• Title/Summary/Keyword: DC 스퍼터링

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마그네트론 스퍼터링을 이용하여 TiN 박막을 증착한 도전성 섬유

  • Jang, Jin-Hyeok;Mun, Seon-U;Kim, Gyeong-Hun;Kim, Seong-Min;Lee, Seung-Min;Kim, Jeong-Su;Han, Seung-Hui
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.168-168
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    • 2013
  • 도전성 섬유(Conductive textile)는 섬유자체의 고유 특성을 유지하면서 전기적인 도전 특성을 갖는 섬유로서, Cu, Ag, Ni 등의 전기전도성이 높은 금속 박막을 증착하여 제작하고 있다. 그러나, 이러한 금속은 공기 중의 산소와 결합하여 쉽게 산화되는 특성을 지니고 있기 때문에 사용 중에 산화되어 도전 특성이 감소하는 단점이 있다. TiN은 금속 못지않은 높은 전기전도성을 지니고 있을 뿐만 아니라, 금속에 비하여 높은 경도에 따른 우수한 내마모 특성, 내부식성 및 낮은 마찰계수를 지니고 있다. 그러나, TiN은 경도가 높기 때문에 섬유의 고유 특성인 유연성이 저하되는 문제가 있다. 본 연구에서는 면(Cotton), PE (Polyester), PP (Polypropylene) 등의 섬유 위에 TiN 박막을 증착하여, 섬유의 유연성을 유지하며 전기전도성과 내마모 특성이 우수한 도전성 섬유를 제작하고자 하였다. TiN 박막 증착을 위하여 ICP-assisted pulsed-DC reactive magnetron sputtering 장비를 사용하였으며, Ar:N2 유량비(Flow rate), Ti 타겟 power, ICP RF power 등을 변화시켜 Ti와 N의 조성비를 조절하였고, 이를 통하여 섬유의 휨이나 접힘에도 도전 특성이 변하지 않고 내마모 특성이 우수한 TiN 박막을 증착하였다. TiN 박막이 증착된 섬유의 전기전도도는 일정한 압력 하에 전기전도도를 측정할 수 있는 장치를 제작하여 측정하였으며, 표면 조성 분포 및 접합력 측정을 위하여 XPS (X-ray Photoelectron Spectroscopy)와 Peel-tester를 이용하였다.

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Effects of Demagnetization Field in Patterned Micro-magnetic Film Elements (패턴 된 미크론 자기박막 소자에서의 자기소거장 효과분석)

  • Kim, Ki-Chul;Suh, Jeong-Dae;;Lee, C.S.;Song, Y.J.
    • Journal of the Korean Magnetics Society
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    • v.13 no.3
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    • pp.103-108
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    • 2003
  • A micromagnetic model and a Stoner-Wohlfarth model are used to analyze the effect of demagnetization field in patterned permalloy films. Permalloy films of 20 $\mu\textrm{m}$${\times}$(40 $\mu\textrm{m}$∼200 $\mu\textrm{m}$) are fabricated by DC magnetron sputtering and photo lithography. Measured magnetoresistance data of patterned permalloy films are compared with simulation results. The micromagnetic model gives a better agreement with the measured MR data than the Stoner-Wohlfarth model. Based on the simulation results, we propose a revised approximation formula for dernagnetization field in Stoner- Wohlfarth model for a few fm patterned magnetic films.

Magnetic properties of NdEeB thin films with perpendicular anisotropy (수직자기이방성 NdFeB 박막자석의 자기특성)

  • 김만중;유권상;양재호;김윤배;김택기
    • Journal of the Korean Magnetics Society
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    • v.10 no.6
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    • pp.280-294
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    • 2000
  • [(300nm)Ta/(500nm)NdFeB/(300nm)Ta] thin films were deposited at 5 mTorr Ag gas pressure by RF-DC magnetron sputtering, and their magnetic properties were investigated. The [Ta/NdFeB/Ta] films deposited on heated Si substrates showed high perpendicular anisotropy and excellent hard magnetic properties. The films sputtered at tile substrate temperature of T$\sub$s/=650$^{\circ}C$ and 700$^{\circ}C$ showed (BH)$\sub$max/=20 MGOe and $\sub$i/H$\sub$c/= 18.9 kOe along the perpendicular direction to the film plane, respectively.

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Deposition of Al Doped ZnO Films Using ICP-assisted Sputtering on the Plastic Substrate (유도결합 플라즈마 스퍼터링을 이용한 플라스틱 기판 상의 Al이 도핑된 ZnO 박막 증착)

  • Jung, Seung-Jae;Han, Young-Hun;Lee, Jung-Joong
    • Journal of Surface Science and Engineering
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    • v.39 no.3
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    • pp.98-104
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    • 2006
  • Al-doped ZnO (AZO) films were deposited on the plastic substrate by inductively coupled plasma (ICP) assisted DC magnetron sputtering. The AZO films were produced by sputtering a metallic target (Zn/Al) in a mixture of argon and oxygen gases. AZO films with an electrical resistivity of ${\sim}10^3\;{\Omega}cm$ and an optical transmittance of 80% were obtained even at a low deposition temperature. In-situ process control methods were used to obtain stable deposition conditions in the transition region without any hysteresis effect. The target voltage was controlled either at a constant DC power. It was found that the ratio of the zinc to oxygen emission intensity, I (O 777)/I (Zn 481) decreased with increasing the target voltage in the transition region. The $Ar/O_2$ plasma treatment improve the adhesion strength between the polycarbonate substrate and AZO films.

Exchange and Interlayer Coupling in NiO Spin Valve Films (NiO 스핀밸브 박막에서 교환결합과 사잇층 결합에 관한 연구)

  • 박창만;고성호;황도근;이상석;이기암
    • Journal of the Korean Magnetics Society
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    • v.7 no.5
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    • pp.258-264
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    • 1997
  • Exchange and interlayer couplings between a NiFe ferromagnetic layer and an antiferromagnetic NiO layer in NiO/NiFe/Cu/NiFe spin-valve films prepared by rf/dc magnetron sputtering were investigated. The interlayer coupling field ($H_{int}$ decreased with the Cu layer thickness, and the exchange coupling field $(H_{ex}$ saturated to 90 Oe. the magnetitudes of $H_{ex}$ and $H_{int}$ decreased with increasing thickness of the pinned NiFe layer. The increase of $H_{int}$ with the free NiFe layer may be due to the increased magnetization.

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Growth Behavior of Nanocrystalline CrN Coatings by Inductively Coupled Plasma (ICP) Assisted Magnetron Sputtering (유도결합 플라즈마를 이용한 마그네트론 스퍼터링으로 증착된 나노결정질 CrN 코팅막의 성장)

  • Seo, Dae-Han;Chun, Sung-Yong
    • Journal of the Korean Ceramic Society
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    • v.49 no.6
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    • pp.556-560
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    • 2012
  • Nanocrystalline CrN coatings were deposited by DC and ICP-assisted magnetron sputtering on Si (100) substrates. The influences of the ICP power on the microstructural and crystallographic properties of the coatings were investigated. For the generation of the ICP, radio frequency was applied using a dielectric-encapsulated coil antenna installed inside the deposition chamber. As the ICP power increased from 0 to 500W, the crystalline grain size decreased. It is believed that the decrease in the crystal grain size at higher ICP powers is due to resputtering of the coatings as a result of ion bombardment as well as film densification. The preferential orientation of CrN coatings changed from (111) to (200) with an increase in the ICP power. The ICP magnetron sputtering CrN coatings showed excellent surface roughness compared to the DC magnetron sputtering coatings.

The electrical properties of Ni/Cr/Si thin film with sputtering process parameters (스퍼터링 조건변화에 따른 Ni/Cr/Si 박막의 전기적 특성)

  • Lee, Boong-Joo;Park, Gu-Bum;Kim, Byung-Soo;Lee, Duck-Chool
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.52 no.2
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    • pp.56-60
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    • 2003
  • In this work, we have fabricated thin film resistors using the DC/RF magnetron sputter of 51wt%Ni-41wt%Cr-8wt%Si alloy target and studied the effect of the process parameters on the electrical properties. In fabrication process, sputtering power, substrate temperature and annealing temperature have been varied as controllable parameters. TCR decreases with increasing the substrate temperature, but TCR increases over 300 [$^{\circ}C$]. The films are annealed to 400 [$^{\circ}C$] in air atmosphere, TCR increases with increasing the annealing temperature. The resistivity was 172 [${\mu}{\Omega}{\cdot}cm$] and 209 [${\mu}{\Omega}{\cdot}cm$] for the RF and DC as a sputtering power sources, respectively. Also, TCR was -52 [$ppm/^{\circ}C$] and -25 [$ppm/^{\circ}C$]. As a results of them, it is suggested that the sheet resistance and TCR of thin films can be controlled by variation of sputter process parameter and annealing of thin film.

Interlayer Formation During the Reactive DC Magnetron Sputtering Process (직류 마그네트론 스퍼터링 공정 중 타겟 오염에 따른 박막 및 계면 형성 특성)

  • Lee, Jin Young;Hur, I Min;Lee, Jae-Ok;Kang, Woo Seok
    • Journal of the Semiconductor & Display Technology
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    • v.18 no.1
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    • pp.1-4
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    • 2019
  • Reactive sputtering is widely used because of its high deposition rate and high step coverage. The deposition layer is often affected by target poisoning because the target conditions are changed, as well, by reactive gases during the initial stage of sputtering process. The reactive gas affects the deposition rate and process stability (target poisoning), and it also leads unintended oxide interlayer formation. Although the target poisoning mechanism has been well known, little attention has been paid on understanding the interlayer formation during the reactive sputtering. In this research, we studied the interlayer formation during the reactive sputtering. A DC magnetron sputtering process is carried out to deposit an aluminum oxide film on a silicon wafer. From the real-time process monitoring and material analysis, the target poisoning phenomena changes the reactive gas balance at the initial stage, and affects the interlayer formation during the reactive sputtering process.

Effect of fabrication conditions on microstructure and performance of electrodes for SOFCs (SOFC용 전극 제작 조건에 따른 전극 성능 및 구조 분석)

  • Lah, Se-Yun;Jee, Young-Seok;Lee, Yoon-Ho;Cho, Goo-Young;Cha, Suk-Won
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.06a
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    • pp.307-310
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    • 2009
  • In order to develop SOFC cell performance, many kind of things were investigated. Electrode microstructure is the one of them therefore we focus on electrodes fabrication easily and efficiently. We can fabricate electrodes easily with Pt using DC magnetron sputtering and sintering. However sputtering is difficult to handle and to grow porous electrodes what we require. On the other hand sintering is much easier than sputtering to make porous and adhesive electrodes. So in this paper we deal with sintering and optimize to deposit electrodes conditions by analyzing electrode microstructure with sacnning electron microscopy(SEM) micrograph. Also, we compare electrochemical performance of cells fabricated by sputtering and sintering.

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스퍼터링 방법을 이용한 사극 자석 진공용기 시제품 제작

  • Na, Dong-Hyeon;Park, Jong-Do;Ha, Tae-Gyun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.259-259
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    • 2013
  • 4세대방사광 가속기의 언듈레이터 사이에 설치되는 사극자석 진공용기는 내경 12 mm, 길이 300 mm인 매우 얇고 긴 형태로 제작되어야 하며, 비자성체이면서 전기 전도도와 내부 표면 거칠기 또한 우수하여야 한다. 스테인리스강 316 L EP 튜브는 비자성체로써 기계가공성 및 내부 표면 거칠기가 우수하다. 또한 내부에 DC Magnetron Sputtering을 통하여 알루미늄 층을 형성함으로써 높은 전기 전도도를 확보할 수 있다. 여기서는 스테인리스강 316 L EP 튜브를 이용하여 손쉽게 사극 자석 진공용기를 제작한 후, Cylindrical Magnetron Sputtering System을 구성하여 내부에 균일한 알루미늄 층을 증착하는 공정에 대해 설명하려고 한다. 또한 치밀한 알루미늄 산화막을 형성하는 공정에 대하여 현재까지 수행한 결과를 정리하여 보고하며 앞으로의 개발 과정도 다루고자 한다.

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