• 보존과학회지
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• 제38권4호
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• pp.334-346
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• 2022

The manufacturing technique was studied through the structure and material characteristics of the walls and the painting layers of the Avalokitesvara Bodhisattva mural of Geungnakjeon Hall, Daewonsa Temple. The mural is painted and connected to the earthen wall and the Junggit, and the wall is composed of wooden laths as a frame, the first and middle layers, the finishing layer, and the painting layer. The first layer, middle layer, and finishing layer constituting the wall were made by mixing weathered soil and sand. It was confirmed that the first layer had a high content of loess below silt, and the finishing layer had a high content of fine-sand and very fine sand. For the painting layer, a ground layer was prepared using soil-based mineral pigments, and lead white, white clay, atacamite, minium, and cinnabar (or vermilion) pigments were used on top of it. The Avalokitesvara Bodhisattva mural was confirmed to belong to a category similar to the soil-made buddhist mural paintings of Joseon Dynasty. However, it shows characteristics such as a high content of fine sand in the finishing layer and overlapping over other colors. Such material and structural characteristics can constitute important information for future mural conservation status diagnoses and conservation treatment plans.

• 보존과학연구
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• 통권27호
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• pp.23-42
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• 2006

This study is about gilt bronze ornament, that is from Deok Cheon-Ri in Gyeong Ju, of conservation treatment process and of scientific analysis. This relic gathered with soil around the relic by Polyurethane foam. While the relic got rid of soil, Took X-rays. As the result, we decided to process reconstruction as condition that the relic was dug up. After the conservation treatment processed, we made a frame to display the relic. Investigated manufacture techniques of the relic after the conservation treatment processed, and thenexecuted scientific analysis of the relic for a chemical experiment. A analysis of the results of components for composition layers using the SEM-EDS can be briefly summarized as below; Firstly, the average contents of outer, inner and body corrosion layer have a Cu-60.9~39.3wt% and analyzed a little impurities material which is Fe-0.5wt%.Secondly, the average contents of body have a Cu-99.7wt% which was using manufactured by pure copper. Thirdly, gold layer have a mercury of 9.5wt% which indicate that layer was manufactured by mercury amalgam gilding technique.

• 보존과학회지
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• 제37권6호
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• pp.748-766
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• 2021

익산 쌍릉은 대왕릉과 소왕릉을 포함하는 명칭으로 백제 사비기(538~660 AD)의 횡혈식석실묘이다. 소왕릉의 발굴과정에서 노출된 봉분 동측 토층은 하부로부터 기반층, 정지층, 백제시대 판축층, 도굴층 및 일제강점기 복토층으로 나눌 수 있다. 이 연구를 위해 층준을 세분하여 시료를 확보하고 재료학적 특성을 분석하였다. 토층의 입도분석 결과, 대체로 사양토의 토성을 보이며, 백제시대 판축토층에서는 양질사토가 성토되어 있고 그 위로 사양토가 판축의주를 이룬다. 백제층의 중앙부와 최상부에는 점토 함량이 많고 일정한 입도를 가진 양토를 사용하였다. 모든 토층은 층위에 따라 약간의 차이가 있지만, 유사한 지구화학적 거동특성을 보여 토양의 모재와 성인은 거의 같은 것으로 나타났다. X-선 회절분석으로 모든 층위에서 카올리나이트를 동정하였으며, 주사전자현미경으로 카올리나이트와 할로이사이트를 확인하였다. 따라서 소왕릉 봉분의 백제시대 판축토층은 유적 일대에서 조달한 고령토가 함유된 사양토로 성토하였으며, 중상부에 점성이 강한 양토를 사용하여 불투수층을 조성하고 봉분 최상부를 밀실하게 마감한 것으로 해석된다.

• 한국디지털건축인테리어학회논문집
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• 제3권2호
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• pp.14-19
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• 2003

In this paper, I tried to apply the viewpoint and the method of "Cultural Study" to the analysis of a Architecture. "SE HAN DO(歲寒圖/ Jeonghee Kim 金正喜/ 1844)", the masterpiece of the "literary artist's paintings"(文人畵) is used as a 'TEXT‘(: parole) and analysed to show how artist's value and social-cultural ideology (as a 'CONTEXT':langue) are projected to the space and architectural vocabulary.

• 보존과학회지
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• 제35권6호
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• pp.573-587
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• 2019

본 연구는 전통적인 철화분청사기 안료를 재현하기 위하여 국내산 자철석과 점토, 비가소성 원료를 혼합하여 재현시편을 제작하고, 발색이 양호한 30개의 시편들을 과학적으로 분석함으로써 유약의 발색특성을 알아보고자 하였다. 안료의 주원료인 자철석은 1,200℃의 환원 환경에서 짙은 흑색으로 발색하는 안료이나, 부가적으로 첨가되는 석회 성분과 반응하여 1,230℃ 산화 환경에서는 녹황색 계열로 변색된다. 적철석은 소성 온도 및 환경에 크게 영향을 받지 않으나 Fe를 10 wt% 이상 함유한 점토와 혼합하였을 때는 짙은 흑색으로 발색한다. 안료의 유동성은 R₂O₃/RO₂ 값에 의해 결정되며, 이는 발색에도 영향을 미친다. 미세조직 관찰에서 안료의 입자크기와 소성 환경에 따라 유약층의 발색과 철산화물 결정들이 일부 다른 양상을 보인다. 자철석을 원료로 한 안료는 1,200℃ 산화 환경에서는 유약층과 분장토의 경계면에 철산화물이 응집체 형태로 존재하며, 흑갈색으로 발색하지만, 환원 환경 소성에서는 철산화물의 응집체가 존재하지 않고 유약층에 균질하게 분포하며, 짙은 흑색으로 발색한다. 반면, 적철석을 기반으로한 안료는 산화 환경에서 유약층내 수지상 조직을 형성하며, 흑색으로 발색한다.

• 보존과학연구
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• 통권8호
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• pp.13-34
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• 1987

A large number of metallic relics were excavated by a team of Kyungsang University museum (Nov. 25, 1985 - Jan. 29, 1986) from the groups of tombs located at No. 9 Mountain,Okchun Village, Sungsan-Ri, Ssangchak-Myon, Hyopchun-Kun, Kyungsangnam-Do which are believed to date back to Kaya period. The Research Institute of Cultural Properties was in charge performing scientific conservation and restoration for the iron cuirass and horse halmet (for one year and seven months, Feb. '86 - Sep. '87)The scientific processing for them are as follows :1. Taken Photo and record the actual conditions prior to conservation.2. Taken radiography3. Elimate Goethite ($\alpha$-FeOOH) layer on the surface using Air-brasive, remaining Magnetite ($Fe_3O_4$) layer.4. Treat to dechlorinize with 3% Sodium-Sesquicarbonate5. Protected the relics with Ruscoat acryl resin using vacuum infiltration method.6. Joint the sherd using Araldite and Microballoon mixture.7. Restored missing parts by Araldite SV 427 and HV 4278. Made record and taken photo after restoration Several hundred of sherds of relics, small or large, were restored by assortment which this method for the purpose of contributing to the further study of ancient Kaya history.* Conservator, National Research Institute of Cultural Properties.

• 보존과학연구
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• 통권30호
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• pp.189-202
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• 2009

Ceramics from Taean shipwreck were studied to investigate the deterioration by soluble salts and desalination pattern according to each ceramic characterization. NaCl crystals were found as a crystal growth on the ceramic microstructure and deteriorated to push off the glaze layer of some Puncheong ware sample. As a result of monitoring the desalination pattern of ceramics for 74days, the earthenware sample with big pores and no glaze removed soluble salts so fast, but Puncheong ware and Whiteware samples removed lots of soluble salts slowly and continuously. Generally, it takes long time to remove soluble salts from porcelains, due to small pores and glaze, but the long-term desalination probably can cause the damage on the surface layer such like glaze. As some soluble salts still remains in the ceramic microstructures after desalination, it is very important to control and keep the relative humidity stable through the proper storage. There are various ceramic deterioration patterns by soluble salts. Therefore, it needs to select the desalination method of ceramics from shipwreck, considering the material characteristics and the production techniques.

• 한국제4기학회지
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• 제17권2호
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• pp.145-148
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• 2003

The Kunang cave paleolithic site is located at Tanyang [$N37^{\circ}2'$, $128^{\circ}21'E$], Chungbuk Province, which is in the Central part of the Korean peninsula. The cave is developed at 312 amsl in a karstic mountainous area. The South Han River flows across this region and other caves can also be found near the river. The site was discovered in 1986 and excavated 3 times by the Chungbuk National University Museum until now. The cave was wellpreserved from modem human activities until the first discovery. The full length of the cave is estimated to be ca. 140 m. However, a spacious part up to 11 m from the entrance has been excavated. Eight lithological units are divided over the vertical profile at a depth of 5 m. Each unit is deposited in ascending order as follow: mud layer (Unit 9), lower complex (Unit 8) which is composed of angular blocks and fragments with a muddy matrix, lower travertine layer (Unit 7； flowstone), middle complex (Unit 6; cultural layer) which is composed of fragments with a muddy matrix, middle travertine layer (Unit 5； flowstone), yellowish muddy layer (Unit 4), upper complex (Unit 3； cultural layer) which has a similar composition to Unit 8. the upper travertine layer (Unit 2； flowstone), and finally surface soil layer (Unit 1). The most abundant vestiges in the cultural layers are the animal bones. They are small fractured pieces and mostly less than 3 cm in length. About 3,800 bone pieces from 25 animal species have been collected so far, 90 percent of them belonging to young deers. Previous archaeological study of these bone pieces shows thatprehistoric people occupied the cavenot for permanent dwelling but for temporary shelter during their seasonal hunting activity. More extensive studies of these bones together with pollen analysis are in progress to reconstruct the paleoenvironment of this cave. Only a single date (12,500 BP) obtained from a U-Th measurement of the upper travertine layer was previously available. In spite of the importance of the cave stratigraphy, there was no detail chronological investigation to establish the depositional process of the cultural layers and to understand the periodic structure of the cave strata, alternating travertine floor and complex layers. We have measured five 14C age dating (38900+/-1000, 36400+/-900, 40600+/-1600, more than 51000 and 52000 14C BP) using Seoul National University 14C AMS facility, conducted systematic process of the collagen extraction from bone fragments samples. From the result, we estimate that sedimentation rate of the cave earth is constant, and that the travertine layers, Unit 2 and Unit 3, was formed during MIS 5a(ca. 80 kBP) and MIS 5c (ca. 100 kBP) respectively. The Kunang Cave site is located at Yochonli of the region of Danyang in the mid-eastern part of Korea. This region is compased of limestones in which many caves were found and the Nam-han river flows meanderingly. The excavations were carried out three times in 1986, 1988, and 1998.

• 보존과학회지
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• 제35권4호
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• pp.363-372
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• 2019

Animal glue has been used as a binder in Dancheong since the Joseon dynasty. Binders play an important role in determining the physical characteristics of a painting layer. The analysis of binders can be used to identify the materials and techniques used in traditional Dancheong. Binders can be investigated using physicochemical component analyses methods such as gas chromatography/mass spectrometry, pyrolysis-gas chromatography/mass spectrometry, and fourier transform infrared spectroscopy, but the detection characteristics vary depending on the degradation properties of the pigment and binder. Therefore, cross-validation using a combination of physicochemical analysis and enzyme immunoassay is used to increase the reliability of the results. In this study, we present an enzyme-linked immunosorbent assay (ELISA) as an example of an enzyme immunoassay as a method for analyzing animal glue, a traditional binder used in Korea. The applicability of ELISA was tested using commercial animal glue, in addition to animal glue produced using a variety of extraction conditions. The animal glue was analyzed in a Noerok-additionally coated-replica sample to evaluate the possibility of analyzing the animal glue in a paint layer mixed with pigment. Based on the results, we performed an assay on the use of animal glue in the Dancheong sample of the temples of the Joseon dynasty, that are estimated to have been built in the 17^th century.

• 보존과학연구
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• 통권14호
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• pp.77-93
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• 1993

In order to study for the production techniques and the materials of using in Korean Lacquer Antiques, we examined the section structure by SEM and Microscope, the qualitative analysis of lacquer layer by XRF and XRD, the qualitative analysis of Golhae layer by XRF and XRD, the qualitative analysis of Golhae by EDS on the locquer-wares which was excavated from Anapchi Pond Site in Kyungju and Miruksa Temple Site in Iksan. In the lacquer-wares excavated from Anapchi Pond Site, the lacuqer-wares layers made by a cloth attached on the surface of wooden vessel and Golhae-a mixture of clay and lacquer-covered on the cloth and finally finished with the red lacqure, being mixed with pure mercury sulfide(HgS) and lacquer. And raw materials of Golhae made of clay. The lacquer-wares excavated from Miruksa Temple Site in Iksan, we presumed that the lacquer-wares used fine born grains in place of clay for the raw materials of Golhae. Expecially in case of black lacquer-tray, we found that lacquer put on the surface of wooden vessel without cloth attaching and Golhae covering and the production of wooden vessel was used power-driven machine.