• 한국군사과학기술학회지
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• 제23권5호
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• pp.435-443
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• 2020

Thermal barrier coating(TBC) applied to fighter and turbine engines is a technology that improves the durability of core parts by lowering the surface temperature of base material. The thermal stress caused by mis-match of the coefficient of thermal expansion between the top coating and the TGO interface is the main cause of TBC breakage. Since the thermal stress is dependent on the microstructure of the TBC, designing microstructure of TBC can improve the durability as well as lower the thermal stress. In this study, the effect of coating thickness, volume of porosity and vertical cracking on the thermal stress was analyzed through finite element analysis. Through the analysis results, a design range of a microstructure that can improve the durability of thermal barrier coating by lowering thermal stress is proposed.

• 한국세라믹학회지
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• 제41권2호
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• pp.176-181
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• 2004

지정폐기물인 전기로 제강 분진은 현재 대부분이 매립 등 부적절하게 처리되고 있어 지하수 오염 등의 환경파괴를 일으킬 위험이 있다. 전기로 제강 분진의 자원화를 위하여 전기로 제강 분진/점토의 조성으로 다공체를 제조하였으며, 다공체의 기공 특성 분석을 하였다. 다공체는 서로 다른 두 개의 미세구조로 형성되어있으며, 표면부위의 미세구조는 치밀하고 검은색이 아니고, 내부부위는 검은색이며 다공성의 미세구조(black coring)를 갖는다. 블랙코아 부위의 면적과 경량화정도를 정량화하기 위하여 Ic(core index)와 Is(shell index)를 정의하였으며, 인공경량골재로서의 최적 경량화 조건은 Ic가 0.5이상이고, Is는 0.4이상이다.

• Journal of Ceramic Processing Research
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• 제13권spc2호
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• pp.363-367
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• 2012

DLC (diamond liked carbon) coating of the tungsten carbide (WC) alloy core surface for molding a glass aspheric lens improves the quality of glass lens and the molding core and is characterized by high hardness, high elasticity, abrasion resistance and chemical stability. In this study, the effect of DLC coating of a thin film by means of the filtered AIP (arc ion plating) technique was examined on Ra and shape of the coated surface. Roughness before and after DLC coating was measured and the result showed that the roughness was improved after coating as compared to before coating. It was observed that DLC coating of the WC alloy core surface for molding had an effect on improving the roughness and shape of the core surface. It is considered that this will have an effect on improving abrasion resistance and the service life of the core surface.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2009년도 추계학술발표대회
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• pp.11.1-11.1
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• 2009

Ternary Al2O3.ZrO2.Y2O3 samples with a eutecticcomposition were prepared by slow cooling. The microstructural evolution wasobserved with X-ray diffraction (XRD), scanning electron microscopy (SEM). TheSEM observation of the ternary samples agreed with the XRD with a completion ofcrystallisation by slow cooling. The target materials commonly have 'cantaloupe skin' microstructures as shown inthe previous studies by Han et al. The nanocomposite may have experienceddifferent cooling rates with two different microstructures, near the surfacehaving experienced optimal conditions for the eutectic reaction during theircooling and thus formed the eutectic microstructure, near the centre havingexperienced a slower cooling rate. The crystallised eutectic ternary Al2O3.ZrO2.Y2O3 system had three different phaseswith a 3Y2O3. 5Al2O3 (yttrium.aluminiumgarnet phase), an alumina phase formed by the eutectic reaction, and a solidsolution of ZrO2 and Y2O3.

• 한국분말재료학회지
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• 제22권3호
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• pp.181-186
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• 2015

In this study, the effect of the friction stir welding (FSW) was compared with that of the gas tungsten arc welding (GTAW) on the microstructure and microhardness of Cu-Ni alloy weldment. The weldment of 10 mm thickness was fabricated by FSW and GTAW, respectively. Both weldments were compared with each other by optical microstructure, microhardness test and grain size measurement. Results of this study suggest that the microhardness decreased from the base metal (BM) to the heat affected zone (HAZ) and increased at fusion zone (FZ) of GTAW and stir zone (SZ) of FSW. the minimum Hv value of both weldment was obtained at HAZ, respectively, which represents the softening zone, whereas Hv value of FSW weldment was little higher than that of GTAW weldment. These phenomena can be explained by the grain size difference between HAZs of each weldment. Grain size was increased at the HAZ during FSW and GTAW. Because FSW is a solid-state joining process obtaining the lower heat-input generated by rotating shoulder than heat generated in the arc of GTAW.

• 소성∙가공
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• 제27권5호
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• pp.281-288
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• 2018

This study deals with the microstructure and tensile properties of 600 and 700 MPa-grade high-strength seismic reinforced steel bars. High-strength seismic resistant reinforced steel bars (SD 600S and SD 700S) were fabricated by TempCore process, especially the SD 700S specimen was more rapid cooled than the SD 600S specimen during the TempCore process. Although two specimens had microstructure of tempered martensite in the surface region, the SD 600S specimen had ferrite-degenerated pearlite in the center region, whereas the SD 700S specimen had bainite-ferrite-degenerated pearlite in the center region. Therefore, their hardness was highest in the surface region and revealed a tendency to decrease from the surface region to the center region because tempered martensite has higher hardness than ferrite-degenerated pearlite or bainite. The SD 700S specimen revealed higher hardness in the center region than SD 600S specimen because it contained a larger amount of bainite as well as ferrite-degenerated pearlite. On the other hand, tensile test results indicated the SD 600S and SD 700S specimens revealed continuous yielding behavior because of formation of degenerated pearlite or bainite in the center region. The SD 600S specimen had a little higher tensile-to-yield ratio because the presence of ferrite and degenerated pearlite in the center region and the lower fraction of tempered martensite enhance work hardening.

• 한국표면공학회지
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• 제42권2호
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• pp.73-78
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• 2009

Quinary Ti-Al-Si-C-N films were successfully synthesized on SUS 304 substrates and Si wafers by a hybrid coating system combining an arc ion plating technique and a DC reactive magnetron sputtering technique. In this work, the effect of Si content on the microstructure and mechanical properties of Ti-Al-C-N films were systematically investigated. It was revealed that the microstructure of Ti-Al-Si-C-N coatings changed from a columnar to a nano-composite by the Si addition. Due to the nanocomposite microstructure of Ti-Al-Si-C-N coatings, the microhardness of The Ti-Al-Si-C-N coatings significantly increased up to 56 GPa. In addition the average friction coefficients of Ti-Al-Si-C-N coatings were remarkably decreased with Si addition. Therefore, Ti-Al-Si-C-N coatings can be applicable as next-generation hard-coating materials due to their improved hybrid mechanical properties.

• Computers and Concrete
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• 제32권1호
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• pp.45-60
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• 2023

Concrete in water environment is easily subjected to the attack of leaching, which causes its mechanical reduction and durability deterioration, and the key to improving the leaching resistance of concrete is to increase the compaction of its microstructure formed by the curing. This paper performs a numerical investigation on the intrinsic relationship between microstructures formed by the hydration of cement and slag and leaching resistance of concrete in water environment. Firstly, a shrinking-core hydration model of blended cement and slag is presented, in which the interaction of hydration process of cement and slag is considered and the microstructure composition is characterized by the hydration products, solution composition and pore structure. Secondly, based on Fick's law and mass conservation law, a leaching model of hardened paste is proposed, in which the multi-species ionic diffusion equation and modified Gérard model are established, and the model is numerically solved by applying the finite difference method. Finally, two models are combined by microstructure composition to form an integrated curing-leaching model, and it is used to investigate the relationship between microstructure composition and leaching resistance of slag-blended cement pastes.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.451-452
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• 2006

The influence of Hi-flux powders characteristics on the performance of magnetic powder cores was studied. It was found that different cooling rate and nozzle configuration could change the shape and microstructure of powders. Smooth surface and spherical shape of powders were beneficial to improve DC bias performance and reduce core losses of magnetic powder core.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2009년도 춘계학술대회 논문집
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• pp.177-181
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• 2009

Compositional gradient CrNx coatings were fabricated using arc ion plating in Ar/$N_2$ gaseous mixture by gradually increasing $N_2$ flux rate from 0 to 120 SCCM. The effect of negative substrate bias on the film microstructure and mechanical properties were systematically investigated with XRD, GDOES, and SEM. The results show that substrate bias has an important influence on film growth and microstructure of gradient CrNx coatings. The coatings mainly crystallized in the mixture of hexagonal $Cr_{2}N$ and fcc CrN phases. By increasing substrate bias, film microstructure evolved from an apparent columnar structure to an equiaxed one. With increasing substrate bias, deposition rate first increased, and then decreased. The maximum of deposition rate was 15 nm/min obtained at a bias of -50V.