• Title/Summary/Keyword: Disc absorption

Search Result 36, Processing Time 0.023 seconds

Optical Properties of Sea Water ( IV ) - Coastal Waters of Southern Part of Korea - (해수의 광학적 성질에 관한 연구 ( IV ) - 한국남해안 -)

  • 양용림
    • Journal of the Korean Society of Fisheries and Ocean Technology
    • /
    • v.14 no.1
    • /
    • pp.37-41
    • /
    • 1978
  • Optical properties were studied in the costal waters of the southern part of Korea based on twenty oceanographic stations from 1 st to 9 th February, 1977. Submarine daylight intensity was measured by using an underwater luxmeter (Toshiba No.9). Daylight intensity in the upper 30m depth layer was measured at 1 m depth interval. The absorption coefficient of the sea water in the area ranged from 0.101 to 2.539 (mean 0.578). The Secchi-disc depth in the area ranged from 0.8 to 13 meters (mean 5.33 meters). The relationship between absorption coefficient (K) and transparency (D) was k= 1. 704/ D. The mean water color in the area was 5. 75 (3-9) in Forel scales. The rates of light penetration for daylight at 1m layer in the area ranged from 13.18 to 82. 05% and the mean was 59.56%, while the rate at 5m layer ranged from 0.007 to 46.1% and the mean was 18.47%.

  • PDF

Synthesis and Properties of Biaxial LC from Dumbbell-shaped Molecules

  • Xu, Fei;Choi, E-Joon
    • 한국정보디스플레이학회:학술대회논문집
    • /
    • 2009.10a
    • /
    • pp.651-654
    • /
    • 2009
  • Novel compounds with rod and disc mesogens were synthesized and characterized. The molecular structures were confirmed by FT-IR, $^1H$-NMR spectroscopy and elemental analysis. The optical properties of these molecules were investigated by UV-vis absorption spectroscopy and photo-luminescence spectroscopy. We found that they are a novel series of blue light-emitting molecules. The absorption spectra peaks of these compounds varied from 336 nm-341 nm, while the maximum emissions centered form 410 nm-450 nm in chloroform solution. However, unexpectedly we could not found their biaxiality and mesomorphic properties by POM, conoscopy and DSC method.

  • PDF

Analysis of Drugs and Chemicals by Infrared Absorption Spectrophotometry(II) Quantitative Analysis of Sulfamethoxydiazine and Sulfamethoxypyridazine in Pharmaceutical Preparations. (Infrared spectrophotometry에 의한 의약품의 분석연구 (II) 적외선흡수 Spectra에 의한 Sulfamethoxydiazine 및 Sulfamethoxy-pyridazine의 정량분석)

  • 옥치완;권영훈
    • YAKHAK HOEJI
    • /
    • v.13 no.2_3
    • /
    • pp.51-56
    • /
    • 1969
  • In quantitative analysis of sulfonamide drugs by means of infrared Spectrophotometry, the author tried to analyse Sulfamethoxydiazine and Sulfamethoxypyridazine in their Pharmaceutical Preparations. By the survey of infrared absorption spectra of Sulfamethoxydiazine and Sulfamethoxypyridazine. We found quantitative properties at the peaks of wave number 1150 cm$^{-1}$ (Sulfamethoxydiazine) and 1090 cm$^{-1}$ (Sulfamethoxypyridazine) in the spectra. These peaks obey Beer's Law in a range of 50-150 ug for Sulfamethoxydiazine and 70-350 ${\mu}$g for Sulfamethoxypyridazine in 300 mg KBr disc. By this method, Sulfamethoxydiazine and Sulfamethoxypyridazine could be analyzed less than 2% error.

  • PDF

Studies on $\alpha$-Amylase of Bacillus circulans F-2 (Part I) Purification of $\alpha$-amylase (Bacillus circulans F-2가 생산하는 $\alpha$-Amylase에 관한 연구 (제 1보) $\alpha$-Amylase의 정제)

  • ;Hajime Taniguchi;Yoshiharu Maruyama
    • Microbiology and Biotechnology Letters
    • /
    • v.9 no.4
    • /
    • pp.185-190
    • /
    • 1981
  • 1. $\alpha$-amylase from B. circulans F-2 was purified with specific activity 55.0 u/mg. protein (about 23 times of the original specific activity) and the yield of 25.5%, by means of corn starch absorption, salting out with ammonium sulfate (80% saturation), gel filtration on Bio-Gel P-100 and DE-32 column chromatography. 2 The purified enzyme showed two closely migrated protin bands on polyacrylamide disc gel electrophoresis, both of which have amylase activity judging from the activity staining of the gel. On SDS-polyacrylamide disc gel electrophoresis, however, the purified enzyme showed a single band suggesting that those two bands are the charge isomers of an amlyase having the slightly different charge. 3. Plot of log mobility of two bands versus polyacrylamide gel concentration according to Hedrick and Smith gave the parallel lines indicating them to be charge isomers. 4. To confirm the action pattern of two enzyme protein bands, each band was separated and was eluted from the gel and eluates were incubated with soluble starch. Oligosaccharide pattern produced by each eluate was examined by paper chromatography. The eluates of two bands showed the same action pattern. 5. The maltohexaose was the only hydrolysis product of soluble starch in the early stage of hydrolysis.

  • PDF

Physical characteristics of ceramic/glass-polymer based CAD/CAM materials: Effect of finishing and polishing techniques

  • Ekici, Mugem Asli;Egilmez, Ferhan;Cekic-Nagas, Isil;Ergun, Gulfem
    • The Journal of Advanced Prosthodontics
    • /
    • v.11 no.2
    • /
    • pp.128-137
    • /
    • 2019
  • PURPOSE. The aim of this study was to compare the effect of different finishing and polishing techniques on water absorption, water solubility, and microhardness of ceramic or glass-polymer based computer-aided design and computer-aided manufacturing (CAD/CAM) materials following thermocycling. MATERIALS AND METHODS. 150 disc-shaped specimens were prepared from three different hybrid materials and divided into five subgroups according to the applied surface polishing techniques. All specimens were subjected up to #4000 grit SiC paper grinding. No additional polishing has been done to the control group (Group I). Other polishing procedures were as follows: Group II: two-stage diamond impregnated polishing discs; Group III: yellow colored rubber based silicone discs; Group IV: diamond polishing paste; and Group V: Aluminum oxide polishing discs. Subsequently, 5000-cycles of thermocycling were applied. The analyses were conducted after 24 hours, 7 days, and 30 days of water immersion. Water absorption and water solubility results were analyzed by two-way ANOVA and Tukey post-hoc tests. Besides, microhardness data were compared by Kruskal-Wallis and MannWhitney U tests (P<.05). RESULTS. Surface polishing procedures had significant effects on water absorption and solubility and surface microhardness of resin ceramics (P<.05). Group IV exhibited the lowest water absorption and the highest microhardness values (P<.05). Immersion periods had no effect on the microhardness of hybrid ceramic materials (P>.05). CONCLUSION. Surface finishing and polishing procedures might negatively affect physical properties of hybrid ceramic materials. Nevertheless, immersion periods do not affect the microhardness of the materials. Final polishing by using diamond polishing paste can be recommended for all CAD/CAM materials.

The Spectral and Thermal Properties of Styrylquinolium Salts for Disc-Recordable Dyes

  • Song, Dong-Hyun;Kim, Jae-Pil;Lee, Chul-Joo;Park, Ki-Hong
    • Journal of Photoscience
    • /
    • v.8 no.3_4
    • /
    • pp.113-117
    • /
    • 2001
  • Several styrylquinolium salts were synthesized to investigate their absorption and thermal properties, which had five different p-aminobenzene units and three different counter ions (iodide, perchlorate, and hexafluorophosphorate anion), respectively. Hydroxy, methoxy, and methyl group in the meta position to the amino group led to bathochromic shift, while Ν-ethyl-Ν-chloroethylamino unit instead of Ν,Ν-diethylamino unit resulted in hypsochromic shift. A dye having a methoxy group in the meta position to the amino group had the highest molar extinction coefficient ($\xi$), while a dye carrying chloro group in Ν-alkyl chains had the lowest $\xi$. The type of counter ions had no effect on spectral properties like the maximum absorption wavelength and $\xi$. All styryl dyes had exothermic peaks at decomposition in DSC curves. Among these styryl dyes, S2 series with perchlorate anions showed the strongest exothermic decomposition. From TGA spectra, S3 series with hexafluorophosphorate anions had the best thermal stability and the sharpest threshold at thermal decomposition.

  • PDF

Instrumented Drop Weight Impact Testing of Polymer Materials (계장화에 의한 고분자 재료의 낙하추식 충격시험)

  • 장경영;김갑용;최만용
    • Journal of the Korean Society of Safety
    • /
    • v.13 no.2
    • /
    • pp.3-12
    • /
    • 1998
  • Polymer materials have been used offensively as construction materials for automobiles, ships, and airplanes in recent years, and their impact resistance has been obliged to be examined. In the present study, a dropped load and a specimen, equipped with high responsible strain gauges respectively, were dropped and then the changes of load and absorption energy with time were observed. It was found that the waveforms for dropped weight coincided with output signal wave for specimen during the destruction test. Based on this experimental result, three disc type of specimens with different compositions were prepared and examined. This instrumented impact test method showed that each specimen can be distinguished from each other better than conventional tests and is expected to contribute to assess test results of impact resistance for some materials under development.

  • PDF

Effect of Butanol Extracts from Prunus mume on the Growth of Salmonella typhimurium (오매의 Butanol추출물이 Salmonella typhimurium의 생육에 미치는 영향)

  • 서명희;배지현
    • Journal of Nutrition and Health
    • /
    • v.35 no.9
    • /
    • pp.926-931
    • /
    • 2002
  • The antimicrobial properties of extracts of Prunus mume were tested on Salmonella paratyphimurium and S. typhimurium. First, the Prumus mume was extracted with methanol at several temperatures, and then fractionation of the methanol extracts from Prunus mume was carried out by using petroleum ether, chloroform, ethyl acetate or butanol. Secondly, absorption column chromatoraphy (using a Diaion HP 20) was conducted to eliminate some water soluble materials that might inhibit the antimicrobial activity of some extracts. The antimicrobial activitry of each of the Prunus mume extracts was determined using a paper disc method against several food-borne pathogens, The growth inhibition curve was determine using butanol extracts of Prunus mume against Salmonella typhimurium. The extraction temperature did not have any significant effect on the yield of the extract or on the level of antimicrobial activity. The butanol extract of Prunus mume showed strong antimicrobial activity against Salmonella paratyphimurium and S. typhimurium; a 1,000 ppm of butanol extract of Prunus mume retared the growth of S. typhimurium up to 36 hours. (Korean J Nutrition 35(9) : 926~931, 2002)

Tribological Properties of Raction-Bonded SiC-Graphite Composites (반응소결 SiC-graphite 복합체의 마찰마모특성)

  • 백용혁;신종윤;곽효섭;박용갑
    • Journal of the Korean Ceramic Society
    • /
    • v.33 no.5
    • /
    • pp.479-484
    • /
    • 1996
  • The tribological properties of ceramics are very important in the application to engineering ceramic parts such as mechanical seal slurry valve disc and so on. In this study the effect of graphite addition on the mechanical and tribological properties of RBSC/graphite composites were investigated. The composites were prepared by adding graphite powder to the mixture of SiC powder metallic siliconcarbon black and alumina. Bending strength water absorption friction coefficient the amount of worn out material at a certain time and maximum surface roughness(Rmax) of the prepared composites were measured and crystalline phases were examined with XRD. The composite containing 5 vol% graphite powder showed improved bending strength due to high green density and decreased friction coefficient and wear resistance. The friction coefficient and the wear resistance of the composite were increased by adding graphite powder up to 10 vol% They decreased however as increasing the amount of graphite powder more that 10vol% There was no linear relationship between the tribological properties and bending strength of the composites.

  • PDF

Spectrophotometric Determination of Nickel in Steel with Di-2-pyridylmethanone 2-Thiophenecarboxylic Hydrazone

  • Nakanishi, Tsutomu
    • Analytical Science and Technology
    • /
    • v.8 no.4
    • /
    • pp.469-475
    • /
    • 1995
  • Di-2-pyridylmethanon 2-thiophenecarboxylie hydrazone(DPMTCH) was synthesized and used as a chromogenic reagent in the spectrophotometric determination of nickel in steel. The proton disc spectrophotometrically, were $pK_{a1}= 2.66$ and $pK_{a2}= 10.98$ ${\mu}=0.5(NaCl)$. Nickel(II) reacts with DPMTCH to form a 1:2 metal-2-ligand ratio complex, the xylene solution of which has an absorption maximum at 417 nm. Beer's law is obeyed over the range $0-1.17\;mg\;ml^{-1}$ of nickel(II). The molar absorptivity of the nickel(II) complex is $4.17{\times}10^4l\;mol^{-1}\;cm^{-1}$. The precision of the method was estimated for 4.7 mg of nickel(II), the coefficient of variation for 15 replicate determinations being 0.34%.

  • PDF