• Title/Summary/Keyword: Curing effect

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Effect of light source on depth of cure and polymerization shrinkage of composites

  • Na, Joon-Sok;Oh, Won-Mann;Hwang, In-Nam
    • Proceedings of the KACD Conference
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    • 2001.11a
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    • pp.578.1-578
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    • 2001
  • The aim of this study was to evaluate the efficiency of the recently introduced light curing units to polymerize a light curing resin composite. Four light curing units XL 3000, Optilux 500 for halogen light source, Apollo 95E for plasma arc and Easy cure for LED (blue-light Emitting Diode) were evaluated. Radiometer was used for measure the light intensity.(omitted)

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Drying shrinkage of Non-Sintered Cement Concrete with various curing condition (양생조건 변화에 따른 비소성 시멘트 콘크리트의 건조수축)

  • Mun Kyoung-Ju;Park Won-Chun;Soh Yang-Seob
    • Proceedings of the Korea Concrete Institute Conference
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    • 2005.05b
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    • pp.357-360
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    • 2005
  • This research investigates the drying shrinkage of non-sintering cement(NSC) matrix added phosphogypsum(PG) and waste lime(WL) to granulated blast furnace slag(GBFS) as sulfate and alkali activators with various curing condition. The experimental results are follow: When the moisture is fully supplied at the early curing age, there is effect which carries out abundant generation of the ettringite which is an expansion nature mineral, and compensates for contraction with a chemical prestress concept.

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Hydration Characteristics according to First Curing Condition in Solid Hydrated by Hydro-Thermal Synthesis Reaction (수열합성경화체의 1차 양생조건에 따른 수화특성)

  • Kim, Jin-Man;Jung, Eun-Hye;Park, Sun-Gyu
    • Journal of the Korea Concrete Institute
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    • v.20 no.5
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    • pp.543-548
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    • 2008
  • Solid hydrated by hydro-thermal synthesis reaction is cured two times, the first curing is the steam curing at atmospheric pressure and the second one is a high-pressure steam curing, that is autoclaving. Steam curing is to acquire the proper strength for the resistance of treatment in the first curing process, it was not evaluated properly so far. Because of ignorance about curing, some engineers even think that the dry curing is better than the steam curing. The relation between compressive strength of solid hydrated by hydrothermal synthesis reaction and curing condition are presented in this paper. In order to investigate the effect of curing on the strength properties of specimen, the hydration behavior of solid hydrated by hydro-thermal synthesis reaction has been studied over curing condition using XRD, DT-TGA and porosimeter, SEM analysis technique. The results show that the specimens which are cured with blended method of dry and steam curing appear to have better strength properties than that of dry curing and steam curing. Also, there are significant difference of hydration behavior among curing condition in the solid hydrated by hydro-thermal synthesis reaction.

Residual Stress Comparison of Type III Hydrogen Tank by Curing Conditions (Type III 수소탱크 경화조건에 따른 잔류응력 비교)

  • Yong-Chul Shin
    • Composites Research
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    • v.37 no.1
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    • pp.15-20
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    • 2024
  • Since the residual stress of hydrogen tank is directly related to durability, it is very important to reduce it for safety. Type II~IV hydrogen tank are manufactured by the filament winding method, in which the fiber is impregnated with resin and wound around the liner. Residual stress in composite is affected by curing conditions and fiber tension etc. In this study, the effect of curing conditions on residual stress was analyzed when manufacturing a Type III hydrogen tank using carbon fiber filament winding process. First, the curing behavior of the epoxy resin was analyzed using a differential scanning calorimetry. Through this, the curing temperature was set to 140℃. During the same curing time, the specimens were cured under 2-stage curing condition that reached 140℃ earlier and a 4-stage curing condition that reached 140℃ later, respectively. After curing, the residual stress of the composite material was measured by the ring slitting method, and the experimental values were compared with numerical values. It was confirmed that there was a significant difference in residual stress according to the optimization of curing conditions.

Effect of Cultivar, Drying Agent and Preservative on Quality Changes of Fall Harvested Oat Hay (품종, 건조제 및 보존제의 처리가 추계수확 연맥건초의 품질변화에 미치는 영향)

  • 한건준;김동암
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.16 no.4
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    • pp.315-326
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    • 1996
  • An experiment was carried out to determine effect of cultivar, drying agent concentration and preservative on the moisture content, temperature and quality changes of fall harvested oat(Avena sativa L.) hay during field curing and storage. The main plots consisted of the cultivar such as 'Foothill' and 'Swan', the subplots consisted of drying agent concentration such as 7Skg/ha(C1), lOSkglha(C2) and control(C0) and the sub-subplots consisted of preservative such as buffered acid(BA), lactic bacteria inoculant(LB) and control(C0). Moisture contents of 'Foothill' and 'Swan' oat cultivar at harvest were 635.5 and 385.4%DW(Dry weight), respectively, but the final moisture contents of the oat cultivars were 117 and 86%DW. The moisture content of cut oat was not affeded by drying agent concentration. Core temperature of baled 'Swan' oat hay was a little higher than that of 'Foothill' and no consistent preservative effect was found. Total nitrogen content of 'Swan' oat hay was 3.08% and that of 'Foothill' oat hay was 3.45%(P<0.05). Drying agent treatment increased total nitrogen content of 'Swan'(P <0.05), but preservative had no effect. Crude fiber content of oat cultivar was increased as the curing progressed(P<0.05) and the difference of crude fiber content of oat cultivar was maintained through the whole curing period. Effect of drying agent concentration on crude fiber content was not found after preservation. Crude fiber content of 'Swan' oat hay was higher than that of 'Foothill' by 1.O% in ADF and 3.1 % in NDF(P<0.05). No preservative effect was found in crude fiber content. According to RFV of oat cultivar at harvest, forage quality of 'Foothill' and 'Swan' was Prime and Grade 1, respectively, but that of both cultivm was above Grade 2 at the final curing day. RFV of the stored 'Foothill' and 'Swan' oat hay was 122 and 114(P<0.05), respectively, and the quality of oat hay was classified as Grade 1 and 2, respectively, according to the forage quality standard assigned by AFGC.

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POLYMERIZATION SHRINKAGE OF COMPOSITE RESINS CURED BY VARIABLE LIGHT INTENSITIES (가변 광도 중합에 따른 복합레진의 중합수축에 관한 연구)

  • Lim, Mi-Young;Cho, Kyung-Mo;Hong, Chan-Ui
    • Restorative Dentistry and Endodontics
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    • v.32 no.1
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    • pp.28-36
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    • 2007
  • The purpose of this study was to compare the effect of exponential curing method with conventional curing and soft start curing method on polymerization shrinkage of composite resins. Three brands of composite resins (Synergy Duo Shade, Z250, Filtek Supreme) and three brands of light curing units (Spectrum 800, Elipar Highlight, Elipar Trilight) were used. 40 seconds curing time was given. The shrinkage was measured using linometer for 90 seconds. The effect of time on polymerization shrinkage was analysed by one-way ANOVA and the effect of curing modes and materials on polymerization shrinkage at the time of 90s were analysed by two-way ANOVA. The shrinkage ratios at the time of 20s to 90s were taken and analysed the same way. The results were as follows : 1. All the groups except Supreme shrank almost within 20s Supreme cured by soft start and exponential curing had no further shrinkage after 30s (p < 0.05). 2. Statistical analysis revealed that polymerization shrinkage varied among materials (p = 0.000) and curing modes (p = 0.003). There was no significant interaction between material and curing mode. 3. The groups cured by exponential curing showed the statistically lower polymerization shrinkage at 90s than the groups cured by conventional curing and soft start curing (p < 0.05). 4. The initial shrinkage ratios of soft start and exponential curing were statistically lower than conventional curing (p < 0.05). From this study, the use of low initial light intensities may reduce the polymerization rate and, as a result, reduce the stress of polymerization shrinkage.

Effect of soil overburden pressure on mechanical properties of carbon FRP strips

  • Toufigh, Vahid;Bilondi, Meysam Pourabbas;Tohidi, Farshid
    • Structural Engineering and Mechanics
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    • v.61 no.5
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    • pp.637-643
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    • 2017
  • Carbon fiber reinforced polymers (CFRPs) have been recently investigated as an alternative material for Geosynthetics to improve soil properties. One of the factors influencing the fiber orientation and mechanical properties of CFRP is the effect of soil overburden pressure. This study investigates the tensile behavior of cast-in-place CFRP. During the curing time of specimens, a wide range of normal stress is applied on specimens sandwiched between the soils. Two different soil types are used to determine the effect of soil grain size on the mechanical properties of CFRP. Specimens are also prepared with different specifications such as curing time and mixing soil in to the epoxy. In this study, tensile tests are conducted to investigate the effect of such parameters on tensile behavior of CFRP. The experimental results indicate that by increasing the normal stress and soil grain size, the ultimate tensile strength and the corresponding strain of CFRP decrease; however, reduction in elastic modulus is not noticeable. It should be noted that, increasing the curing period of epoxy resin and mixing soil in to the epoxy have no significant effect on the tensile properties of CFRP.

A STUDY OF CONTRACTION SHRINKAGE OF COMPOSITE RESINS AND ORMOCERS WITH VARIOUS CURING TIMES (광조사 시간에 따른 복합레진과 Ormocer의 중합수축에 관한 연구)

  • Chung, Yeon-Chung;Min, Kyung-San;Lee, Hae-Hyoung;Cho, Kyung-Mo;Cho, Yong-Bum
    • Restorative Dentistry and Endodontics
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    • v.28 no.4
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    • pp.326-333
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    • 2003
  • Ormocer has organic-inorganic compound polymers. One of advantages of ormocer is reduced polymerization shrinkage. The purpose of this study was to compare the amount of contraction shrinkage of composite resins and ormocers. Additionally, the time of each material when there is no further change of contraction shrinkage was analysed. Four brands of composite resins (P-60. Surefil, Z-250 and Denfil) and two brands of ormocers (Definite and Admira) were used. 20 seconds, 40 seconds and 60 seconds of curing times were given. Contraction shrinkage of them were measured using a linometer for 80 seconds. The effect of material and curing time to contraction shrinkage at the time of 80 seconds was analysed by two-way ANOVA. The effect of time to contraction shrinkage was analysed by one-way ANOVA and the time when there was no further change of the contraction shrinkage was analysed. The results are as follows: 1. P-60, Definite, Z-250 and Denfil had no further change of contraction shrinkage from the time of 20 seconds, and Surefil and Admira had no further change of contraction shrinkage from the time of 10 seconds. 2. Statistical analysis revealed volumetric shrinkage varied among material (p<0,05). No significant difference of contraction shrinkage among different curing times was found, and there was no effect of interaction between materials and curing times to contraction shrinkage. 3. Definite and Admira showed the statistically same contraction shrinkage with those of Z-250 and P-60. which is higher than that of Surefil and lower than that of Denfil (p<0.05).

Effects of Curing Conditions on the Chemical Compositions of Positive Plate for Lead Acid Battery Plates (납축전지 극판의 숙성 조건이 양극판의 화학적 조성에 미치는 영향)

  • Ku, Bon-Keun;Jeong, Soon-Wook
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.4
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    • pp.347-354
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    • 2006
  • Generally, it has been known that positive plate efficiency is the most influential effect on the initial current capacity of lead acid battery. Thus, in this study, we have investigated the curing effect of the positive plate, which is one of the important lead acid battery processes. The curing process of the positive plate is performed either with the separation of each plate with 1mm gap or with no gap of plate. As a result, when there is no interval between each plate, the higher temperature current happened than expected, resulting in the changes in the initial current efficiency of the lead acid battery. The chemical composition and crystal structure of a material coated on the positive plate were identified with XRD and SEM. It was resulted that were only there not a lot of 4BS (tetrabasic-lead sulfate, $4PbO{\cdot}PbSO_4)$ on the plate in case of curing of plates without interval, but a large quantity of $Pb_3O_4$ also formed on the surface. On the other hand, it was observed that 3BS (tribasic-lead sulface, $3PbO{\cdot}PbSO_4{\cdot}H_2O)$ was the main product on the plate in case of typical curing process with some interval. From the initial current capacity test, the positive plate having 3BS was approximately 40% higher in initial current capacity than that having 4BS. It was concluded that 4BS and $Pb_3O_4$ on the plate surface were harmful to the initial current capacity of lead acid battery.

Effect of Curing Conditions on the ASR of Lightweight Aggregate Concrete (양생조건이 경량골재 콘크리트의 ASR에 미치는 영향)

  • 성찬용;김성완;민정기
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.35 no.4
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    • pp.38-46
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    • 1993
  • This study is to analyze effect of exposure environment and mode of ASR on the engineering properties of synthetic lightweight aggregate concrete, such as dynamic modulus of elasticity and ultrasonic pulse velocity. The results of this study are summarized as foflows ; 1. The expansion rate of each exposure environment in 380$^{\circ}$C and NaCI 4% solution was shown higher than in 20$^{\circ}$C and normal water. The expansion rate of each exposure mode was largely shown in order of fjill immersion, wetting/drying, half immersion. 2. The dynamic modulus of elasticty and ultrasonic pulse velocity of each exposure environment in 38$^{\circ}$C and NaCl 4% solution was shown less than in 20$^{\circ}$C and normal water. The dynamic modulus of elasticity and ultrasonic pulse velocity of each exposure mode was shown smaller in order of full immersion, wetting/drying, half imersion.3. The relation between dynamic modulus of elasticity and ultrasonic pulse velocity was highly significant. The dynamic modulus of elasticity was increased with increase of ultrasonic pulse velocity. The decreasing rate of the dynamic modulus of elasticity was shown 2.1~3.4 times higher than the ultrasonic pulse velocity at each age, exposure environment and mode, respectively. 4. The expansion of each exposure environment and mode was increased with increase of curing age. The dynamic modulus of elasticity and ultrasonic pulse velocity of those concrete was increased with increase of curing age. At the curing age 28 days, the highest properties was showed at each type concrete, it was gradually decreased with increase of curing age. Specially, at the curing age 98 days of full immersion, the rate of expansion of type D was shown 3.95 times higher than the type A. But the dynamic modulus of elasticity and ultrasonic pulse velocity was decreased 17% and 8.3%.

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