• 제목/요약/키워드: Corprecipitation method

검색결과 2건 처리시간 0.018초

공침법에 의한 $Ni_2Y$ 자성 분말의 합성 (Synthesis of $Ni_2Y$ magnetic particles by coprecipitation method)

  • 김한근;사공건
    • E2M - 전기 전자와 첨단 소재
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    • 제9권9호
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    • pp.906-910
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    • 1996
  • Ferroxplana N $i_{2}$Y(B $a_{2}$N $i_{2}$F $e_{12}$ $O_{22}$ ) magnetic particles, which is one of the hexagonal ferrite were synthesized by a coprecipitation method. The coprecipitates were prepared by adding aqueous solution of BaC $I_{2}$ - 2 $H_{2}$O, NiC $I_{2}$ - 6 $H_{2}$O and FeC $I_{3}$ - 6 $H_{2}$O(of which the mole ratio is $Ba^{+2}$ : N $i^{+2}$ : F $e^{3+}$= 1 : 1 : 6) to a mixture of NaOH and N $a_{2}$C $O_{3}$. The shape of Ferroxplana N $i_{2}$Y magnetic particles obtained at 1, 100(.deg. C) was hexagonal plate-like, average particle size and aspect ratio were 2(.mu.m) and 7, respectively.y.

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결정성장 억제재를 첨가한 SnO$_{2}$ 미세입자의 메탄가스 감지효과 (Methane gas sensing effect of SnO$_{2}$ fine particle mixed with inhibitor to crystal growth)

  • 홍영호;강봉휘;이덕동
    • E2M - 전기 전자와 첨단 소재
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    • 제9권1호
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    • pp.38-43
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    • 1996
  • A coprecipitation method was used for preparing Ca and Pt doped $SnO_2$ fine powder. Components of the powder were investigated by XPS and SIMS. Crystallite size and specific surface area were investigated by TEM, XRD, and BET analysis. $SnO_2$(Ca)/Pt based thick film devices were prepared by a screen printing technique for methane gas detection. Then sensing characteristics of the devices were investigated. As Ca and Pt added, the crystal growth of $SnO_2$ was suppressed during calcining and sintering, and the sensitivity of $SnO_2$(Ca)/Pt thick film to methane gas was enhanced. For the Pt doped $SnO_2$ fine particle, the thick film device shows sensitivity of about 83% to 2000 ppm methane gas at an operating temperature of >$400^{\circ}C$.

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