• Title/Summary/Keyword: Defect Characterization

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Characterization of Resistive Switching in PVP GQD / HfOx Memristive Devices (PVP GQD / HfOx 구조를 갖는 전도성 필라멘트 기반의 저항성 스위칭 소자 특성)

  • Hwang, Sung Won
    • Journal of the Semiconductor & Display Technology
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    • v.20 no.1
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    • pp.113-117
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    • 2021
  • A composite active layer was designed based on graphene quantum dots, which is a low-dimensional structure, and a heterogeneous active layer of graphene quantum dots was applied to the interfacial defect structure to overcome the limitations. Increasing to 1.5~3.5 wt % PVP GQD, Vf changed from 2.16 ~ 2.72 V. When negative deflection is applied to the lower electrode, electrons travel through the HfOx/ITO interface. The Al + ions are reduced and the device dominates at low resistance. In addition, as the PVP GQD concentration increased, the depth of the interfacial defect decreased, and the repetition of appropriate electrical properties was confirmed through Al and HfOx/ITO. The low interfacial defects help electrophoresis of Al+ ions to the PVP GQD layer and the HfOx thin film. A local electric field increase occurred, resulting in the breakage of the conductive filament in the defect.

Magnetic Flux Leakage (MFL) based Defect Characterization of Steam Generator Tubes using Artificial Neural Networks

  • Daniel, Jackson;Abudhahir, A.;Paulin, J. Janet
    • Journal of Magnetics
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    • v.22 no.1
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    • pp.34-42
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    • 2017
  • Material defects in the Steam Generator Tubes (SGT) of sodium cooled fast breeder reactor (PFBR) can lead to leakage of water into sodium. The water and sodium reaction will lead to major accidents. Therefore, the examination of steam generator tubes for the early detection of defects is an important requirement for safety and economic considerations. In this work, the Magnetic Flux Leakage (MFL) based Non Destructive Testing (NDT) technique is used to perform the defect detection process. The rectangular notch defects on the outer surface of steam generator tubes are modeled using COMSOL multiphysics 4.3a software. The obtained MFL images are de-noised to improve the integrity of flaw related information. Grey Level Co-occurrence Matrix (GLCM) features are extracted from MFL images and taken as input parameter to train the neural network. A comparative study on characterization have been carried out using feed-forward back propagation (FFBP) and cascade-forward back propagation (CFBP) algorithms. The results of both algorithms are evaluated with Mean Square Error (MSE) as a prediction performance measure. The average percentage error for length, depth and width are also computed. The result shows that the feed-forward back propagation network model performs better in characterizing the defects.

Spectroscopic Characterization of Phosphorus Doped HPHT Diamond (인이 첨가된 고온 . 고압 다이아몬드의 분광학적 특성)

  • Chung Jung In;Kim Hee-Soo
    • Journal of the Mineralogical Society of Korea
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    • v.17 no.4
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    • pp.291-297
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    • 2004
  • Phosphorus is one of the interesting impurities in diamond, because it produces n-type semiconducting character. The character has been studied with spectroscopic methods as well as electric method, but most of the diamond used for these studies are conducted by the CVD (Chemical Vapor Deposition) diamond. In this study, we synthesized the phosphorus doped HPHT (High Pressure and High Temperature) diamond and investigated the characterization using CL spectroscopy to determine how phosphorus incorporated. As a result, the undocumented peaks of 248 and 603 nm as well as the reported peaks (239 nm, 240 ~ 270 nm) at the previous studies were observed. These luminescence peaks may be due to the complex defect of phosphorus with other impurities such as boron and nitrogen.

NDE Inspecting Techniques for Wind Turbine Blades Using Terahertz Waves (테라헤르츠파를 이용한 풍력터빈 블레이드 NDE 탐상 평가기법)

  • Im, Kwang-Hee;Kim, Sun-Kyu;Jung, Jong-An;Cho, Young-Tae;Woo, Yong-Deuck
    • Journal of Advanced Engineering and Technology
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    • v.11 no.4
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    • pp.245-251
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    • 2018
  • Terahertz waves (T-ray) was extensively studied for the NDE (nondestructive evaluation) of characterization of trailing edges for a use of turbines composed with composite materials. The used NDE system were consisted of both CW(Continuous wave) and TDS (Time domain spectroscopy). The FRP composites were utilized for two kinds of both trailing edges of wind energy (non-conducting polymeric composites) and carbon fiber composites with conducting properties. The signals of T-ray in the TDS (Time domain spectroscopy) mode resembles almost that of ultrasound waves; however, a terahertz pulse could not penetrate a material with conductivity unlike ultrasound. Also, a method was suggested to obtain the "n" in the materials, which is called the refractive index (n). The data of refractive index (n) could be solved for the trailing edges. The trailing edges were scanned for characterization and inspection. C-scan and B-scan images were obtained and best optimal NDE techniques were suggested for complicated geometry samples by terahertz radiation. Especially, it is found that the defect image of T-ray corresponded with defect locations for the trailing edges of wind mill.

Fabrication and Characterization of Cu3SbS4 Solar Cell with Cd-free Buffer

  • Han, Gyuho;Lee, Ji Won;Kim, JunHo
    • Journal of the Korean Physical Society
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    • v.73 no.11
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    • pp.1794-1798
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    • 2018
  • We have grown famatinite $Cu_3SbS_4$ films by using sulfurization of Cu/Sb stack film. Sulfurization at $500^{\circ}C$ produced famatinite $Cu_3SbS_4$ phase, while $400^{\circ}C$ and $450^{\circ}C$ sulfurization exhibited unreacted and mixed phases. The fabricated $Cu_3SbS_4$ film showed S-deficiency, and secondary phase of $Cu_{12}Sb_4S_{13}$. The secondary phase was confirmed by X-ray diffraction, Raman spectroscopy, photoluminescence and external quantum efficiency measurements. We have also fabricated solar cell in substrate type structure, ITO/ZnO/(Zn,Sn)O/$Cu_3SbS_4$/Mo/glass, where $Cu_3SbS_4$ was used as a absorber layer and (Zn,Sn)O was employed as a Cd-free buffer. Our best cell showed power conversion efficiency of 0.198%. Characterization results of $Cu_3SbS_4$ absorber indicates deep defect (due to S-deficiency) and low shunt resistance (due to $Cu_{12}Sb_4S_{13}$ phase). Thus in order to improve the cell efficiency, it is required to grow high quality $Cu_3SbS_4$ film with no S-deficiency and no secondary phase.

Microstructural Characterization of MDF Cement-SiC Whisker Composites (MDF 시멘트-SiC 위스커 복합재료의 미세구조적 특성)

  • 김태현;최상흘
    • Journal of the Korean Ceramic Society
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    • v.29 no.8
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    • pp.617-622
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    • 1992
  • In order to study on the effect of SiC whisker in flexural strength characterization of macro defect-free (MDF) cement composites, which composed of high alumina cement and polyvinyl alcohol, microstructural characterization of the composite specimens fabricated by the addition of SiC whiskers was investigated. Microproes are created around the SiC whisker, MDF cement didn't react with the SiC whisker. However, flexural strength of the composites have been improved. Fracture morphology of the composites, presents mainly intergranular type fracture passing around the unhydrated particles and siC whiskers, and partially transgranular type fracture. The main strengthening mechanisms of the MDF cement composites reinforced with SiC whiskers are characterized by crack deflection, microcracking, and bridging of cracks.

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Directivity Analysis of Ultrasonic Wave Reflected from the Artificial Defect in Simulated Butt Welded Joint (가상 용접부내의 결함으로부터 반사된 초음파의 지향성 해석)

  • Nam, Young-Hyun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.15 no.2
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    • pp.378-385
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    • 1995
  • The ultrasonic non-destructive testing uses the directivity of the ultrasonic pulse wave which propagates in one direction. The directivity is expressed as the relationship between the propagate direction and its sound pressure. The directivity of ultrasonic wave is closely related to determination of probe arrangement, testing sensitivity, scanning pitch and defect location and characterization. The paper measured the directivity of shear wave, which reflected from artificial defect located in weld metal zone in butt welded joint similar model made of pyrex glass by using visualization method. 2 MHz and 4 MHz angle probes were used to measure the directivity of reflection wave at the artificial defect. The directivity of shear waves reflected from the defect was different according to the probe position and the shape of butt welded joint. The difference of directivity of reflection wave was existed between 2 MHz and 4 MHz angle probes. The angle of reflection wave became equal to angle of incidence as increase of the height of excess metal.

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The Defect Characterization of $Gd_2O_2S$: Tb Crystals by Positron Annihilation Spectroscopy (양전자 소멸 분광법을 이용한 $Gd_2O_2S$ : Tb 결함 특성)

  • 이종용;김창규
    • Journal of the Korean Vacuum Society
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    • v.13 no.2
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    • pp.92-98
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    • 2004
  • DBPAS has been used to characterize atomic size defect structures in materials. In this investigation the numerical analysis of the Doppler spectra was employed to the determination of the shape parameter, S, defined as the ratio between the amount of counts in a central portion of the spectrum and the total counts of whole spectrum. As the samples were exposed by X-ray increasing the exposed doses from 3, 6, and 9 Gy with 6 MV and 15 MV, respectively and also irradiated by X-ray as the medical applications used for in 0, 2, 4 and 6 years. The S-parameter values were increased as increasing the exposed time and the energies, that indicated the defects generate more. The S-parameters of the samples with medical treatment is varied from 0.4932 to 0.4956.

Infrared Thermography Characterization of Defects in Seamless Pipes Using an Infrared Reflector

  • Park, Hee-Sang;Choi, Man-Yong;Park, Jeong-Hak;Lee, Jea-Jung;Kim, Won-Tae;Lee, Bo-Young
    • Journal of the Korean Society for Nondestructive Testing
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    • v.32 no.3
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    • pp.284-290
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    • 2012
  • Infrared thermography uses infrared energy radiated from any objects above absolute zero temperature, and the range of its application has been constantly broadened. As one of the active test techniques detecting radiant energy generated when energy is applied to an object, ultrasound infrared thermography is a method of detecting defects through hot spots occurring at a defect area when 15~100 kHz of ultrasound is excited to an object. This technique is effective in detecting a wide range affected by ultrasound and vibration in real time. Especially, it is really effective when a defect area is minute. Therefore, this study conducted thermography through lock-in signal processing when an actual defect exists inside the austenite STS304 seamless pipe, which simulates thermal fatigue cracks in a nuclear power plant pipe. With ultrasound excited, this study could detect defects on the rear of a pipe by using an aluminium reflector. Besides, by regulating the angle of the aluminium reflector, this study could detect both front and rear defects as a single infrared thermography image.