• Title/Summary/Keyword: Densification Behavior

검색결과 273건 처리시간 0.018초

Effect of Particle Size on Zirconia Gel-Casting Process

  • Kim, In-Woong;Lee, Sang-Jin
    • 한국세라믹학회지
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    • 제52권6호
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    • pp.449-454
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    • 2015
  • The fabrication process of zirconia gel-casting was studied to obtain dense zirconia on a large scale or with complicated shapes. As an experimental parameter, two different particle sizes ($0.1{\mu}m$ and $0.7{\mu}m$) of zirconia powder were applied to the gel-casting process. The viscosity behavior of slurries incorporating 40 vol% of zirconia powder was examined as a function of the dispersant content and the solid load to determine the optimum dispersion conditions. In addition, the gelation time with an initiator, the de-binding behavior, and the main factors affecting densification were examined. The densification of the gel-casted zirconia green body depended on the mixing ratio between the monomer and the dimer and on the zirconia particle size. A green body with a small particle size of $0.1{\mu}m$ showed less densification, with a relative density of 93%. This may be due to the excess number of bubbles created through interactions between the larger particle surface and polymer additives during the ball-milling process.

Effect of $TiO_2$ and $Al(OH)_3$ on Sintering Behavior of $UO_2 - Gd_2 O_3$ Fuel Pellets

  • Kang, Ki-Won;Kim, Keon-Sik;Song, Kun-Woo;Yang, Jae-Ho;Jung, Youn-Ho
    • Nuclear Engineering and Technology
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    • 제32권6호
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    • pp.559-565
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    • 2000
  • The sintering behavior of UO$_2$-Gd$_2$O$_3$fuel pellets under H$_2$gas has been investigated using dilatometry and XRD methods. The addition of TiO$_2$or Al(OH)$_3$increased the density and grain size. A density of 95% TD and a grain size larger than 6 ${\mu}{\textrm}{m}$ are achieved by the addition of 0.1 wt% TiO$_2$or Al(OH)$_3$. It was found that the densification of UO$_2$-Gd$_2$O$_3$pellets was suppressed in the temperature range of 1300 to 150$0^{\circ}C$, compared to UO$_2$pellets. The formation of a (U,Gd)O$_2$solid solution is the main reason for the suppression of densification. The role of TiO$_2$in densification and grain growth is discussed on the basis of the densification cuwe and ceramography.

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분말직송압연 티타늄의 치밀화 거동 (Densification Behavior of Titanium in Direct Powder Rolling Process)

  • 강동환;홍재근;박노광;김태원
    • 대한기계학회논문집A
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    • 제36권10호
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    • pp.1255-1260
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    • 2012
  • 분말직송압연에 따른 티타늄 분말 집합체의 치밀화 거동을 연구하였다. 이와 관련하여 실험 시 나타나는 롤-밀림 현상을 분석하기 위한 이론적 모델을 개발하였으며, 이를 통해 보다 실질적인 유한요소 해석을 수행하였다. 개발된 롤-밀림 모델을 통해 공정변수에 따른 롤-밀림의 경향을 정량적으로 파악하였으며, 분말직송압연 공정의 유한요소 해석을 통해 판재의 위치 별 최종 상대 밀도를 비교적 정확히 예측할 수 있었다. 아울러 공정 시 분말집합체의 치밀화 현상을 이해하기 위해 분말-롤 간 접촉 압력 및 전단응력을 계산하였으며 이를 통해 분말의 물림현상이 나타나는 영역을 보다 명확히 확인할 수 있었다.

Al-20Si-5.5Fe-1.2Mg-0.5Mn 합금분말의 치밀화에 미치는 소결온도와 분위기의 영향 (Effects of Sintering Temperature and Atmosphere on Densification of Hypereutectic Al-Si Alloy Powders)

  • 이재욱;박상빈;양상선;김용진
    • 한국분말재료학회지
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    • 제15권3호
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    • pp.196-203
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    • 2008
  • The densification behavior of Al-20Si-5.5Fe-1.2Mg-0.5Mn powders was investigated through micro-structure analysis of sintered specimens. The specimens sintered in vacuum or in high purity (99.999%) nitrogen showed porous near-surface microstructures. The densification of near-surface part was enhanced by means of ultra-high purity (99.9999%) nitrogen atmosphere. The relationship between slow densification and oxide surfaces of Al alloy powders was discussed. And the effects of Mg addition, nitrogen gas, and humidity on densification were discussed. In addition, the rapid growth of primary Si crystals above the critical temperature was reported.

등통로각압축이 결합된 압출 공정에 의한 알루미늄 분말의 치밀화 거동 (Analysis of Aluminum Powder Densification by Continuous Front Extrusion-Equal Channel Angular Pressing)

  • 윤승채;김형섭
    • 한국분말재료학회지
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    • 제15권3호
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    • pp.204-209
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    • 2008
  • Aluminum alloys are not only lightweight materials, but also have excellent thermal conductivity, electrical conductivity and workability, hence, they are widely used in industry. It is important to control and enhance the densification behavior of metal powders of aluminum. Investigation on the extrusion processing combined with equal channel angular pressing for densification of aluminum powders was performed in order to develop a continuous production process. The continuous processing achieved high effective strain and full relative density at $200^{\circ}C$. Optimum processing conditions were suggested for good mechanical properties. The results of this simulation helped to understand the distribution of relative density and effective strain.

비정질/다이아몬드 복합재료에서 상분율과 비정질-다이아몬드 입자 크기 비가 성형특성에 미치는 영향 (Effects of Phase Fraction and Metallic Glass-Diamond Size Ratio on the Densification of Metallic Glass/Diamond Composite)

  • 신수민;김택수;강승구;김정곤
    • 한국분말재료학회지
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    • 제16권3호
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    • pp.173-179
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    • 2009
  • In the present study, Zr-base metallic glass(MG)/diamond composites are fabricated using a combination of gas-atomization and spark plasma sintering (SPS). The densification behaviors of mixtures of soft MG and hard diamond powders during consolidation process are investigated. The influence of mixture characteristics on the densification is discussed and several mechanism explaining the influence of diamond particles on consolidation behaviour are proposed. The experimental results show that consolidation is enhanced with increasing diamond/Metallic Glass(MG) size ratio, while the diamond fraction is fixed.

혼합 금속 분말의 고온 치밀화 거동 (Densification Behavior of Mixed Metal Powders under High Temperature)

  • 조진호;김기태
    • 대한기계학회논문집A
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    • 제24권3호
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    • pp.735-742
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    • 2000
  • Densification behaviors of mixed metal powder under high temperature were investigated. Experimental data of mixed copper and tool steel powder with various volume fractions of Cu powder were obtained under hot isostatic pressing and hot pressing. By mixing the creep potentials of McMeeking and co-workers and of Abouaf and co-workers originally for pure powder, the mixed creep potentials with various volume fractions of Cu powder were employed in the constitutive models. The constitutive equations were implemented into a finite element program (ABAQUS) to compare with experimental data for densification of mixed powder under hot isostatic pressing and hot pressing. Finite element calculations by using the creep potentials of Abouaf and co-workers agreed reasonably well with experimental data, however, those by McMeeking and co-workers underestimate experimental data as observed in the case of pure metal powders.

냉간압축하에서 혼합금속분말의 치밀화 모델 (A Densification Model for Mixed Metal Powder under Cold Coompaction)

  • 조진호
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2000년도 춘계학술대회논문집
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    • pp.112-118
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    • 2000
  • Densification behavior of mixed copper and tool steel powder under cold compaction was investigated. By mixing the yield functions proposed by Fleck et al. and by Gurson for pure powder in terms of volume fractions and contact numbers of Cu powder new mixed yield functions were employed for densification of powder composites under cold compaction. The constitutive equations were implemented into a finite element program (ABAQUS) to compare with experimental data for densificatiojn of mixed powder under cold isostatic pressing and cold die compaction. finite element calculations by using the yield functions mixed by contact numbers of Cu powder agreed better with experimental data than those by volume fractions of Cu powder.

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알루미나-anorthite 계의 액상소결에서 MgO의 첨가가 치밀화 및 미세구조에 미치는 영향 (Effects of MgO Addition on Densification and Microstructural Development during Liquid-Phase Sintering of Alumina-Anorthite System)

  • 김호양;이정아;김정주
    • 한국세라믹학회지
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    • 제36권11호
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    • pp.1243-1251
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    • 1999
  • Densification behavior and microstructural evolution during the liquid-phase sintering of alumina-anorhite system were investigated as a function of MgO addition. When MgO component was added in either alumina or anorthite glass powder the aspect ratio of alumina grains decreased and concurrently the are of flat interface which was formed as a result of contact solid alumina gains rather increased. Consequently addition of MgO component in the Al2O3-amorthite system brought about suppression of the rearrangement of solid grains during the liquid phase sintering and then densification of specimens was also retarded.

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골판지 적층재와 EPS 사이의 압축거동에 대한 실험적 연구 (Experimental Study on Compression Behavior between Multi-layered Corrugated Structure and EPS Packaging Materials)

  • 박종민;최원식;김종순
    • 한국산업융합학회 논문집
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    • 제23권1호
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    • pp.83-91
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    • 2020
  • The evaluation of the compression behavior of the cushioning material is of importance to achieve appropriate packaging design. In order to change packaging design from polymeric-based to more eco-friendly cellulose-based nire effectively, comparative study on the compression behavior between these two packaging materials is crucial. In this study, the stress-strain behavior, hysteresis loss, and response characteristics for cyclic loading were analyzed through compression tests on multi-layered corrugated structure (MLCS) and expanded polystyrene (EPS) packaging materials. MLCS produced in Korea is produced by winding a certain number of single-faced corrugated paperboard, and the compression behavior of this material was turned out to be 6 stages: elastic stage, first buckling stage, sub-buckling stage, densification stage, last buckling stage and high densification stage. On the other hand, EPS's compression behavior was in 3 stages: linear elastic stage, collapse plateau, and densification stage. The strain energy per unit volume (strain energy density) of MLCS did not differ depending on the material thickness, but it showed a clear difference depending on the raw material and flute type. Hysteresis loss of MLCS ranged from 0.90 to 0.93, and there were no significant differences in the raw material and flute type. These values were about 5 to 20% greater than the hysteresis of the EPS (about 0.78 to 0.87).