• Title/Summary/Keyword: D.B.H. analysis

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The Crystal Structure of Licarin-B $(C_{20}H_{20}O_4)$, A Component of the Seeds of Myristica fragrans

  • Kim, Yang-Bae;Park, Il-Yeong;Shin, Kuk-Hyun
    • Archives of Pharmacal Research
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    • v.14 no.1
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    • pp.1-6
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    • 1991
  • The crystal structure of licarin-B, a component of Myristicae Semen was determined by single crystal X-ray diffraction analysis. Crystal of the compound, which was recrystallized from the mixture of hexane and ether, is monoclinic with a=12.740(1), b=7.219(1), c=9.284(1) ${\AA}$, ${\beta}=94.75(1)^{\circ}$, $D_x=1.26$, $D_m=1.27\;g/cm^3$, space group P21, and Z=2. The structure was solved by direct method and refined by least-squares procedure to the final R value of 0.040 for 1532 independent reflections ${F{\ge}3{\sigma}(F)}$. The compound is a dimeric phenylpropanoid, and belongs to the neolignan analogues. The molecules are arranged along with the screw axis. The intermolecular contacts appear to be the normal van der Waals' forces.

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The Effects of Media on the Intramolecular Photocycloaddition of 3-(3-Butenyl)cyclohex-2-enone

  • 노태희;최균선;박종욱
    • Bulletin of the Korean Chemical Society
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    • v.19 no.5
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    • pp.501-503
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    • 1998
  • In this work, we applied the 1D $11^B$ nutation NMR method for the analysis of the local structural environments in powdered borosilicates $(SiO_2-B_2O_3)$. Spin dynamics during a rf irradiation for spin I=3/2 was analytically calculated with a density ma trix formalism. Spectral simulation programs were written in MATLAB on a PC. Two borosilicates prepared by the sol-gel process at different stabilization temperature were used for the 1D $11^B$ nutation NMR experiment. The $11^B$ NMR parameters, quadrupole coupling constants $(e^2qQ/h)$ and asymmetry parameters (η), for each borosilicate were extracted from the nonlinear least-squares fitting. The effects of heat treatments on the local structures of boron sites in borosilicates were discussed.

The Analysis of Varing Mover on PM Excited Transverse Flux Linear Motor for Compressor (이동자 형상 변화에 따른 압축기용 영구자석 여자 횡자속 선형 전동기의 특성해석)

  • Jeong, D.H.;Woo, B.C.;Kang, D.H.;Chang, J.H.;Kim, J.M.;Hong, D.K.;Park, G.W.
    • Proceedings of the KIEE Conference
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    • 2005.10c
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    • pp.150-152
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    • 2005
  • On this study is PM excited transverse flux linear motor for compressor on an air condenser. The present day, it is general use for linear motor on compressor, so this paper conducted efficiency to compare with varing mover and stator's shape.

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Characteristic Analysis of a Magnet for Magnetically Levitated Vehicle using FLUX3D (FLUX3D를 이용한 자기부상용 전자석의 특성 해석)

  • Lee, Jae-Kun;Shin, Pan-Seok
    • Proceedings of the KIEE Conference
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    • 1996.07a
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    • pp.127-129
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    • 1996
  • A 3-dimensional analysis is desired for a magnet of magnetically levitated vehicle because the geometrical shape of the magnet is complicated and nonsymmetric. A FEM package of FLUX3D is used to analyze the characteristic of the magnet. Various quantities could be observed like levitation force, flux density distribution along the air gap, edge and fringing effect, leakage flux pattern, etc. The simulation results from FLUX3D are compared with those of 2-D analysis and test results. There are a little difference between results due to the boundary conditions and magnetized B-H curve of the core.

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The Analysis of Inground LNG Storage Tank Compression Ring Behavior during Concrete Pouring (콘크리트 타설에 따른 지하식 LNG 저장탱크 컴프레션 링 거동 분석)

  • Kim Y.K.;Kim J.H.;Yoon I.S.;Oh B.T.;Yang Y.M.
    • 한국가스학회:학술대회논문집
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    • 2004.11a
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    • pp.82-87
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    • 2004
  • Compression ring is a part of LNG storage tank. The main function of the compression ring is connected the roof plate with concrete side wall. End of its one side is embedded in the side concrete wall and the other's connected with the roof plate by welding. It is designed to support stably for all the loads such as self weight of steel roof, inner pressure and concrete weight. We fulfill the FEM analysis to analysis the compression ring behavior during construction. Also we studied the effect of the change of design variables. On the basis of the results, we could introduce a more reasonable design method for compression ring.

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Surface and Interface Analysis with Medium Energy Ion Scattering Spectroscoppy

  • Moon, Dae-Wom
    • Proceedings of the Korean Vacuum Society Conference
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    • 1998.02a
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    • pp.129-129
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    • 1998
  • Most of the surface/interface analysis tools have limited depth profiling c capability in terms of the profiling range and the depth resolution. However, M MEIS can profile the surface and subsurface composition and structure q quantitatively and non-destructively with atomic layer depth resolution. I In this presentation, the MEIS system developed at KRISS will be briefly d described with an introduction on the principle of MEIS. Recent MEIS r results on the surface and interface composition and structural change due to i ion bombardment will be presented for preferential sputtering of T:없Os and d damage depth profiles of SHooD, Pt(l11), and Cu(l1D due to Ar+ ion b bombardment. Direct observation of strained Si lattices and its distribution i in the SHool)-SiCh interface and the initial stage of Co growth on Pt(l11) w will be reported. H surfactant effects on epitaxial growth of Ge on Si(ooD w will be discussed with STM results from SND.

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Identification and sequence analysis of small subunit ribosomal RNA gene of bovine Theileria isolates from Korea and Japan (한국과 일본 소에 감염된 Theileria 분리주의 small subunit ribosomal 유전자의 동정 및 분석)

  • Chae, Joon-seok;Park, Jin-ho;Kwon, Oh-deog;Waghela, Suryakant D.;Holman, Patricia J.;Wagner, Gerald G.;Lee, Joo-mook
    • Korean Journal of Veterinary Research
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    • v.38 no.4
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    • pp.909-917
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    • 1998
  • Six different sequences types(A through E and H) and a subtype(Bl) of the small subunit ribosomal RNA(SSUrRNA) gene were found in bovine Theileria isolates from different areas of Korea and Japan. The sequences were aligned and three hypervariable regions were observed in the nucleotide position ranges 212~231, 261~270 and 632~690. Five of the Theileria isolates yielded sequence type A; these were the field isolates KCB, KCN, and KCJ, and the laboratory stock KLS, all from Korea, and a single isolate from Japan (JHS). This sequence type is identical to the SSUrRNA gene sequence listed for Theileria buffeli (GenBank Accession No. Z15106) from Marula, Kenya. The Korean field isolate KKB yielded only a single sequence type (B), but multiple sequence types were found in some isolates. For example, KCB and JHS isolates yielded both types A and B ; isolate KKW showed types B and H; isolate KCN showed types A, C, and D ; and isolate KCJ showed types A, B, E, and a subtype B1. Finding of the multiple sequences SSUrRNA gene sequences suggests that bovine Theileria isolates from both Korea and Japan may consist of mixed populations.

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Electromagnetic Vector Fields Simulation with Mathematica (전자기 벡터장 시각화를 위한 Mathematica 시뮬레이션)

  • Choi, Yong-Dae;Yun, Hee-Joong
    • Journal of the Korean Vacuum Society
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    • v.21 no.2
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    • pp.69-77
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    • 2012
  • Visualization of the electromagnetic vector fields are presented and examined with Mathematica. Vector fields may be used to represent a great of many physical quantities in various area of physics, including electromagnetism with vector differential operators. Because they deal with abstract, three-dimensional fields that are some times very difficult to visualize, electromagnetism can be conceptually rather difficult. Visual representation of such an abstract vector fields is invaluable to student or researchers working in this field and also helps teaching electromagnetism to physics or engineering students. Mathematica provides a wider range of graphical tools including plot of vector fields and vector analysis, which can be applied to visualization of electromagnetic system. We have visualized the most fundamental concepts of the electromagnetic vector $\vec{E}=-\vec{\nabla}_{\varphi}$, $\vec{D}={\epsilon}\vec{E}$, $\vec{\nabla}{\times}\vec{A}$, $\vec{B}={\mu}\vec{H}$, $\vec{B}={\mu}_0(\vec{H}+\vec{M})$, which are confirmed with vector calculations and valid graphically with some presentations.

Characteristics of White Soybean Chungkookjang Fermented by Bacillus subtilis D7 (Bacillus subtilis D7에 의하여 발효된 백태 청국장의 특성)

  • Lee, Na-Ri;Park, Sung-Bo;Lee, Sang-Mee;Go, Tae-Hun;Hwang, Dae-Youn;Kim, Dong-Seob;Jeong, Seong-Yun;Son, Hong-Joo
    • Journal of Life Science
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    • v.23 no.4
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    • pp.529-536
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    • 2013
  • This study was carried out to investigate the characteristics of white soybean Chungkookjang fermented by Bacillus subtilis D7. The highest germination rate was obtained under $25^{\circ}C$ when water was supplied for 4 days at intervals of 2 hr. The total isoflavone content was 971.3 ${\mu}g/g$ before germination and 1023.8 ${\mu}g/g$ after germination. The amino type- and ammonia type-nitrogen contents of Chungkookjang were proportional to the fermentation time. The pH values of all Chungkookjang soybeans increased up to pH 7.8-8.0 during fermentation. The number of viable cells in all Chungkookjang soybeans increased significantly up to 24 hr. The protease activity of all Chungkookjang soybeans increased up to 30-36 hr. The ${\alpha}$- and ${\beta}$-amylase activities of Chungkookjang fermented by B. subtilis D7 were enhanced with increasing fermentation time. Analysis of the effect of Chungkookjang intake on the liver function of mouse showed that the alkaline phosphatase (ALP) activity and the superoxide dismutase (SOD) activity in the Chungkookjang diet group were markedly higher than those in the control group. The asparatate aminotransferase (AST) activity in the germinated soybean Chungkookjang diet group was higher than that in the nongerminated soybean Chungkookjang diet group. Therefore, Chungkookjang soybeans fermented with B. subtilis D7 can be expected to have an increased content of functional components and improved quality characteristics.

Quantitative Analysis of Vitamin B5 and B6 Using High Performance Liquid Chromatography (고속액체크로마토그래피를 이용한 비타민 B5 및 B6의 정량 분석)

  • Kim, Gi-Ppeum;Hwang, Young-Sun;Choung, Myoung-Gun
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.46 no.10
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    • pp.1186-1194
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    • 2017
  • Recently, many people have demanded reliable nutritional data even for minor-components. On the other hand, an analytical method for the analyses of vitamin $B_5$ and $B_6$ is lacking. Therefore, this study attempted to validate with accuracy and precision the analysis of vitamin $B_5$ and $B_6$ using a high-performance liquid chromatography (HPLC) method. The vitamin $B_5$ and $B_6$ contents were analyzed using an Agilent 1260 series HPLC system. YMC-Pack ODS-AM ($250{\times}4.6mm$ I.D.) and YMC-Pack Pro RS $C_{18}$ ($250{\times}4.6mm$ I.D.) columns were used for the analyses of vitamin $B_5$ and $B_6$, respectively. In the case of vitamin $B_5$, the flow rate was set to 1.0 mL/min by isocratic elution using the 50 mM $KH_2PO_4$ solution (pH 3.5)/acetonitrile (ACN) (95:5, v/v) with monitoring at 200 nm using HPLC/DAD, whereas the flow rate for vitamin $B_6$ was set to 1.0 mL/min of flow rate by isocratic elution using a 20 mM $CH_3CO_2Na$ solution (pH 3.6)/ACN (97:3, v/v) with monitoring by excitation at 290 nm and emission at 396 nm using HPLC/FLD. The column temperature was set to $30^{\circ}C$. The injection volume was $20{\mu}L$ for each experiment. The specificity of the accuracy and precision for vitamin $B_5$ and $B_6$ were also validated by HPLC. The results showed high linearity in the calibration curve for vitamin $B_5$ ($R^2=0.9998^{{\ast}{\ast}}$), the limit of detection (LOD) and limit of quantitation (LOQ) were 0.4 mg/L and 1.3 mg/L, respectively, In contrast, for the calibration curve of vitamin $B_6$, which showed high linearity ($R^2=0.9999^{{\ast}{\ast}}$), the LOD and LOQ were 0.006 mg/L and 0.02 mg/L, respectively.