• Title/Summary/Keyword: Curing Equipment

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Failure Paths of Polymer/Roughened Metal Interfaces under Mixed-Mode Loading (혼합 하중하에서의 고분자/거친금속 계면의 파손경로)

  • Lee Ho-Young;Kim Sung-Ryong
    • Korean Journal of Materials Research
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    • v.14 no.5
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    • pp.322-327
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    • 2004
  • Copper-based leadframe sheets were oxidized in two kinds of hot alkaline solutions to form brown-oxide or black-oxide layer on the surface. The oxide coated leadframe sheets were molded with epoxy molding compound (EMC). After post mold curing, the oxide-coated EMC-leadframe joints were machined to form sandwiched Brazil-nut (SBN) specimens. The SBN specimens were used to measure the fracture toughness of the EMC/leadframe interfaces under mixed-mode (mode I + mode II) loading conditions. Fracture surfaces were analyzed by various equipment to investigate failure path. The results revealed that the failure paths were strongly dependent on the oxide type. In case of brown oxide, hackle-type failure was observed and failure path lay near the EMC/CuO interface with a little inclining to CuO at all case. On the other hand, in case of black oxide, quite different failure path was observed with respect to the distance from the tip of pre-crack and phase angle. Different failures occurred with oxide type is presumed to be due to the difference in microstructure of the oxides.

Evaluation of Gelation Characteristics with The Variation of Additive Contents in The Alumina Slurry for Gel Casting Process (겔 캐스팅 공정을 위한 알루미나 슬러리에서의 첨가제 함량 변화에 따른 겔화특성 평가)

  • Chung, J.K.;Oh, C.Y.;Ha, T.K.
    • Transactions of Materials Processing
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    • v.31 no.5
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    • pp.290-295
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    • 2022
  • Recently, the use of high-tech ceramic parts in functional electronic parts, automobile parts and semiconductor equipment parts is increasing. These ceramics materials are required to have high reproducibility, reliability, large size and complex shapes. The researchers initiated the work to develop a new shaping method called gel casting, which allows high performance ceramic materials with a complex shape to be produced. The manufacturing process parameters of gel casting include uniform mixing of the initiator, bubble removal, and slip injection. In this study, we analyzed the dispersion and gelation characteristics according to the change in the additive content of the alumina slurry in the gel casting process. The alumina slurry for gel casting was prepared by mixing a solvent, a monomer and a dispersant through a ball mill. Alumina powder and a gelation initiator were added to the mixed solution, and ball milling was performed for 24 hours. A viscosity of 6,435 cps and a stable zeta potential value were obtained under the conditions of alumina powder content of 55 vol% and dispersant 2.0 wt%. After curing for 12 hours by adding aps 0.1wt%, TEMED 0.2wt%, and Monomer 3, 5wt%, it was possible to separate from the molding cup, confirming that the gelation was completed.

An Experimental Study on the Microstructure Characteristics of Cementitious Composites by MIP (MIP를 통한 혼합 시멘트계 재료의 미세구조 특성에 관한 실험적 연구)

  • Kim, Tae-Sang;Jung, Sang-Hwa;Chae, Seong-Tae;Lee, Bong-Chun;Woo, Young-Je;Song, Ha-Won
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.533-536
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    • 2008
  • Recently, in Korea, there has been an increasing number of research papers published which are to improve durability of concrete, particularly by analyzing correlation between diffusivity of chloride and porosity/pore size distribution. In these studies, such test methods as mercury intrusion porosimetry(MIP), gas adsorption or image analysis method are used to analyze the microstructure of materials while MIP is most widely used for concrete. This study analyzes the results of porosity and pore size distribution of paste and concrete adding fly ash or blast furnace slag by using MIP equipment which is widely used for determining micro-porosity structure of cementitious materials. A variation in porosity and pore size distribution at the curing day 3, 7 and 28 has been observed by using MIP equipment for cement paste 35%, 40%, 45%, 50%, 55%, 60% of W/C when using $300kg/m^3$ of cement, 35%, 45%, 55% of W/C when replaced 60% with blast-furnace slag, and 35%, 45%, 55% of W/C when replaced 30% with fly ash. For long-term water cured normal OPC concrete and mixed concrete replaced 60% with blast-furnace slag powder, micro-structure of the sample has been analyzed by using MIP equipment when W/C indicated 40%, 45%, 50% respectively and the binder varied $300kg/m^3$, $350kg/m^3$, $400kg/m^3$, and $450kg/m^3$.

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Analysis of Helical Pile Behavior in Sands Varying Helix Pitch Based on Numerical Analysis Results (사질토에 근입된 헬릭스 피치에 따른 헬리컬 파일의 수치해석적 거동분석)

  • Bak, Jongho;Lee, Kicheol;Choi, Byeong-Hyun;Kim, Dongwook
    • Journal of the Korean Geosynthetics Society
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    • v.17 no.4
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    • pp.29-40
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    • 2018
  • Oil sands, which are largely distributed in Canada and Venezuela, are a mixture of crude oil and sandy soils. In order to extract crude oil from oil sands, construction of massive oil sand plants is required. Generally, the typically-used foundation types of the oil sand plant are driven piles and cast-in-place piles. Most of the oil sand plants are located in cold and remote regions. Installation of driven piles in frozen or organic surface soils is difficult due to high resistance and installation equipment accessability, while the cast-in-place pile has concrete curing problem due to cold temperature. Helical pile can be installed quickly and easily using rotation with a little help of vertical load. As the installation of helical pile is available using a small and light-weight installation equipment, accessibility of installation equipment is improved. The helical pile has an advantage of easy removal by rotation in reverse direction compared with that of installation. Furthermore, reuse of removed helical piles is possible when the piles are structurally safe. In this study, the behavior of helical piles varying helix pitch was analyzed based on the numerical analysis results. Numerical model was calibrated based on the results of model helical pile tests in laboratory. The ultimate helical pile loads, the displacement of each helix attached to the shaft of the helical pile, and the load sharing ratio of each helix were analyzed.

Evaluation of engineering characteristics and field applicability of inorganic thixotropic-grout for backfilling of shield TBM tail voids (쉴드 TBM 뒤채움용 무기계 가소성 그라우트의 공학적 특성 및 현장적용성 평가)

  • Kim, Dae-Hyeon;Jung, Du-Hwoe;Jeong, Gyeong-Hwan
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.12 no.1
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    • pp.75-85
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    • 2010
  • The focus of this study is to evaluate the field applicability of the newly developed inorganic thixotropic-grout in various ways. In order to do this, the volume stability and the permeability of the inorganic thixotropic-grout have been measured and compared to the existing silica type grouts. In addition, the filling capability of the grout into the tail void has been evaluated through both an experiment with a miniature tail-void filling equipment and a test filling at the shield TBM construction site. The volume loss of the inorganic thixotropic-grout after a 14 day-curing under the atmosphere condition was appeared to be minimal. The excellent waterproofing ability of the inorganic thixotropic-grout was confirmed through a permeability test. The toxicity of the inorganic thixotropic-grout has been evaluated through a toxicity test of aquatic fishes (KS M 0111) and the pH value of the liquid eluviated from inorganic thixotropic-grout was measured as an average of 8.0 and a fatality rate of goldfish after 96 hours was 10% or so. The existence of harmful heavy metals in the liquid eluviated from the inorganic thixotropic-grout has been also examined through an atomic absorption spectroscopy (AAS) test. Any of harmful heavy metals were not detected and the detected level of $Cr^{6+}$ and Cd was far below the standard. Based on both an experiment with a miniature tail-void filling equipment and a test filling at the shield TBM construction site, the filling ability of inorganic thixotropic-grout into the tail void was proved to be excellent.

A Study on Experimental Method of Blasting Vibration in Curing Concrete (양생중인 콘크리트에서의 발파진동의 영향 시험방법에 대한 연구)

  • Kim, Jang-Deuk;Kim, Yong-Ha
    • The Journal of Engineering Geology
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    • v.19 no.3
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    • pp.417-422
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    • 2009
  • Tunnels that have recently been constructed are characterized by longer length than ever before and furthermore they frequently go through the ground area with poor conditions such as fractured zones. If ground strength is weak, plastic deformation of tunnel occurs, and occasionally a big fall may be brought about. Up to now, the construction work of tunneling has been executed as a sequential method placing the lining concrete after completion of excavation. Such a method requires a long time and much money to complete the tunnel. It is hard to ensure the stability of tunnel if tunnel is left undone for a long time after excavation in fracture zones or plastic grounds. For this reason, we tried to take simultaneous construction of tunnel excavation and lining concrete in order to not only shorten construction schedule but also stabilize the tunnel at the highly fractures zone as soon as possible. As preliminary consideration for simultaneous construction, in-situ tests are performed to calculate the isolation distance over which blasting vibration does not influence the strength of lining concrete. Improvement of ling form, placing method of concrete, ventilation using a dust collector, together with equipment arrangement, was made to assure the simultaneous construction work.

DLC Structure Layer for Piezoelectric MEMS Switch (압전 MEMS 스위치 구현을 위한 DLC 구조층에 관한 연구)

  • Hwang, Hyun-Suk;Lee, Kyong-Gun;Yu, Young-Sik;Lim, Yun-Sik;Song, Woo-Chang
    • Journal of Satellite, Information and Communications
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    • v.6 no.1
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    • pp.28-31
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    • 2011
  • In this paper, a new set of structural and sacrificial material that is diamond like carbon (DLC)/photoresist for high performance piezoelectric RF-MEMS switches which are actuated in d33 mode is suggested. To avoid curing problem of photoresist sacrificial layer, DLC structure layer is deposited at room temperature by radio frequency plasma enhanced chemical vapor deposition (RF-PECVD) method. And lead zirconate titanate (PZT) piezoelectric layer is deposited on structure layer directly at room temperature by rf magnetron sputtering system and crystallized by rapid thermal annealing (RTA) equipment. Particular attention is paid to the annealing of PZT film in order to crystallize into perovskite and the variation of mechanical properties of DLC layer as a function of annealing temperature. The DLC layer shows good performance for structure layer in aspect to Young's modulus and hardness. The fabrication becomes much simpler and cheaper with use of a photoresist.

Preparation of PMMA Marbles by Film Molding Method (필름 성형법에 의한 PMMA 인조석의 제조)

  • 길기승;김의식;김대수
    • Polymer(Korea)
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    • v.27 no.2
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    • pp.152-158
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    • 2003
  • Two commercial processing methods have been used to produce poly(methyl methacrylate) (PMMA) marbles; cell molding method and belt molding method. Cell molding method has low productivity and belt molding method has high equipment cost as well as high production cost. A new production method far PMMA marbles using plastic films as molds was studied in this investigation to overcome the shortcomings of cell molding and belt molding method. As plastic film molds for producing PMMA marbles, poly(vinyl acetate) film was used. A methyl methacrylate compound, which has good processability in film molding and shows good mechanical properties after curing, was prepared and used to produce PMMA marbles by film molding method. Properties of the PMMA marbles produced by film molding method were similar to, or higher than, those of commercial PMMA marbles produced by cell molding and belt molding method respectively. The film molding method is considered to have high possibility in commercial application.

The Optimum Mixture Condition for Stabilization of Songdo Silty Clay (송도 지역 실트질 점성토 고화처리를 위한 최적 배합 조건)

  • Kim, Jun-Young;Jang, Eui-Ryong;Chung, Choong-Ki;Jang, Soon-Ho
    • Journal of the Korean Geotechnical Society
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    • v.27 no.5
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    • pp.5-15
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    • 2011
  • Recent increase of large scale construction near costal area has also increased the application of soft ground treatment. As a result, solidification with cement and lime which increases stability and durability of soils, is frequently used for surface layer stabilization in soft ground site. While stabilization of very soft clay with high plasticity and compressibility has widely been studied, studies on silty clay with low plasticity and compressibility are relatively rare. In this study, after stabilizing low plasticity silty clay of Songdo area with cement and lime under various water contents, mixing ratio, and curing time, uniaxial compression test and plate load test were performed. Strength properties from both tests were considerably consistent. And trackability of construction equipment on the treated surface layer of dredged land was estimated. Finally, optimum mixing condition for Songdo silty clay was proposed.

A Study on Productivity Improvement Scheme Through Site Case Study In PSM (현장 사례를 통한 PSM 공법의 생산성 향상 방안에 관한 연구)

  • Lee Tai Sik;Lee Won Yong;Kim Gil Hong
    • Proceedings of the Korean Institute Of Construction Engineering and Management
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    • autumn
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    • pp.541-544
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    • 2001
  • PC Box Girder was constructed by PSM(Precast Span Method) to solve the shortage of the construction period. The site case study was used in the PSM to find the construction productivity improvement. In this case study, main reasons of low productivity were founded unskilled technical engineers and insufficient equipment management winter season concrete curing condition. Productivity improvements are presented by assigning production personnel appropriately, motivation which increased by providing incentives for technical engineers, strictly cooperation of each participant, organizational teamwork, and Promoting productive work condition. Additional method of productivity improvements are continuous improvement of the work methods by considering the feedback on previous work, and continuous training to best handle the site conditions. This study of productivity improvement will help to use the most advantage of the PSM method and desire to successfully plan the future construction performance.

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