• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1183-1184
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• 2006

Core loss of soft magnetic powder cores have been focused on to achieve high efficiency of power supplies. In this study the effects of crystal grain size on core loss were investigated by changing heat treatment conditions. It was found that core loss is influenced by crystal grain size because eddy current loss decreased and hysteresis loss increased by making crystal grain size smaller, and it is also influenced by particle size.

• 한국결정성장학회지
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• 제23권6호
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• pp.272-278
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• 2013

본 논문에서는 CZ법으로 성장시킨 300 mm 사파이어 단결정의 c-축 변형 특성 및 내부 응력 상태를 수치해석하고, 사파이어 단결정에서 sub-grain 결함이 없는 성장 길이를 예측하였다. CZ 성장로의 hot zone 구조는 Ir 도가니 형상 및 상부 단열재 추가 설치 등으로 변경하였다. 본 연구의 시뮬레이션 결과, hot zone 구조 변경에 의한 c-축 변형 차이는 결정 내부에 sub-grain 결함 등이 내부에 생성되어 발생한다. Hot zone 구조 변경에 의해 sub-grain 결함이 없는 성장 길이를 기존 보다 최대 약 57 mm 정도 증가시킬 수 있을 것으로 예측되었다. 그리고 c-축 wafer에 대한 sub-grain 결함을 실험적으로 분석하고, 시뮬레이션 예측 결과와 잘 일치하고 있는 것을 확인하였다. 그 결과, CZ 공정을 이용해 약 250 mm까지 sub-grain 결함이 없는 사파이어 결정을 성공적으로 성장시킬 수 있었다.

• Interaction and multiscale mechanics
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• 제4권2호
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• pp.155-164
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• 2011

The lattice strain evolution within polycrystalline solids is influenced by the crystal orientation and grain interaction. For multi-phase polycrystals, due to potential large differences in properties of each phase, lattice strains are even more strongly influenced by grain interaction compared with single phase polycrystals. In this research, the effects of the grain interaction and crystal orientation on the lattice strain evolution in a two-phase polycrystals are investigated. Duplex steel of austenite and ferrite phases with equal volume fraction is selected for the analysis, of which grain arrangement sensitivity is confirmed in the literature through both experiment and simulation (Hedstr$\ddot{o}$m et al. 2010). Analysis on the grain interaction is performed using the results obtained from the finite element calculation based on the model of restricted slip within crystallographic planes. The dependence of lattice strain on grain interactions as well as crystal orientation is confirmed and motivated the need for more in-depth analysis.

• 대한기계학회논문집A
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• 제20권2호
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• pp.461-472
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• 1996

The relationship between plastic deformation and crystal grain change in warm forging processes of SM10C carbon steel is studied. If the carbon steel is deformed at warm forging temperature(about recrystallization range), material properties are changed due to microstructural chanre of the crystal grain and cementite of the internal part. Some experimental values are investigated in terms of the elliptic degree of cementite, the grain size of cementite and ferrite grain size. When plastic deformation proceeds, the elliptic degree of cementite becomes larger and the grain size of cementite particle becomes small. In addition, the size of ferrite grain becomes fines by recrystallization. The elliptic degree of cementite has a considerable effect on formability. The distribution of effective strain in the forging was calculated by the rigid visco-plastic FEM analysis. The effective strain distribution obtained from the FEM simulation is compared with the experimental result, At the level of effective strain 0.3, dynamic recovery and dynamic recrystallization begin and at the level of over 2.5, the organization of material has better internal structure that is suitable for the following cold forming.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 1995년도 제2회 단조심포지엄 단조기술의 진보
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• pp.100-123
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• 1995

The relationship between plastic deformation and crystal grain change in warm forging processes of SM100 carbon steel is studied. If the carbon steel is deformed in warm forging temperature (about recrystallization range), the crystal grain and cementite of the internal part are changed, so material properties are changed. Some experimental values, such as the elliptic degree of cementite, the grain size of cementitie and ferrite grain size, are investigated. When the plastic deformation proceeds, the elliptic degree of cementite becomes large, the grain size of cementite particle is small, and the size of ferrite grain appears fine by recrystallization. The elliptic degree of cementite has a considerable effect on formability. The distribution of effective strain in the forging is calculated by the rigid visco-plastic FEM analysis. The effective strain distribution obtained from the FEM simulation is compared with the experimental result. At effective strain 0.3 dynamic recovery and dynamic recrystallization begin, over 2.5 the organization of material has better quality that is suitable for the following cold forming.

• 한국주조공학회지
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• 제10권4호
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• pp.324-331
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• 1990

The single crystal of CdTe was grown by modified 6 zone Bridgman method under the conditions of excess Te and excess Cd. To prevent the constitutional supercooling, the crystal growth was done under the temperature gradient of $17^{\circ}C/cm$ in front of the solid /liquid interface and the growth rate was 3mm/hr. The grain morphologies and the growth mechanism were investigated in excess Te and excess Cd conditions. The grain size of excess Te crystal was increased with an increase of the distance from the tip but, in the case of excess Cd crystal, single crystal was not obtained because of the cavities due to the excess Cd vapors so that the grain size was not increased with an increase of the distance from the tip. In addition, the growth of single crystal of CdTe was done with repeated necking ampoule. It was found that the necking had no effects on the grain selection because the cavities trapped in the necking portion acted as heterogeneous nucleation sites.

• 한국초전도ㆍ저온공학회논문지
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• 제24권3호
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• pp.35-40
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• 2022

To fabricate large grain YBCO bulk superconductors by melt process, Sm123 single crystal with a high melting point are mostly used as seeds. However, it also uses Y123 film deposited on MgO single crystal substrate. This study investigated the growth behavior of the Y123 grain during a melt process when single grain YBCO bulk was used as a seed. Single grain Y123 bulk was grown when the seed size was small. When the seed size was relatively large, multiple grains were grown but the grains were still large. Y123 seed crystal was completely decomposed during high temperature anneal at 1040℃ and new Y123 crystals were nucleated during a slow cooling stage below a peritectic temperature. Thereafter, newly formed Y123 crystals from the seed area are thought to grow into the Y1.8 powder compact. The crystallographic orientations of newly nucleated Y123 grains are independent of the crystallographic orientation of Y123 seed. It is thought that the crystallographic orientation of newly nucleated Y123 crystal can be controlled by using Y211-free Y123 single crystal as a seed of homo-seeding melt growth.

• Journal of Welding and Joining
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• 제19권3호
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• pp.325-333
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• 2001

The effect of base metal grain size on isothermal solidification behavior of Ni-base superalloy, CMSX-2 during transient liquid phase (TLP) bonding was investigated employing MBF-80 insert metal. TLP-bonding of single crystal. coarse-grained and fine-grained CMSX-2 was carried out at 1373∼1548k for various holding time in vacuum. The eutectic width diminished linearly with the square root of holding time during isothermal solidification process for single crystal, coarse-grained and fine-grained base metals. The completion time for isothermal solidification decreased in the order ; single crystal, coarse-grained and fine-grained base metals. The difference of isothermal solidification rates produced when bonding the different base metals could be explained quantitatively by the effect of base metal grain boundaries on the apparent average diffusion coefficient of boron in CMSX-2.

• 한국세라믹학회지
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• 제43권11호
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• pp.728-733
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• 2006

The equilibrium or growth shape of ceramic materials is classified largely into two categories according to the thermodynamic conditions imposed. One is a polyhedral shape where the surface free energy is anisotropic, and the other a spherical shape where the surface free energy is isotropic. In the case of grains with a polyhedral shape of anisotropic surface free energy, socalled abnormal grain growth usually takes place due to a significant energy barrier for a growth unit to be attached to the crystal surface. In the case of grains with a spherical shape of isotropic surface free energy, however, normal grain growth with a uniform size distribution takes place. In this contribution, the state-of-the-art of our current understanding of the relationship between the crystal shape and the microstructure evolution during the sintering of ceramic materials in the presence of a liquid phase was discussed.

• Journal of Welding and Joining
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• 제27권6호
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• pp.62-67
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• 2009

Friction stir welding (FSW) was carried out for Al-Mg-Si series aluminum alloys which are being used for automotive body structure. Consequently, Post weld heat treatment (PWHT) was applied to the friction stir welds to evaluate the effect of the paint baking process which is one of the automotive fabrication process on friction stir welded zone (FSWZ) in 443K for 1.2Ks. Grain structure and its crystal orientation distribution was measured about both the as welded specimens and the post weld heat treated specimens. An optical microscope (OM) and an field emission scanning electron microscope (FE-SEM) was used for observing the grain structure and measuring its crystal orientation distribution, respectively. Changes on the grain structure and its crystal orientation distribution were not detected. From the present results, it was confirmed that the paint baking process after FSW do not affect on the grain structure and its crystal orientation distribution of FSWZ. The comprehensive investigations will be performed for various automotive aluminum alloys manufactured by different processes, in the future.