• 한국분말재료학회지
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• 제31권3호
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• pp.255-262
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• 2024

Nano-oxide dispersion-strengthened (ODS) superalloys have attracted attention because of their outstanding mechanical reinforcement mechanism. Dispersed oxides increase the material's strength by preventing grain growth and recrystallization, as well as increasing creep resistance. In this research, atomic layer deposition (ALD) was applied to synthesize an ODS alloy. It is useful to coat conformal thin films even on complex matrix shapes, such as nanorods or powders. We coated an Nb-Si-based superalloy with TiO₂ thin film by using rotary-reactor type thermal ALD. TiO₂ was grown by controlling the deposition recipe, reactor temperature, N₂ flow rate, and rotor speed. We could confirm the formation of uniform TiO₂ film on the surface of the superalloy. This process was successfully applied to the synthesis of an ODS alloy, which could be a new field of ALD applications.

• 한국재료학회지
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• 제29권4호
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• pp.271-276
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• 2019

Oxide-dispersion-strengthened (ODS) alloy has been developed to increase the mechanical strength of metallic materials; such an improvement can be realized by distributing fine oxide particles within the material matrix. In this study, the ODS layer was formed in the surface region of Zr-based alloy tubes by laser beam treatment. Two kinds of Zr-based alloys with different alloying elements and microstructures were used: KNF-M (recrystallized) and HANA-6 (partial recrystallized). To form the ODS layer, $Y_2O_3$-coated tubes were scanned by a laser beam, which induced penetration of $Y_2O_3$ particles into the substrates. The thickness of the ODS layer varied from 20 to $55{\mu}m$ depending on the laser beam conditions. A heat affected zone developed below the ODS layer; its thickness was larger in the KNF-M alloy than in the HANA-6 alloy. The ring tensile strengths of the KNF-M and HANA-6 alloy samples increased more than two times and 20-50%, respectively. This procedure was effective to increase the strength while maintaining the ductility in the case of the HANA-6 alloy samples; however, an abrupt brittle facture was observed in the KNF-M alloy samples. It is considered that the initial microstructure of the materials affects the formation of ODS and the mechanical behavior.

• 한국산업경영시스템학회:학술대회논문집
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• 한국산업경영시스템학회 2002년도 춘계학술대회
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• pp.37-44
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• 2002

In order to review the failure rate of PC monitor under normal environmental conditions, we experimented for various levels of each factors, e.g Power on/off, DPM mode, using voltage, Incoming Surge, Torque strength etc. According to the results of experiment and SN ratios we investigated that the causes of the failure for the horizontal output TR of monitor are Mode change, dispersion of Torque and $h_{FE}$ and these are critical effect. For the new reliability test we suggested that strengthened part tests In IQC branch, Torque change controls in the TR specification are necessary.

• 한국분말재료학회지
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• 제5권2호
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• pp.122-128
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• 1998

NiAl based ODS (Oxide Dispersion Strengthened) intermetallic alloys have been produced by mechanical alloying (MA) process and consolidated by hot extrusion. Subsequent thermomechanical treatments have been applied to induce secondary recrystallization in an attempt to improve creep resistance in this material. The creep behavior of secondary recrystallized MA NiAl has been investigated and compared with those of as-extruded condition. Minimum creep rate were shown to be approximately two orders of magnitude lower than that in as-extruded condition. The improvement in creep resistance is believed due to the grain coarsening, restricting of dispersoid coarsening as well as increase in grain aspect ratio. Creep threshold stress behavior, below which no measurable creep rate can be detected, has been discussed on the basis of particle-dislocation interaction theory. The threshold stress becomes negligible after secondary recrystallization in MA NiAl, presumably due to dispersoid coarsening and a decrease in grain boundary area during secondary recrystallization.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2000년도 추계학술대회 및 발표대회 강연 및 발표논문 초록집
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• pp.10-10
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• 2000

Mechanical alloying (MA) is a powder metallurgy processing technique involving cold welding, fracturing, and rewelding of powder particles in a high-energy ball mill. This has now become an established commercial technique in producing oxide dispersion strengthened (ODS) nickel- and iron-based materials. The technique of MA is also capable of synthesizing non-equilibrium phases such as supersaturated solid solutions, metastable crystalline and quasicrystalline intermetallic phases, nanostructures, and amorphous alloys. In this respect, the capabilities of MA are similar to those of another important non-equilibrium processing technique, viz, rapid quenching of metallic melts. however, the science of MA is being investigated only during the past ten years or so. The technique of mechanochemistry, on the other hand, has had a long history and the materials produced this way have found a number of technological applications, e.g., in areas such as hydrogen storage materials, heaters, gas absorber, fertilizers. catalysts, cosmetics, and waste management. The present talk will concentrate on the basic mechanisms of formation of non-equilibrium phases by the technique of MA and these aspects will be compared with those of rapid quenching of metallic melts. Additionally, the variety of technological applications of mechanically alloyed products will be highlighted.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1988년도 추계학술대회 논문집 학회본부
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• pp.179-182
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• 1988

This study is to investigate the adhesive strength of composite material's interface on the experimental methode of tree growth in the material. The results are as fellows 1) The irradiations of ultrasonic energy cause the mechanical vibration in the polymer composite materials of fluid state, so then bring about physical dispersion and heat form inorganic materials, being supposed to produce chemical crosslinking reaction, decreasing of voids between filler and matrix. 2) The characterics of the breakdown are increased by using coupling agent in the composite material. 3) As the intensity of ultrasonic energy and its irradiated time are larger, the tree inception and break-down voltages increase and the tree growing is slower. so we obtain that the interface adhesive force tan be strengthened by the irradiation of ultrasonic energy.

• 연구논문집
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• 통권25호
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• pp.169-173
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• 1995

The high temperature deformation of mechanically alloyed Al-Ti-Si alloy (Al-9.64wt% Ti-1.56wt% Si) was investigated by performing constant load compression creep tests over the temperature range of $673^\circC$K to $723^\circC$K. From the calculation based on the modified power law creep equation for dispersion strengthened alloy, the true creep activation energy, was 176kJ/mole, the true stress exponent was 4.9. Considering the value of activation energy, stress exponent, the shape of primary creep region, it could be concluded that creep deformation in the MA Al-Ti-Si alloy is controlled by dislocation climb.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1988년도 전기.전자공학 학술대회 논문집
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• pp.813-816
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• 1988

This study is to investigate the adhesive strength of composite material's interface on the experimental methode of tree growth in the material. The results are as follows 1) The irradiations of ultrasonic energy cause the mechanical vibration in the polymer composite materials of fluid state, so then bring about physical dispersion and heat for inorganic materials, being supposed to produce chemical interlinking reaction, decreasing of voids between filler and matrix. 2) As the intensity of ultrasonic energy and its irradiated time are larger, the tree inception and breakdown voltages increase and the tree growing is slower. so we obtain that the interface adhesive force can be strengthened by the irradiation of ultrasonic energy.

• 한국원자력학회:학술대회논문집
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• 한국원자력학회 2005년도 춘계학술발표회
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• pp.471-472
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• 2005

After thermal aging treatment at 693 K for 322 hours, any discernable precipitation could not be found in the $13{\sim}22$ Cr ODS steels, but showing an increase in SP-DBTT and reduction in upper shelf energy. The degree of aging embrittlement increases with Cr content such that the increases in SP-DBTT are 10, 50 and 73 K in 13, 16 and 19 Cr ODS steel, respectively. Amount of hardening also increased linearly as a function of Cr content. Based on the TEM observation, the origin of hardening must be related to the invisibly fine size of Cr-rich ${\acute{\alpha}}-phase$ (<1 nm).

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.964-965
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• 2006

The injection molded Fe sintered bodies were fabricated using two kinds of nano Fe powders, $Fe-5%vol.ZrO_2$ and $Fe-10vol.%ZrO_2$ powders. The relationship between microstructure and mechanical properties depending on the $ZrO_2$ contents and sintering temperature were characterized by SEM and TEM techniques. In the wear test, the $Fe-0vol%ZrO_2$ sintered bodies showed mainly adhesive wear, but in the Fe-5%vol. $ZrO_2$ and Fe-10vol. % $ZrO_2$ composites the main wear behavior showed abrasive wear mode.