• Title/Summary/Keyword: Curing Time

Search Result 1,197, Processing Time 0.027 seconds

THE EFFECT OF FLOWABLE RESIN LINING ON THE MARGINAL MICROLEAKAGE OF CONDENSABLE RESIN RESTORATION (응축형 복합레진 수복시 유동성 레진 이장이 변연부 미세누출에 미치는 영향)

  • 문주훈;고근호
    • Restorative Dentistry and Endodontics
    • /
    • v.26 no.1
    • /
    • pp.16-22
    • /
    • 2001
  • The purpose of this study was to evaluate the marginal microleakage of condensable composite resin restorations according to flowable resin lining of internal cavity wall. The eighty extracted human molar teeth without caries and/or restorations are used The experimental teeth were randomly assigned into four groups of ten teeth each. Eighty caries-free extracted human molars were used in this study. The conventional class II cavities (box-shaped on mesial and distal surface, faciolingual width : 3mm, gingival wall depth : 1.5mm) were prepared 1mm below cementoenamel junction with a # 701 carbide bur. The teeth were divided into four groups, and then each group were subdivided into A & B group according to flowable resin & compomer lining ; Group 1-A : Tetric Ceram filling, Group 1-B : Tetric Flow lining and Tetric Ceram filling, Group 2-A Ariston pHc filling, Group 2-B : Tetric Flow lining and Ariston pHc filing, Group 3-A SureFil filling, Group 3-B : Dyract Flow lining and SureFil filling, Group 4-A : Pyramid filling, Group 4-B : Aeliteflo lining and Pyramid filling. To simulate as closely as possible the clinical situation during retoration placement, a "restoration template" was fabricated, and the condensable resin was filled using a three-sited light-curing incremental technique. All the materials used were applied according to the manufacturers' instructions. The specimens were stored in the 100% humidity for 7 days prior to thermocycling (100 thermal cycles of 5~55$^{\circ}C$ water with a 30-second dwell time) The specimens were immersed in 2% metyleneblue dye for 24 hours, and then embedded in transparent acrylic resin and sectioned mesiodistally with diamond wheel saw. The degree of marginal leakage was scored under stereomicroscope ($\times$20) and the data were analyzed by Kruskal-Wallis test and Wilcoxon signed ranks test. The results were as follows : 1. In the gingival margins of all the group, microleakage of subgroup B was less than subgroup A. 2. In the group 1, 2, 4, there was significant differences between subgroup A and B (p<0.05), but in the group 3, there was not significant different between group 3-A (SureFil) and group 3-B (Dyract flow/SureFil) (p>0.05). 3. In the subgroup A and B, there was significant different between all group except group 4 of subgroup A. From the results above, it was suggested that the cavity lining of flowable resin and flowable compomer in condensable resin restoration decrease microleakage at gingival margin, and does improve their ability to seal the gingival margin of class II preparation.

  • PDF

A Study on the Development of Poly-Urea for Porcelain Restoration (폴리우레아 도자기 복원 재료의 적용)

  • Han, Won-Sik;Wi, Koang-Chul;Oh, Seung-Jun;Lee, Young-Hoon
    • Journal of Conservation Science
    • /
    • v.34 no.1
    • /
    • pp.23-29
    • /
    • 2018
  • This study synthesized poly-urea and used it as a filler material for the restoration of porcelain. The synthesized poly-urea was manufactured as a resin and hardener mix that does not undergo contraction during curing, and is unfading. Given an adhesion strength of $180kg/cm^2$ and shearing strength of $200kg/cm^2$, the synthesized poly-urea exhibited the same efficacy as the epoxy putty currently sold in the market. Moreover, it also overcame the drawback of foaming encountered by urethane restoratives, which are a structurally similar type. The hardening time and pot life could also be controlled using additives. The poly-urea used for the restoration of modern artifacts presented a pot life of approximately one hour and took 12 h for complete hardening ($T_{90}$). When a $2{\times}2{\times}2cm$-sized test sample was added to xylene, poly-urea started to separate approximately two hours later and completed perfect pulverization within the solution 24 h later, demonstrating its reversibility. When directly applied to contemporary artifacts, it demonstrated the potential for restoration, as well as convenience and colorfulness.

Effects of Concrete Materials for the Stream Restoration on Bombina orientalis Embryos (하천복원용 콘크리트 소재가 무당개구리 (Bombina orientalis) 배아에 미치는 영향)

  • Park, Chan Jin;Ahn, Hong Kyu;Gye, Myung Chan;Lee, Tae Hyeong
    • Ecology and Resilient Infrastructure
    • /
    • v.2 no.2
    • /
    • pp.147-153
    • /
    • 2015
  • Various adverse effects can occur due to direct exposure from toxic substances when toxic materials are used to restore river ecosystems. Thus, this study performed analysis on the development of toxicity in terms of survival and abnormality rates using embryos of Bombina orientalis living in Korea to analyze the toxicity of materials used in the river projects. The results showed that the toxicity in cement (C group) was the strongest whereas the toxicity in plant-based polyurethane (P1 group) was the weakest. Survival rates of B. orientalis embryos were 100%, 94 - 95%, 66 - 89% and 0% in control, P1, polyurethane (P2) and C groups, respectively. Abnormalities of embryos were 10.5%, 5.3 - 10.5%, 26.3 - 27.8% and 35.7% in control, P1, P2 and C groups, respectively. Furthermore, we verified that having a sufficient curing time reduced toxic substances that were extracted. The above result suggest that cement and polyurethane hamper the early development of amphibians. In conclusion, it is highly important to review biological safety with respect to the selection of materials used to restore rivers. This study shows the importance of the selection of eco-friendly materials and processes.

An Evaluation of the Structural Integrity of the Polymer-Modified Cement Waste Form (폴리머 시멘트 고화체에 대한 구조적 건전성 평가)

  • Ji, Young-Yong;Kwak, Kyung-Kil;Hong, Dae-Seok;Kim, Tae-Kuk;Ryu, Woo-Seog
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
    • /
    • v.9 no.2
    • /
    • pp.81-86
    • /
    • 2011
  • Polymer-modified cement is the composite material made by partially replacing and strengthening the cement hydrate binders of conventional mortar with polymeric modifiers such as polymer latexes and redispersible polymeric modifiers. It is known that the addition of polymer to cement mortar leads to improved quality, which would be expected to have a high chemical resistance. Therefore, the purpose of this study is to identify the improved chemical resistance, such as low permeability and low ion diffusivity, of the polymer-modified cement as a solidification agent for the radwaste. First, polymer-modified cement specimens by latex modification were prepared according to the polymer content from 0% to 30% to select the optimized polymer content. At those specimens, the water-to-cement (W/C) ratio was maintained to 33% and 50% respectively. After the much curing time, the structural integrity of specimens was evaluated through the compressive strength test and the porosity evaluation by the water immersion method. From the results, 10% of the polymer content at 33% of the W/C ratio was shown to have the most improved quality. Finally, the leaching test referredfrom ANS 16.1 for the specimens having the most improved quality was conducted. Dedicated specimens for the leaching test were then mixed with radioisotopes of $^{60}Co$ and $^{137}Cs$ at the specimen preparation.

Properties of Strength Development of Concrete at Early Age Using High Fineness Cement and Fly Ash (고분말도 시멘트와 플라이애시를 치환한 콘크리트의 조기강도 발현 특성)

  • Ha, Jung-Soo;Kim, Han-Sic;Lee, Young-Do
    • Journal of the Korea institute for structural maintenance and inspection
    • /
    • v.22 no.2
    • /
    • pp.154-160
    • /
    • 2018
  • Cement industries are considered key industries for reducing carbon emissions, and efforts are off the ground to reduce the use of cement in the concrete sector. As a part of this effort, research is off the ground to utilize a large amount of industrial by-products that can be used as a substitute for a part of cement. Concrete using industrial by-products has advantages such as durability, environment friendliness and economical efficiency, but there are problems such as retarding and early-age strength deterioration. Therefore, this study aimed to reduce the use of cement and solve the problem of early-age strength deterioration while using fly ash, which is an industrial by-product. Accordingly, it was confirmed that the strength was improved at all ages irrespective of curing temperature by accelerating the hydration reaction by using high fineness cement. Subsequently, high fineness cement was partially replaced with fly ash and the strength development characteristics were examined. As a result, it was possible to exhibit strength equal to or higher than ordinary portland cement even at the early age. Also, it was confirmed that even when the fly ash is replaced by 30%, it is possible to shorten the time for dismantling the forms of vertical and horizontal members.

Evaluation of Unit Weight and Strength of Sand Using Electro-mechanical Impedance (전기-역학적 임피던스를 이용한 모래의 단위중량 및 강도 평가)

  • Park, Sung-Sik;Woo, Seung-Wook;Lee, Jung-Shin;Lee, Sae-Byeok;Lee, Jun Cheol
    • Journal of the Korean Geotechnical Society
    • /
    • v.34 no.2
    • /
    • pp.33-42
    • /
    • 2018
  • In this study, the EMI (electro-mechanical impedance) of a small piezoelectric sensor was applied for measuring a unit weight and cementation (strength) of sand. Three different sizes of uncemented Nakdong River sand were filled loosely or densely into a compaction mold. A piezoelectric sensor with 20 mm in diameter was installed within sand for impedance measurement. A small Nakdong River sand was mixed with cement ratios of 4, 8 12, 16% and then compacted into a specimen with 50 mm in diameter and 100 mm in height. The specimen consisted of 6 layers with a sensor at the third layer. The impedance signals for 3 days and unconfined compressive strength at the 3rd day were measured. As the unit weight of uncemented sand increased, the resonant frequency increased slightly from 102 to 105 kHz but a conductance at resonant frequency decreased. For cemented sands, as the curing time and cement ratio increased, the resonant frequency increased significantly from 129 to 266 kHz but the conductance at resonant frequency decreased. The unconfined compressive strength (UCS) of cemented sands was between 289 and 1,390 kPa for different cement ratios. The relationship of UCS and resonant frequency linearly increased but one with a conductance at resonant frequency was in inverse proportion.

Adhesion Properties of UV-curable Acrylic PSA Tape for Automotive Sidemolding and Emblem (자동차용 사이드 몰딩과 엠블럼 적용을 위한 UV 경화형 아크릴 점착 테이프의 점착물성)

  • Park, Ji-Won;Lee, Seung-Woo;Kim, Hyun-Joong;Won, Dong-Bok;Kim, Dong-Bok;Lee, Kang-Shin;Woo, Hang-Soo;Kim, Eun-Ah
    • Journal of Adhesion and Interface
    • /
    • v.12 no.3
    • /
    • pp.81-87
    • /
    • 2011
  • In this study, UV curing and crosslinking process was introduced for synthesis of acrylic foam tape that can be applied to the the automotive assembly process. Polymerized adhesive are laminated to baseform and varying the thickness of specimens were prepared. To measure basic mechanical properties, stainless steel was used. And in the test peel, dynamic shear and t-block were used. The acrylform adhesive show better results compare with typical adhesive and the properties depand on external factors - thick, wetting time -. To analysis functions of acrylic foam adhesive used to automobile production, evaluate the adhesive properties on the various plastic substrate. In PP and PE are categorized low surface energy materials, their properties have not been expressed. But dynamic shear tests show that some properties could be expressed by the difference break mechanism.

Effects of Cryptotympana pustulata on the expression of cytokine genes in human monocytes of THP-1 (선퇴가 인간의 THP-1 단핵구에서 사이토카인 유전자 발현에 미치는 영향)

  • An, Jong-Hyun;Kim, Kyung-Jun
    • The Journal of Korean Medicine Ophthalmology and Otolaryngology and Dermatology
    • /
    • v.23 no.1
    • /
    • pp.94-110
    • /
    • 2010
  • Objective : This study was performed to evaluate the effect of immune reaction inductive substances such as phorbol-myristate-acetate(PMA), lipopolysaccharide(LPS), dermato-phagoides pteronyssus crude extract(DPE), dinitrochloro-benzene(DNCB) and Cryptotympana pustulata(CP), the Cryptotympana pustulata extracting substance at simultaneously on the translocation of nuclear factor-kappa B(NF-${\kappa}B$) towards to the nucleus and the mRNA expression patterns of various cytokine genes in Human acute monocytic leukemia cell line(THP-1 cells), monocytes of human. Experiment : To analyze cytokine genes expression patterns, the RT-PCR method was used, measuring tumor necrosis factor(TNF)-$\alpha$ that had been secreted during cell culture in the ELISA method. The morphological change in the cell observed during THP-1 cell culture was observed using a scanning electron microscope (SEM) and the quantitative distribution in the cell NF-${\kappa}B$ was analyzed through immunocytochemistry and a confocal microscopy. Result : CP showed different influences onto the mRNA expression patterns of cytokine genes with PMA, LPS. DPE and DNCB according to the types of immune inductive substances in the THP-1 cells. The expressions of inter-leukin(IL)-10, interferon(INF)-$\gamma$, TNF-$\alpha$ and monocyte chemoattractantant protein(MCP)-1 induced by PMA were suppressed by CP while the expression of transforming growth factor(TGF)-$\beta$ was promoted. Regarding the secretion pattern of TNF-$\alpha$ according to PMA processing, its secretion amount was increased by CP concurrent processing, in case of processing CP onto PMA and LPS, We discovered that the secretion amount of TNF-$\alpha$ was increased. Upon processing PMA and LPS on the THP-1 cell strain at the same time or either additionally processing CP thereon, the movement increase towards the nucleus from the NF-${\kappa}B$ cell cytoplasm, a transcription factor was able to be observed. Conclusion : In this study, Cryptotympana pustulata extracting substance was confirmed that it had an influence on expression patterns of cytokine genes according to the actions of a variety kinds of immune reaction inductive substances processed on the monocyte THP-1 cell of humans. Therefore, additional studies as for the immune adjusting function of Cryptotympana pustulata are considered to be able to offer important materials for curing immune abnormal diseases such as atopy dermatitis afterward.

A Study on the Electrical Conductivity and Electromagnetic Shielding of High Performance Fiber Reinforced Cementitious Composites(HPFRCC) (고성능 시멘트 복합체의 전기전도도 및 전자파 특성 시험 평가)

  • Lee, Nam-Kon;Park, Gi-Joon;Park, Jung-Jun;Kim, Sung-Wook
    • Journal of the Korea institute for structural maintenance and inspection
    • /
    • v.23 no.2
    • /
    • pp.37-43
    • /
    • 2019
  • This study investigated electrical conductivity, electromagnetic shielding effectiveness, and mechanical property to improve electromagnetic shielding performance of high performance fiber reinforced cementitious composites (HPFRCC). Steel fiber, steel slag and carbon black as a conductive material were incorporated into the HPFRCC mixes. In addition, 2% CNT solution which was produced by dispersing multi-wall carbon nanotube (MWCNT) into water was used as a conductive material. In the test results, electrical conductivity of HPFRCC specimens was very low except for the specimen incorporating 1% carbon black. Micro structure of cement matrix was changed as the curing time increased, which negatively affected the conductive network of HPFRCC. In case of HC1 specimen showing a conductive network (0.083 S/cm), the electrical conductivity of the specimen after being dried at $60^{\circ}C$ for 72 hours to exclude the effect of water on electrical conductivity was significantly reduced to 0.0003 S/cm. The most important parameter of electromagnetic shielding effect was found to be a steel fiber while the effect of carbon black and steel slag was very few. The correlation between electrical conductivity and electromagnetic shielding effect does not seem to be clear.

Application of 3D printer in dental clinic (치과 진료실에서 3D 프린트의 활용)

  • Kim, Hyun Dong
    • Journal of the Korean Academy of Esthetic Dentistry
    • /
    • v.27 no.2
    • /
    • pp.82-96
    • /
    • 2018
  • 3D printing is a process of producing 3d object from a digital file in STL format by joining, bonding, sintering or polymerizing small volume elements by layer. The various type of 3d printing is classified according to the additive manufacturing strategies. Among the types of 3D printer, SLA(StereoLithography Apparatus) and DLP(Digital Light Processing) 3D printer which use polymerization by light source are widely used in dental office. In the previous study, a full-arch scale 3d printed model is less precise than a conventional stone model. However, in scale of quadrant arch, a 3d printed model is significantly precise than a five-axis milled model. Using $3^{rd}$ Party dental CAD program, full denture, provisional crowns and diagnostic wax-up model are fabricated by 3d printer in dental office. In Orthodontics, based on virtual setup model, indirect bracket bonding tray can be generated by 3d printer. And thermoforming clear aligner can be fabricated on the 3d printed model. 3D printed individual drilling guide enable the clinician to place the dental implant on the proper position. The development of layer additive technology enhance the quality of 3d printing object and shorten the operating time of 3D printing. In the near future, traditional dental laboratory process such as casting, denture curing will be replaced by digital 3D printing.