귀분석을 이용한 공정 최적화)

  • Choi, Yong-Seok;Byun, Hun-Soo
    • Korean Chemical Engineering Research
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    • v.53 no.2
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    • pp.181-192
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    • 2015
  • The aim of this study is to obtain optimum process condition for using two tower distribution to recycle the waste Propylene Glycol Monomethyl Ether Acetate (PGMEA) that is formed after washing LCD. The optimum process condition for the content of PGMEA, which is dependent variable, at 1st distillation was calculated according to Bottom temperature (BTM temperature), Reflux amount, Feed amount, Feed temperatures, and the optimum process conditions and optimum factors for the content of PGMEA at 2nd distillation according to Bottom temperature (BTM temperature), Reflux amount, Feed amount, Feed temperatures. At 1st distillation, Reflux amount, Feed amount, and Feed temperature are significant variables. However, it is found that the BTM temperature range is not significant in the range of process condition used in this study. The optimum process conditions are based on $5700{\ell}$ of Feed amount, $2500{\ell}$ of Reflux amount, $165^{\circ}C$ of BTM temperature, and $130^{\circ}C$ of Feed temperature. For the this condition, the predicted content of PGMEA was calculated as 92.12~94.62%. Significant factors at 2nd distillation are Reflux amount, Feed amount, and BTM temperature. Multicollinearity is between Reflux amount and BTM temperature. BTM was omitted in the multiple regression equation because there is a strong positive correlation between Reflux amount and BTM temperature. Base on $199^{\circ}C$ of BTM temperature, The optimum process conditions are based on $4275{\ell}$ of Feed amount, $6200{\ell}$ of Reflux amount and $130^{\circ}C$ of Feed temperature. In this condition, the predicted content of PGMEA was calculated as 99.0~99.5%.

Design and control of extractive distillation for the separation of methyl acetate-methanol-water

  • Wang, Honghai;Ji, Pengyu;Cao, Huibin;Su, Weiyi;Li, Chunli
    • Korean Journal of Chemical Engineering
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    • v.35 no.12
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    • pp.2336-2347
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    • 2018
  • The azeotrope of methyl acetate methanol and water was isolated using extractive distillation with water as entrainer. The pressure-swing extractive distillation (PSED) process and vapor side-stream distillation column (VSDC) with the rectifier process were designed to separate the methyl acetate, methanol and water mixture. It was revealed that the VSDC with the rectifier process had a reduction in energy consumption than the PSED process. Four control schemes of the two process were investigated: Double temperature control scheme (CS1), $Q_R/F$ feedforward control of reboiler duty scheme for PESD (CS2), $Q_R/F$ feedback control scheme for VSDC (CS3), the feedback control scheme of sensitive plate temperature of side-drawing distillation column to dominate the compressor shaft speed (CS4). Feed flow and composition disturbance were used to evaluate the dynamic performance. As a result, CS4 is a preferable choice for separation of methyl acetate-methanol-water mixture. A control scheme combining the operating parameters of dynamic equipment with the control indicators of static equipment was proposed in this paper. It means using the sensitive plate temperature of side-drawing column to control the compressor shaft speed. This is a new control scheme for extractive distillation.

Development of Multi Effect Distillation for Solar Thermal Seawater Desalination System (태양열 해수담수화 시스템을 위한 다중효용 담수기 개발)

  • Joo, Hong-Jin;Hwang, In-Seon;Kwak, Hee-Youl
    • Journal of the Korean Solar Energy Society
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    • v.31 no.1
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    • pp.1-7
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    • 2011
  • This study was accomplished to evaluate the performance of Multi Effect Distillation(MED) for solar thermal desalination system. It was designed Multi effect distillation with $3m^3$/day capacity and Shell&Tube type heat exchanger. Also, The effective heat transfer of Shell&Tube heat exchanger was used Cu(90%)-Ni(10%) corrugated tube. The parameters relating to the performance of Multi Effect Distillation are known as hot water flow rate. The experimental conditions for each parameters were $18^{\circ}C$ for sea water inlet temperature, $6m^3$/hour sea water inlet volume flow rate, $75^{\circ}C$ for hot water inlet temperature, 2.4, 3.6, and $4.8\;m^3$/hour for hot water inlet volume flow rate, respectively. The results are as follows, Development for Multi effect distillation was required about 40kW heat and 35kW cooling source to produce $3m^3$/day of fresh water. Based on the results of this study, It makes possible to secure economics of desalination system with solar energy which is basically needed development of high efficiency fresh water generator.

The Prospect of Membrane Distillation (Membrane Distillation의 전망)

  • 조한욱;신우철
    • Membrane Journal
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    • v.7 no.2
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    • pp.57-64
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    • 1997
  • Membrane Distillation(MD) is reviewed as an application to new separation technology. Hydrophobic membrane which has been used to microfiltration is feasible material for MD process. MD has perfect selectivity under moderate temperature and is promised to simplify typical water treatment process. The principle of MD separation is phase transition by vapor-liquid interface at the pore of membrane surface. Feed and permeate temperature, composition, membrane wetting, heat and mass transfer phenomena affect the selectivity and flux of MD.

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Membrane distillation of power plant cooling tower blowdown water

  • Ince, Elif;Uslu, Yasin Abdullah
    • Membrane and Water Treatment
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    • v.10 no.5
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    • pp.321-330
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    • 2019
  • The objective of this study was to examine the recovery of the power plant cooling tower blowdown water (CTBD) by membrane distillation. The experiments were carried out using a flat plate poly vinylidene fluoride (PVDF) membrane with a pore diameter of $0.22{\mu}m$ by a direct contact membrane distillation unit (DCMD). The effects of operating parameters such as transmembrane temperature difference (${\Delta}T$), circulation rate and operating time on permeate flux and membrane fouling have been investigated. The results indicated that permeate flux increased with increasing ${\Delta}T$ and circulation rate. Whereas maximum permeate flux was determined as $47.4L/m^2{\cdot}h$ at ${\Delta}T$ of $50^{\circ}C$ for all short term experiments, minimum permeate flux was determined as $7.7L/m^2{\cdot}h$ at ${\Delta}T$ of $20^{\circ}C$. While $40^{\circ}C$ was determined as the optimum ${\Delta}T$ in long term experiments. Inorganic and non-volatile substances caused fouling in the membranes.

A Simple Distillation Process Produce Fuel from Plastic Waste using Incorporate Heat Source

  • Thawichsri, Kosart;nilnont, Wanich
    • International journal of advanced smart convergence
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    • v.4 no.1
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    • pp.127-136
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    • 2015
  • This paper is a study of a simple distillation process. Its objective is to compare fuel production from plastic waste, its data collecting is from the factory and simple data calculated a suitable evaluation on the simple distillation plant built before calculation. The experiment with a simple distillation process is separated into three sections. The first section is a simple distillation process of distillation producing diesel using heat source by biomass. The second section is distillation process which produces fuel using heat source by burner. The third section uses heat source by burner incorporate with biomass. The experiment reveals that the result of the second section is the most efficient. In comparison with the experiments and the simple calculation, the result on the efficiency of work has error less than 5% and it is sufficient for the next experimental process. Thus, the study and design on a simple distillation process produces fuel from plastic waste has to concern mainly on design heat exchangers, flow rate and optimized temperature. Further study on this plant can be developed throughout the county due to its low cost and efficiency.

Effect of the Crucible Cover on the Distillation of Cadmium

  • Kwon, S.W.;Jung, J.H.;Lee, S.J.
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2019.05a
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    • pp.69-69
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    • 2019
  • The distillation of liquid cathode is necessary to separate cadmium from the actinide elements in the pyroprocessing since the actinide deposits are dissolved or precipitated in a liquid cathode. It is very important to avoid a splattering of cadmium during evaporation due to the high vapor pressure. Several methods have been proposed to lower the splattering of cadmium during distillation. One of the important methods is an installation of crucible cover on the distillation crucible. A multi-layer porous round cover was proposed to avoid a cadmium splattering in our previous study. In this study, the effect of crucible cover on the cadmium distillation was examined to develop a splatter shield. Various surrogates were used for the actinides in the cadmium. The surrogates such as bismuth, zirconia, and tungsten don't evaporate at the operational temperature of the Cd distiller due to their low vapor pressures. The distillation experiments were carried out in a crucible equipped with cover and in a crucible without cover. About 40 grams of Cd was distilled at a reduced pressure for two hours at various temperatures. The mixture of the cadmium and the surrogate was heated at $470{\sim}620^{\circ}C$. Most of the bismuth remained in the crucible equipped with cover after distillation under $580^{\circ}C$ for two hours, whereas small amount of bismuth decreased in the crucible without cover above $580^{\circ}C$. The liquid bismuth escaped with liquid cadmium drop from the crucible without cover. It seems that the crucible cover played a role to prevent the splash of the liquid cadmium drop. The effect of the cover was not clear for the tungsten or zirconia surrogate since the surrogates remained as a solid powder at the experimental temperature. From the results of this work, it can be concluded that the crucible cover can be used to minimize the deposit loss by prevention of escape of liquid drop from the crucible during distillation of liquid cathode.

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Study on the Distillation of Magnesium Alloy Scrap (마그네슘 합금 스크랩의 진공증류에 관한 연구)

  • Wi, Chang-Hyun;Yoo, Jung-Min;Jang, Byoung-Lok;You, Byoung-Don
    • Korean Journal of Metals and Materials
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    • v.46 no.1
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    • pp.13-19
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    • 2008
  • To develop a recycling process of magnesium alloy scrap, a fundamental study on the distillation of magnesium alloy melt was carried out. Melt temperature, vacuum degree and reaction time were considered as experimental variables. The amount of vaporized magnesium melt per unit surface area of melt increases with the increase of melt temperature, reaction time and vacuum degree. The vapor condensed at the tip of water cooling Cu-condenser as a form of pine cone. Magnesium and zinc were vaporized easily from the melt. However, It's difficult to separate magnesium and zinc by vacuum distillation because vapor pressure of zinc is similar to one of magnesium. The contents of aluminum, manganese and iron, etc. in residual melt increase due to the decrease of magnesium and zinc content after the distillation of magnesium alloy.

The Effect of T90 Temperature on Exhaust Emissions in Low-temperature Diesel Combustion (저온 디젤 연소에서 T90 온도가 배기가스에 미치는 영향)

  • Han, Man-Bae
    • Transactions of the Korean Society of Automotive Engineers
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    • v.19 no.4
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    • pp.72-77
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    • 2011
  • This study is to investigate the effect of the distillation temperature in ultra low sulfur diesel fuel on exhaust emissions in the low-temperature diesel combustion with 1.9L common rail direct injection diesel engine. Low temperature diesel combustion was achieved by adopting an external high EGR rate with a strategic injection control. The engine was operated at 1500 rpm 2.6 bar BMEP. The 90% distillation recovery temperature (T90) was $270^{\circ}C$ and $340^{\circ}C$ for the respective cetane number (CN) 30 and 55. It was found that there exists no distinctive discrepancy on exhaust emissions with regards to the different T90s. The high CN (CN55) fuels follow the similar trend of exhaust emissions as observed in CN30 fuels' except that high T90 fuel (CN55-T340) produced higher PM compared to low T90 fuel (CN55-T270). This may come from that high T90 plays an active role in aggravating the degree of fuel-air mixture preparedness before ignition.