• 소성∙가공
• /
• 제18권3호
• /
• pp.262-267
• /
• 2009

Selective laser sintering is a kind of rapid prototyping process whereby a three-dimensional part is built layer wise by laser scanning the powder. This process is highly influenced by powder and laser parameters such as laser power, scan rate, fill spacing and layer thickness. Therefore a study on fabricating Fe-Ni-Cr powder by selective laser sintering has been performed. In this study, fabrication was performed by experimental facilities consisting of a 200W fiber laser which can be focused to 0.08mm and atmospheric chamber which can control atmospheric pressure with argon. With power increase or energy density decrease, line width was decreased and line surface quality was improved with energy density increase. Surface quality of quadrangle structure was improved with fill spacing optimization.

• 열처리공학회지
• /
• 제20권6호
• /
• pp.323-328
• /
• 2007

This study has been investigated the effect of high temperature gas nitriding (HTGN) heat treatment of STS 444 (18Cr-0.01Ni-0.01C-0.2Nb) ferritic stainless steel in an atmosphere of nitrogen gas at the temperature range between $1050^{\circ}C\;and\;1150^{\circ}C$. The surface layer was changed into martensite and austenite with the nitrides of NbCrN by HTGN treatment. Due to the precipitation of nitrides and matrensite formation, the hardness of the surface layer showed $400Hv{\sim}530Hv$. The nitrogen concentration of the surface layer appeared as 0.05%, 0.12% and 0.92%, respectively, at $1050^{\circ}C,\;1100^{\circ}C\;and\;1150^{\circ}C$. When the nitrogen is permeated from surface to interior, Nb and Cr, which have strong affinities with nitrogen, also move from interior to surface. Therefore it is considered that this counter-current of atoms promotes the formation of NbCrN at the surface layer.

• 한국자기학회지
• /
• 제5권3호
• /
• pp.210-215
• /
• 1995

Glass\Cr/sub 40 .angs. /\[Cr/sub 10 .angs. /\NiFe/sub 50 .angs. /]/sub N/ 다층박막을 층수 N = 1, 2, 3, 4, 5, 6, 10에 따라 dc magnetron sputtering 방법에 의해 제작하였다. 이때 자기 이방성의 형성을 위해 제작 중에 자장을 200 Gauss 가했다. 전류 방향과 외부 자장이 수평, 수직에 따라 자기저항 곡선 MR(xx), MR(xy)를 조사하였다. MR(xx) 곡선의 경우 N = 1, 5, 10 경우 자기저항비가 거의 나타나지 않았으며, 나머지 층수의 경우는 외부 자장에 따라 저항이 증가하는 positive magnetoresistance 현상을 보였다. 또한 곡선의 모양도 H = 0 Oe 근처에서 특이하게 반전되는 자기정항 곡선을 보였다. 이런 현상의 물리적 해석을 NiFe 단층박막의 자기저항 곡선과 비교하여 설명 하였다.

• 한국표면공학회지
• /
• 제30권2호
• /
• pp.93-103
• /
• 1997

High temperature materials used in the elevated temperature and corrosive atmosphere must have the good oxidation resistance and preserve their own mechanical properties simultaneously. For the oxidation resistance, it is very important to form a protective oxide scale such as $Al_2O_3$ or $Cr_2O_3$ on the substrate. However, the additions of protective oxide forming elements such as Cr and Al in the alloy to enhance its oxidation resistance are limited due to the deleterious effects on their mechanical properties. PECVD(P1asma Enhanced Chemical Vapor Deposition) coating processes were employed to improve the oxidation resistance at high temperature. Cr and/or A1 were coated on the substrates of Ni and Inconel 600 at various temperatures of 400, 500, $600^{\circ}C$ and at different conditions of specimen surfaces. Then, coated specimens were exposed to isothermal and cyclic oxidation conditions in air at 1000 and $1100^{\circ}C$. In order to enhance the adhesion between the substrate and coated layer, heat treatments of the coated specimens were conducted in a vacuum. At isothermal oxidation experiments, Al-coated Ni specimen showed better oxidation resistance than pure Ni. At cyclic oxidation experiments at $1000^{\circ}C$. Cr and Al-coated specimen showed better oxidation resistance. Cr-coated Inconel 600 had also showed better oxidation resistance due to Cr in the substrate. By PECVD coating process, oxidation resistance could be improved, but it was not improved as expected due to the weakness of the adhesion between the substrate and the coated layer.

• 소성∙가공
• /
• 제7권5호
• /
• pp.465-473
• /
• 1998

The effect of alloying elements of Ag-Cu-Zr-X brazing alloy on the microstructure and the bond strength of $Al_2O_3/Ni-Cr$ brazed steel joint was investigated. The reaction layer, $ZrO_2$ (a=5.146 ${\AA}$ , b=5.213 ${\AA}$ , c=5.311 ${\AA}$ )was formed at the interface of $Al_2O_3/Ni-Cr$ steel joint by the redox reaction between alumina and Zr. The addition of An and Al to the Ag-Cu-Zr brazing alloy gave rise to changes in the thickness of the reaction product layer and the morphology of the brazement. Sn caused the segregation of Zr was decreased b Al the $ZrO_2$ layer formed at the Ag-Cu-Zr-Al alloy was thinner than that of $ZrO_2$ formed at the Ag-Cu-Zr-An alloy. The fracture shear strength was strongly dependent on the microstructure of the brazement. Brazing with Ag-Cu-Zr-Sn alloy resulted in a better bond strength than with Ag-Cu-Zr or Ag-Cu-Zr-Al alloy.

• 한국윤활학회:학술대회논문집
• /
• 한국윤활학회 2001년도 제34회 추계학술대회 개최
• /
• pp.96-102
• /
• 2001

plasma-sprayed Cr$_2$O$_3$-based coatings containing MoO$_3$ were studied to gain a better understanding of the influence of MoO$_3$ composition in the coatings on their tribological behaviour. A reciprocal type tribo-tester was employed to examine friction and wear behavior of the specimens at high temperature(450。C). The physical characteristics of worn surfaces were investigated by scanning electron microscopy and chemical composition of the coating surfaces was analyzed using a X-ray photoelectron spectrometer. The results showed that friction coefficient of the MoO$_3$-added coatings were lower than those without MoO$_3$ addition. The larger protecting layers were observed at the worn surface of plasma spray coated specimens with MoO$_3$ addition. XPS analysis of the protecting layer indicated that MoO$_3$ composition was dominantly formed at the surface. MoO$_3$ composition in the protecting layer appears to be more favorable in reducing the friction.

• 한국재료학회지
• /
• 제7권1호
• /
• pp.69-75
• /
• 1997

$SiO_{2}/CoNiCr/Cr$ 합금 박막을 RF magnetron sputtering 법으로 Cr의 두께를 변화시키면서 제조하였다. 제조된 박막을 진공 열처리하여 열처리 온도에 따른 포화자화, 보자력, 각형비를 조사하였다. $SiO_{2}/CoNiCr/Cr$ 합금 박막에서 포화자화 값은 Cr 하지층의 두께가 증가함에 따라 감소하고 보자력은Cr 하지층의 두께가 증가함에 따라 증가하였다. 이러한 박막의 포화자화 값은 600 emu/cc, 최대 보자력은 550 Oe를 나타내었다. $SiO_{2}/CoNiCr/Cr(1700{\AA})$ 합금 박막에서는 열처리 온도가 증가함에 따라 포화자화 값은 급격히 감소하고 보자력은 증가하였다. 열처리 온도가 $650^{\circ}C$에서 포화자화 값은 as-deposited상태보다도 1/10로 감소하였고 보자력은 1600 Oe로 최대값ㅇ르 나타내었다. Cr 하지층의 두께와 열처리 온도의 증가에 따른 포화자화의 감소는 하지층에서 자성층으로 Cr이 확산하므로써 자기 모멘트의 감소에 의한 것으로 판단된다. 또한 보자력의 증가는 박막 면에 수직한 방향으로 급격한 결정 성장에 기인한 것이다.

• 한국자기학회:학술대회 개요집
• /
• 한국자기학회 1998년도 춘계연구발표회 논문개요집
• /
• pp.26-27
• /
• 1998

• 한국자기학회:학술대회 개요집
• /
• 한국자기학회 2003년도 하계학술연구발표회 및 한.일 공동심포지엄
• /
• pp.134-135
• /
• 2003

• 한국자기학회:학술대회 개요집
• /
• 한국자기학회 2000년도 춘계연구발표회 논문개요집
• /
• pp.132-133
• /
• 2000