• 제목/요약/키워드: Cure behavior

검색결과 171건 처리시간 0.023초

시아네이트 에스터 수지의 화학유변학적 거동 및 탄소섬유강화 고분자 복합재료의 물성 (Chemorheological Behavior of Cyanate Ester Resin and Properties of Carbon Fiber Reinforced Polymer Composites)

  • 나효열;윤병철;김승환;이성재
    • Elastomers and Composites
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    • 제48권2호
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    • pp.133-140
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    • 2013
  • 탄소섬유강화 고분자(CFRP) 복합재료는 고분자 매트릭스 내에 탄소섬유를 강화제로 사용한 복합재료이다. 최근 고온 및 고진공 조건이 요구되는 항공우주 및 전자산업용 고성능 재료로 사용하기 위해 높은 열안정성과 낮은 기체방출 특성을 갖는 CFRP 복합재료가 활용되고 있다. 이러한 용도에 시아네이트 에스터 수지는 가장 적합한 매트릭스 수지로 꼽히고 있다. 본 연구에서는 시아네이트 에스터 수지와 촉매의 조합, 경화 거동 및 경화 사이클을 최적화하기 위해 화학유변학적 거동을 분석하였다. 최적 조건은 촉매 100 ppm을 첨가한 수지 조성물을 $150^{\circ}C$에서 경화한 경우로 나타났다. 열안정성과 기체방출 특성을 분석한 결과 경화된 수지 조성물은 열분해 온도 $385^{\circ}C$ 및 전체질량손실 0.29%를 나타내었다. 설정한 수지 조성 및 경화 조건을 사용하여 CFRP 프리프레그 및 이를 적층한 복합재료를 제조하였다. 복합재료의 인장 탄성률을 이론적 모델과 비교한 결과 매우 일관성이 있었다.

서울시 교원의 다빈도 질환 및 관리실태 조사 (A Study on Health Problems and Management of School Teachers in Seoul)

  • 전나미;윤재희;김채윤;김영숙;황나미;이경아
    • 한국학교보건학회지
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    • 제25권2호
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    • pp.159-167
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    • 2012
  • Purpose: This study was conducted to identify the job-related health problems of school teachers in Seoul area and investigate their disease management behavior. Methods: This study used the on-line survey to investigate frequent health problems and management behavior of teachers. And job-related diseases were identified using date from the National Health Insurance Corporation. Collected data were analyzed by descriptive statistics, t-test and ANOVA. Results: The frequent health problems of teachers were varicose veins, vocal cord disease and thyroid disease. And Job-related health diseases were varicose veins and vocal cord disease. These problems increased with career. 57.4% and 28.4% teachers in varicose veins and vocal cord disease did not do any management behavior to prevent or cure the disease. 56.8% teachers did not know how to prevent the diseases and 16.3% teachers did not practice even though they know the methods of prevention. Conclusion: Teacher's health examination should include varicose veins and vocal cord disease examination. And schools should try to offer various programs for preventing job-related health problems.

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Amine Terminated Polyetherimide/에폭시 수지 시스템의 경화공정연구와 파괴인성에 관한 연구 (A Study on the Curing Behavior and Toughness of Amine Terminated Polyetherimide/Epoxy Resin System)

  • 김민영;이광기;김원호;황병선;김대식;박종만
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2002년도 춘계학술발표대회 논문집
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    • pp.147-150
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    • 2002
  • The cure kinetics of blends of epoxy (DGEBA:diglycidyl ether of bisphenol A)/anhydride (NMA:nadic methyl anhydride) resin with synthesized amino terminated polyetherimide (AT-PEI) were studied using differential scanning calorimetry (DSC) and Dynamic Mechanical Analysizer(DMA) under isothermal condition to determine the reaction parameters and gel-vitrification behavior. The fracture toughness of AT-PEI 20phr/epoxy resin system was improved over 224% and 42.5% more than neat epoxy resin and commercial PEI/Epoxy Resin System.

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4관능성 에폭시 수지/불소를 함유한 에폭시 수지 블렌드 시스템의 경화거동 및 파괴인성에 관한 연구 (Studies on Curing Behavior and Fracture Toughness of Tetrafunctional Epoxy Resin/Fluorine-containing Epoxy Resin Blend System)

  • Jin, Fan-Long;Lee, Jae-Rock;Park, Soo-Jin;Shin, Jae-Sup
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2002년도 추계학술발표대회 논문집
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    • pp.273-275
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    • 2002
  • In this studies, curing behavior and mechanical properties of tetrafunctional epoxy resin (4EP)/ fluorine-containing epoxy resin (FEP) blend systems was investigated with 4, 4'-diaminodiphenol methane (DDM) as a curing agent. The cure activation energies $(E_a)$) were studied by Flynn-Wall-Ozawa's equation with dynamic DSC method. For the fracture toughness of the casting specimens, the critical stress intensity factor ($K_{IC}$) and the specific fracture energy ($G_{IC}$) were determined by fracture toughness test.

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인터넷쇼핑몰 관련 소비자 피해에 관한 대응행동 -패션상품 구매를 중심으로- (Research for the Consumer's Damage in Internet Shopping Mall -Fashion Goods on Internet Shopping Mall-)

  • 장현선
    • 가족자원경영과 정책
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    • 제10권3호
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    • pp.149-169
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    • 2006
  • As e-commerce is expanding rapidly, the consumer's damage in the e-commerce is also dramatically increased. This research was mainly focused on the consumer's damage experiences through the e-commerce, the consumer's behavior's when they were confronted with troubles, and the way to handle their damages in the e-commerce. This research was made with the intention of not only supplying the academic data on the consumer's damage but also understanding the consumer's basic behavior patterns in e-commerce. This research was supported by the surveys conducted to consumers who had previously experienced fashion e-commerce. Total 1230 questionnaires out of returned questionnaires were sampled for the final analysis. Main findings are as follows. 1) More than 90% of respondents answered that they had experienced troubles 2) Most consumers did complain their damages actively and tried to obtain proper cure from the seller.

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초등학생의 시력건강행위 영향요인 (Factors Related to Visual Health Promotion Behavior of Elementary School Aged Children)

  • 김정숙;오진주
    • 지역사회간호학회지
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    • 제12권1호
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    • pp.142-149
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    • 2001
  • The health education for elementary school students is a very important factor in the development of adult health practices. Particularly, eyesight is difficult to recover if lost. Therefore, prevention is better than cure. This study was conducted to investigate the factors that affect the visual health behavior of elementary school students and to furnish basic materials and directions for the promotion of elementary school health. The investigation was carried out for 4 days from 9. 18. 2000 to 9. 21. 2000 for 199 children in 3 elementary schools. A questionnaire was composed of 3 questions about general property. 20 questions about visual health behavior. 7 questions about visual self-efficacy. 5 questions about visual motivation. 16 questions about self-conception. 20 questions about the health locus of control. The data was analysed by an SAS program for t-test. ANOVA. correlation, and multiple regression tests. The results are as follows. 1. The visual health behavior of elementary school children was good (average 52.53). 2. For visual health behavior, school, year, and sex were influential factors. economic levels were not. 3. Visual health behavior had a significant correlation with visual self-efficacy, visual health motives and self-conception. but not with the locus of control. 4. In the multiple regression test, visual self-efficacy and self-conception were significant prediction factors -- the suitability of the regression model was 30.8%. Suggestions from the results are as follows: First, school year and sex had a significant influence on visual health behavior: therefore, it is necessary to consider these two factors when education programs are developed. Second, this study was carried out for students in a partial area only. Therefore, repeated studies for a large sample are necessary for the future.

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Analyzing Gifted Students' Social Behavior on Social Media at COVID-19 Quarantine

  • Khayyat, Mashael;Sulaimani, Mona;Bukhri, Hanan;Alamiri, Faisal
    • International Journal of Computer Science & Network Security
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    • 제22권9호
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    • pp.7-14
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    • 2022
  • COVID-19 has caused a global disturbance, increased anxiety, and panic, eliciting diverse reactions. While its cure has not been discovered, new infection cases and fatalities are being recorded daily. The focus of the present study was to analyze the reaction of gifted undergraduate students on social media during the quarantine period of the COVID-19. A special group of gifted students, who joined the program of attracting and nurturing talents at the University of Jeddah, University students as were the target sample of this study. To analyze online reactions during the pandemic; the choice of university students was arrived at as they are perceived to be gifted academically. Hence, the analysis of the impacts on their behavior on social media use is imperative. This study presented accurate and consistent data on the effects of social media using Twitter platforms on gifted students during the quarantine occasioned by the COVID-19 pandemic. The behavior of learners due to during the use of social media was extensively explored and results analyzed. The study was carried out between April and May 2020 (quarantine period in Saudi Arabia) to establish whether the online behavior of gifted students reflects positive or negative feelings. The methods used in conducting this study the research were online interviews and scraping participants' Twitter accounts (where most of the online activities and studies take place). The study employed the Activity theory to analyze the behavior of gifted students on social media. The sample size used was 60 students, and the analysis of their behavior was based on Activity theory Overall, the results showed proactive, positive behavior for coping with a challenging situation, educating society, and entertaining. Finally, this study recommends investing in gifted students due to their valuable problem-solving skills that can help handle global pandemics efficiently.

수종 광중합 복합 레진의 중합 깊이와 광조사 시간에 따른 중합률에 관한 연구 (A STUDY ON THE DEGREE OF CONVERSION OF LIGHT CURING COMPOSITE RESIN ACCORDING TO THE DEPTH OF CURE AND LIGHT CURING TIME)

  • 김경현;권오승;김현기;백규철;엄정문;권혁춘
    • Restorative Dentistry and Endodontics
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    • 제22권1호
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    • pp.35-60
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    • 1997
  • Physical properties of composite resins such as strength, resistance to wear, discoloration, etc, depend on the degree of conversion of the resin components. The clinical behavior of restorative resins varies brand to brand. Part of this variation is associated with the filler and differences in the polymer matrix. The polymer matrix of resins may differ because the involved monomers are dissimilar and because of variation in the catalyst system. The purpose of this study was to evaluate the degree of conversion of the composite resins according to the depth of cure and light curing time. 7mm diameter cylindrical aluminum molds were filled with each of five different hybrid light curing composite resins(Z-100, Charisma, Herculite XRV, Prisma TPH, Veridonfil) on the thin resin films. The molds were 1mm, 2mm, 3mm, 4mm, and 5mm in depth to produce resin films of various heights. Each sample was given 20sec, 40sec, and 60sec illumination with a light source. The degree of conversion of carbon double bonds to single bonds in the resin films was examined by means of Fourier Transform Infrared Spectrometer. The results were obtained as follows; 1. There was difference in the degree of conversion among five light curing composite resins according to the depth of cure for 20sec, 40sec, and 60sec illumination with light source with statistical significance(P<0.05). 2. Five light curing composite resins show lower degree of conversion at surface of the resin than depth of 1mm. 3. The degree of conversion of five light curing composite resins was siginificantly reduced from the maximum for the resin film when the light passed through as little as 1mm of each composite. 4. The degree of conversion of five light curing composite resins decrease significantly at the depth of 4mm, and polymerization was not occured at the depth of 5mm except for Prisma TPH. 5. The degree of conversion of five light curing composite resins was increased with increased light curing time, and there was no significant differences in the degree of conversion above 4mm in Z-100, 3mm in Charisma, and at depth of 5mm in Herculite XRV and Veridonfil(P>0.05).

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치환기 변화에 따른 열잠재성 양이온 촉매의 합성과 잠재특성 연구 (Synthesis and Latent Characteristics of Thermal Cationic Latent Catalysts by Change of Substituent)

  • 박수진;허건영;이재락;심상연;서동학
    • 폴리머
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    • 제25권4호
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    • pp.558-567
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    • 2001
  • 피라진염의 치환기를 변화시킨 열잠재성 양이온 촉매를 합성하고, 이관능성 에폭시(diglycidylether of bisphenol-A, DGEBA)에 개시제로서 1 wt% 촉매를 혼합하여 동적 DSC방법을 이용한 경화 거동과 열잠재 특성에 대해 연구하였다. 그 결과 합성된 촉매들은 에폭시 시스템에서 우수한 열잠재성을 가지고 있음을 확인하였다. 치환기의 염기도(basicity)가 높을수록 경화온도와 활성화 에너지는 높아지고 활성은 낮아졌는데 이는 활성과 경화거동이 링 스트레인(ring strain) 및 도입된 치환기의 염기도(basicity)에 의해 조절되기 때문인 것으로 사료된다. 결론적으로, 전자공여 그룹인 메틸기를 도입한 촉매의 활성은 경화시 개시단계에서 염기도 증가로 인한 피라진의 이탈능과 벤질 양이온의 안정성이 감소되었기 때문에 낮아졌으며, 전자수용 그룹인 시아노기를 도입한 촉매의 활성은 유기효과와 공명에 인해서 벤질 양이온의 안정성이 증가됨으로써 높아졌다.

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미세역학적 시험법을 이용한 단-섬유 형태 형상기억합금/에폭시 복합재료의 계면특성 및 응력-경화 감지능 (Interfacial Properties and Stress-Cure Sensing of Single-Shape Memory Alloy (SMA) Fiber/Epoxy Composites using Electro-Micromechanical Techniques)

  • 장정훈;김평기;왕작가;이상일;박종만
    • 접착 및 계면
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    • 제9권3호
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    • pp.20-26
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    • 2008
  • 형상기억합금(SMA)의 구조는 부가된 온도 혹은 응력에 의해 마텐자이트로부터 오스테나이트로의 변화가 가능하다는 것은 잘 알려져 있다. 형상기억합금섬유의 자체 형상회복력으로 인해 응력과 온도가 적용되는 동안에 응력이나 경화 모니터링 센서 또는 작동기로서 사용되었다. 초탄성 현상은 연속적인 기계적 하중 하에서나 온도변화 중에 응력-변형률 곡선에서 확인되었다. 반복하중 실험을 통해 응력-변형률 곡선에서 나타난 초탄성 현상 구간이 나타나는 응력 이력현상이 발생함을 확인하였다. 이것은 형상기억합금섬유 혹은 에폭시에 함침된 형상기억합금섬유 복합재료가 반복하중으로 계면물성 저하로 인한 형상기억 회복 성능의 저하를 의미한다. 강성도가 큰 에폭시 사용과 형상기억합금섬유의 표면처리 이후 형상기억합금섬유와 에폭시 사이의 계면결합력의 증대에도 불구하고 유사한 불완전한 초탄성을 보여 주었다. 단-형상기억합금섬유/에폭시 복합재료 내부에 남은 잔류 열과 이에 따른 잔류 응력으로 인해 에폭시에 함침된 단-형상기억합금섬유에서는 경화과정에서 불완전한 회복을 나타났다.

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