• Title/Summary/Keyword: Cu Powder

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Effects of F-doping on perparation and superconducting characteristics of ag-sheathed Tl-1223 tapes

  • 정대영;김희권;이준호;차무경;김영철;이호섭
    • Progress in Superconductivity and Cryogenics
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    • v.2 no.1
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    • pp.1-6
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    • 2000
  • The effects of partial substitution of fluorine on physical properties were studied in Ag-sheathes tapes of $Tl_{0.8}Pb_{0.2}Sr_{1.8}Ba_{0.2} Ca_{2.2}Cu_3O_yF_x (0{\leq}x{\leq}1)$ nominal compositions. The tapes were prepared using the powder-in-tube method incorporating an in-situ reaction method. $CuF_2$ was used as a source of F. It was found that F-doping in Tl-1223 system resulted in a decrease in formation temperatire of Tl-1223 phase. and thus significantly deteriorated their superconducting properties. Such disadvantages seem to originate by the fromation of non-beneficial phases such as SrF2 in the early stage of the powder preparation process.

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A Study on the Well-being Technique Natural Dyeing with Natural Resources (1) - Natural Dyeing of Cotton Fabric using Perilla frutescens var. acuta - (천연물질을 활용한 웰빙기법 천연염색에 관한 연구 (1) - 소엽을 이용한 면직물의 염색 -)

  • Kim, Sang-Yool
    • Fashion & Textile Research Journal
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    • v.10 no.5
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    • pp.771-778
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    • 2008
  • The natural dyeing of cotton fabric with Perilla frutescens var. acuta extract was investigated. The proper extraction temperature and time were $100^{\circ}C$ and 120 minutes. The proper temperature, time and colorant powder concentration for the dyeing of cotton fabric with Perilla frutescens var. acuta powder were $90^{\circ}C$, 60 minutes and 15%(o.w.b.), respectively. In various mordanted methods, the K/S values of simultaneous-mordanted methods were higher than those of pre-and post-mordanted methods. And the Cu-and Fe mordant showed higher K/S values than those of other mordants. Light colorfasness of mordanted cotton fabric was poor, but the other colorfasnesses were shown to be good. The cotton fabric mordanted with Cu mordant was showed effective bacterial reduction.

Preparation of the Copper Oxalate Powder by Ethanol Oxalic Acid Method (수산에타놀법을 이용한 수산동 분말의 합성)

  • Choi, H.L.;Lee, B.W.
    • Journal of Power System Engineering
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    • v.9 no.4
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    • pp.124-129
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    • 2005
  • Copper oxide, CuO, are very important components include of high temperature super- conductors, and widely used. The properties of sintered materials were affected by the size and shape of copper oxide with starting materials in the solid-phase reaction. A homogeneous and fine CuO powder was prepared by thermal decomposition of the copper oxalate precursor. Copper oxalate was precipitated by the addition of copper nitrate solution to an oxalic acid solution. The influence of various factors such as temperature, pH, concentration as well as ultrasonic irradiation in the solution were investigated.

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Electromagnetic Properties of Bi System Superconductor for Neutron Irradiation

  • Lee, Sang-Heon;Choi, Yong
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1239-1240
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    • 2006
  • Effects of $Ag_2O$ doping on the electromagnetic properties in the BiSrCaCuO superconductors. The electromagnetic properties of $Ag_2O$ doped and undoped BiSrCaCuO superconductor were evaluated to investigate the contribution of the pinning centers to the magnetic effect. It was confirmed experimentally that a large amount of magnetic flux was trapped in the $Ag_2O$ doped sample than that in the undoped one, indicating that the pinning centers of magnetic flux are related closely to the occurrence of the magnetic effect. It is considered that the area where normal conduction takes place increases by adding $Ag_2O$ and the magnetic flux penetrating through the sample increases. The results suggested that Ag acts to increase pinning centers of magnetic flux, contributing to the occurrence of the electromagnetic properties.

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Effect of Metal Oxide on the Superconductivity of YBCO

  • Lee, Sang-Heon
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1241-1242
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    • 2006
  • Electromagnetic properties of $CeO_2$ doped and undoped YBaCuO superconductors were evaluated to investigate the effect of pinning center on the magnetization and magnetic shielding. The variation $\DeltaM$ with doping was maximum for 3% doping and decrease with further doping. The magnetic shielding was evaluated by measuring the induced voltage in secondary coil and the voltage initially set to 0.5V, decreased to 0.17V and 0.28V respectively for the undoped and 3% $CeO_2$ doped sample. The much less change in the induced voltage for the 3% doped sample is attributed to the increased flux shielding by shielding vortex current. The $CeO_2$ was converted to fine $BaCeO_3$ particles which were trapped in YBaCuO superconductor during the reaction sintering. The trapped fine particles, $BaCeO_3$ may be acted as a flux pinning center.

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TiB2-Cu Interpenetrating Phase Composites Produced by Spark-plasma Sintering

  • Kwon, Young-Soon;V. Dudina, Dina;I. Lomovsky, Oleg;A. Korchagin, Michail;Kim, Ji-Soon
    • Journal of Powder Materials
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    • v.10 no.3
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    • pp.168-171
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    • 2003
  • Interpenetrating phase composites of $TiB_2$-Cu system were produced via Spark-Plasma Sintering (SPS) oi nanocomposite powders. Under simultaneous action of pressure, temperature and electric current titanium diboride nanoparticles distributed in copper matrix move, agglomerate and form a fine-grained skeleton. Increasing SPS-temperature and he]ding time promote densification due to local melting of copper matrix When copper melting is avoided the compacts contain 17-20% porosity but titanium diboride skeleton is still formed representing the feature of SPS . High degree of densification and formation of titanium diboride network result in increased hardness of high-temperature SPS-compacts.

A Study on Crystal Structure Growth of YbBCO Superconductor (YbBCO초전도체의 결정성장에 관한 연구)

  • 박정철;이영매;소대화
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.06a
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    • pp.367-370
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    • 1998
  • In this paper, based on the research of high temperature YBCO superconductor, using the Yb instead of Y, with the YbBCO superconductor powder which was combined by means of conventional solid reaction, textured directional crystal was prepared by MCP method and the character was analyzed. Mixing the starting elements and calcining at 890$^{\circ}C$, 900$^{\circ}C$, 910$^{\circ}C$, single phase YbBCO, Yb$_2$BaCuO$\sub$5/ and BaCuO$\sub$2/ were certified. And from the powder which was calcined at 900$^{\circ}C$ the, sample which became texture-growth by MCP method was well oriented. The result of DTA measurement, the fusing point of YbBCO superconductor and it\`s critical current was measured to be 979$^{\circ}C$, 87K respectively. The critical current density was obtained at the value of 700A/$\textrm{cm}^2$(77K. 0H) calculated by Bean's Model using the measured hysteresis curve of VSM.

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The Effect of Milling Conditions on Microstructure and Phase Transformation Behavior of Ti-Ni Based Alloy Powders (Ti-Ni계 합금분말의 미세조직 및 상변태거동에 미치는 밀링조건의 영향)

  • 강상호;남태현
    • Journal of Powder Materials
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    • v.8 no.1
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    • pp.42-49
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    • 2001
  • Ti-50Ni(at%) and Ti-40Ni-10Cu(at%) alloy powders have been fabricated by ball milling method, and their microstructure and phase transformation behavior were investigated by means of scanning electron microscopy/energy dispersive spectrometry, differential scanning calorimetry (DSC), X-ray diffractions and transmission electron microscopy. In order to investigate the effect of ball milling conditions on transformation behavior, ball milling speed and time were varied. Ti-50Ni alloy powders fabricated with the milling speed more than 250 rpm were amorphous, while those done with the milling speed of 100rpm were crystalline. In contrast to Ti-50Ni alloy powders, Ti-40Ni-10Cu alloy powders were crystalline, irrespective of ball milling conditions. DSC peaks corresponding to martensitic transformation were almost discernable in alloy powders fabricated with the milling speed more than 250 rpm, while those were seen clearly in alloy powders fabricated with the milling speed of 100 rpm. This was attributed to the fact that a strain energy introduced during ball milling suppressed martensitic transformation.

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Fundamental Aspects of Resistance Sintering under Ultrahigh Pressure Consolidation

  • Zhou, Zhangjian;Kim, Ji-Soon;Yum, Young-Jin
    • Journal of Powder Materials
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    • v.19 no.1
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    • pp.19-24
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    • 2012
  • The consolidation results of fine tungsten powders, W-Cu composite and W/Cu FGM by using a novel method combining resistance sintering with ultra high pressure have been reviewed. The densification effects of the consolidation parameters, including pressure, input power and sintering time, have been investigated. The sintering mechanism of this method was quite different from other sintering methods. Particle rearrangement, sliding, distortion and crushing due to the ultra high pressure are the dominant mehanisms at the initial stage, then the dominant sintering mechanisms are transient arc-fused processes controlled by the input power.