• Title/Summary/Keyword: Copper plate

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Synthesis and Microstructure of Porous Al2O3 with Nano-Sized Cu Dispersions (나노크기 Cu 분산입자를 갖는 Al2O3 다공체의 제조 및 미세조직 특성)

  • Yoo, Ho-Suk;Kim, An-Gi;Hyun, Chang-Yong
    • Korean Journal of Materials Research
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    • v.23 no.1
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    • pp.67-71
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    • 2013
  • Porous $Al_2O_3$ dispersed with nano-sized Cu was fabricated by freeze-drying process and solution chemistry method using Cu-nitrate. To prepare porous $Al_2O_3$, camphene was used as the sublimable vehicle. Camphene slurries with $Al_2O_3$ content of 10 vol% were prepared by milling at $50^{\circ}C$ with a small amount of oligomeric polyester dispersant. Freezing of the slurry was done in a Teflon cylinder attached to a copper bottom plate cooled to $-25^{\circ}C$ while unidirectionally controlling the growth direction of the camphene. Pores were subsequently generated by sublimation of the camphene during drying in air for 48 h. The green body was sintered in a furnace at $1400^{\circ}C$ for 1 h. Cu particles were dispersed in porous $Al_2O_3$ by calcination and hydrogen reduction of Cu-nitrate. The sintered samples showed large pores with sizes of about $150{\mu}m$; these pores were aligned parallel to the camphene growth direction. Also, the internal walls of the large pores had relatively small pores due to the traces of camphene left between the concentrated $Al_2O_3$ particles on the internal wall. EDS analysis revealed that the Cu particles were mainly dispersed on the surfaces of the large pores. These results strongly suggest that porous $Al_2O_3$ with Cu dispersion can be successfully fabricated by freeze-drying and solution chemistry routes.

A Study on Heat Transfer Characteristics of a Closed Two-Phase Thermosyphon with a Low Tilt Angle (낮은 경사각을 갖는 밀폐형 2상 열사이폰의 열전달 특성에 관한 연구)

  • 김철주;강환국;김윤철
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.8 no.1
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    • pp.1-12
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    • 1996
  • In lots of application to heat exchanger systems, closed two-phase thermosyphons are tilted from a horizontal. If the tilt angle, especially, is less than 30$^{\circ}$, the operational performances of thermosyphon are highly dependent on tilt angle. The present study was conducted to better understand such operational behaviors as mech-anni는 of phase change, and flow patterns inside a tilted thermosyphon. For experiment, an ethanol thermosyphon with a 35% of fill charge rate was designed and manufactured, using a copper tube with a diameter 19mm and a length 1500mm. Through a series of test, the tilt angle was kept constant at each of 4 different values in the range 10~25deg. and the heat supply to the evaporator was stepwisely increased up to 30㎾/$m^2$. When a steady state was established to the thermosyphon for each step of thermal loads, the wall temperature distribution and vapor temperature at the condenser were measured. The wall temperature distributions demonstrated a formation of dry patch in the top end zone of the evaporator, with a values of temperature 20~4$0^{\circ}C$ higher than the wetted surface for a moderate heat flux q≒20㎾/$m^2$. Inspite of the presence of hot dry patch, however, the mean values of boiling heat transfer coefficient at the evaporator wall were still in a good agreement with those predicted by Rohsenow's formula, which was based on nucleate boiling. For the condenser, the wall temperatures were practically uniform, and the measured values of condensation heat transfer coefficient were 1.7 times higher than the predicted values obtained from Nusselt's film condensation theory on tilted plate. Using those two expressions, a correlation was formulated as a function of heat flux and tilt angle, to determine the total thermal resistance of a tilted thermosyphon. The correlation formula showed a good agreement with the experimental data within 20%.

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Studies on the Sanitation of Potable Water in Farm Areas (목장지역 음용수의 위생학적 조사연구)

  • 박석기;이강문;김성원;임봉택;박성배;이용욱
    • Journal of Environmental Health Sciences
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    • v.19 no.1
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    • pp.44-50
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    • 1993
  • In order to investigate the hygienic conditions of potable water in farm area, we examined the hygienic bacteriological and chemical tests of the 159 waters in the farm areas of Kwangjugun, Namyangju-gun, Yangpyung-gun Paju-gun and Hwasung-gun.The results were as follows: 1. Of the 159 waters, the average numbers of standard plate count and coliform were 920 $\pm$ 250ml and 450 $\pm$ 380/100 ml, respectively. The average pH was 6.74 $\pm$ 0.08, KMnO$_4$ consumption 4.18 $\pm$ 0.23 mg/l, turbidity 0.74 $\pm$ 0.08 degree, NH$_3$-N 0.07 $\pm$ 0.02 mg/l, NO$_3$-N 7.76 $\pm$ 0.48 mg/l, total hardness 101.3 $\pm$ 4.7mg/l, chlorine 18.6 $\pm$ 1.3mg/l, sulfate 12.9 $\pm$ 1.0 mg/l, lead 0.036 $\pm$ 0.003 mg/l, manganese 0.017 $\pm$ 0.003 mg/l, zinc 0.064 $\pm$ 0.005 mg/l, and copper 0.010 $\pm$ 0.001 mg/l, respectively. 2. Of the 159 waters, 84 samples (52.8%) were over 100 per ml of SPC or detected coliform per 100 ml water and 63 samples (39.6%) exceed over physicochemical limited criteria for potable water. NO$_3$-N was the primary item among excess contents of potable water in farm areas. 3. The contents of total hardness, chlorine and NO$_3$-N in Hwasung-gun were higher than those in the other regions, but the numbers of SPC and coliform in Yangpyung-gun and Namyangjugun were higher than those in the other regions. 4. The correlationships among many items were highly significant (SPC, Coliform, KMnO$_4$ consumption NH$_4$-N, NO$_3$-N, KMnO$_4$, Total hardness, Chlorine, Sulfate).

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A Study of Construction and Efficacy of Thermal Field-Flow Fractionation (열 장 흐름 분획장치의 제작과 효율성에 관한 연구)

  • Dai-Woon Lee;Wook-Hwan Heo;Jeon Sun-Joo;In-Ho Lee
    • Journal of the Korean Chemical Society
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    • v.36 no.3
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    • pp.419-427
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    • 1992
  • The performance of homemade thermal field-flow fractionation (ThFFF) and the optimization for separation are investigated in terms of retention parameters and selectivity using polystyrene standards. The ribbonlike channel was constructed by sandwiching two Mylar spacers between two highly polished copper bars which serve as channel walls. The hot bar was heated by two electrical cartridge heaters and the cold bar had holes through the entire length, allowing tap water as coolant to enter. It has been observed that the retention of polystyrenes increases as the temperature gradient increases. And the retention decreases as the cold wall temperature increases from 20 to $45^{\circ}C$. In comparison with size exclusion chromatography, ThFFF is more selective but has relatively low efficiency. It has been found that the plate height is proportional to the flow velocity and good estimates of polydispersities can be made directly from the ThFFF data.

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A Study on Metal Molding Using Line Transformation and Repetition - Using phosphor bronze wire (선의 변형과 반복을 활용한 금속조형 연구 - 인청동선을 활용하여)

  • Ko, Seung-Geun
    • Journal of Digital Convergence
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    • v.15 no.2
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    • pp.355-360
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    • 2017
  • This study, which was begun in order to create a metal molding by using lines, a basic element of design, examined various characteristics and concept of line and the beauty of lines based on previous research on the subject. The result showed that formative interpretation of lines largely depends on intentional expression by using thickness and rhythm of lines. In order to obtain a metal molding that provides both visual freedom and beauty, rather than the conventional formative expression of lines, I used red copper plate and Phosphor bronze line for creating a pattern based on transformation and repetition of lines and an artwork based on the pattern. The result was not only a creation of a plane but the senses of three-dimension, speed, and unity in the overall shape. Further research will need to be conducted regarding formative interpretation of lines and emotional and intrinsic beauty through expression of lines.

Studies on the Focusing Solar Agricultural Crop Dryer - Part1. Heat Efficiency of Aluminum-laminated Aeryl Film Solar Heater - (농산물(農産物) 건조용(乾燥用) 곡면집광식(曲面集光式) 태양열(太陽熱) 이용(利用) 장치(裝置)에 관한 연구(硏究) - 제1보(第1報). 알루미늄-아크릴 필림을 이용(利用)한 태양열(太陽熱) 집열장치(集熱裝置)의 열이용(熱利用) 효율(?率) -)

  • Chun, Jae-Kun;Mok, Chul-Kyoon;Kim, Hyun-Uk
    • Korean Journal of Food Science and Technology
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    • v.11 no.1
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    • pp.8-12
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    • 1979
  • A cylindrical solar energy focusing collector constructed using aluminum-laminated film plastered on the acrylic plate and examined its performances under the Korean local weather conditions. The reflector surface of this collector· evidenced the reflectivity of 66.1%,which was satisfactory value that could be applicable to the solar collector for its low price and at·availability. Collector efficiency measured at the heat exchanger fluid in absorber-copper pipe black colored was 73% and the resulting natural convection of the heat transfer media (water) was recorded up to 2.82 cm/sec. The overall efficiency of the solar heater in operation was 28.6% and it was correlated with the solar energy input and the temperature elevation difference gained.

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Synthesis of Aligned Porous Sn by Freeze-Drying of Tin Chloride/camphene Slurry (염화주석/camphene 슬러리의 동결건조에 의한 방향성 기공구조의 Sn 다공체 제조)

  • Bang, Su-Ryong;Oh, Sung-Tag
    • Korean Journal of Materials Research
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    • v.25 no.1
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    • pp.27-31
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    • 2015
  • This paper proposes a novel way of fabricating aligned porous Sn by freeze-drying of camphene slurry with stannic oxide ($SnO_2$) coated Sn powders. The $SnO_2$ coated Sn powders were prepared by surface oxidation of the initial and ball-milled Sn powders, as well as heat treatment of tin chloride coated Cu powders. Camphene slurries with 10 vol% solid powders were prepared by mixing at $50^{\circ}C$ with a small amount of oligomeric polyester dispersant. Freezing the slurry was done in a Teflon cylinder attached to a copper bottom plate cooled at $-25^{\circ}C$. Improved dispersion stability of camphene slurry and the homogeneous frozen body was achieved using the oxidized Sn powder at $670^{\circ}C$ in air after ball milling. The porous Sn specimen, prepared by freeze-drying of the camphene slurry with oxidized Sn powder from the heat-treated Sn/tin chloride mixture and sintering at $1100^{\circ}C$ for 1 h in a hydrogen atmosphere, showed large pores of about $200{\mu}m$, which were aligned parallel to the camphene growth direction, and small pores in their internal walls. However, $100{\mu}m$ spherical particles were observed in the bottom part of the specimen due to the melting of the Sn powder during sintering of the green compact.

Microwave Dielectric Properties of $\textrm{BaCo}_{x}\textrm{Ti}_{x}\textrm{Fe}_{12-2x}\textrm{O}_{19}$($1.0\leq\textrm{x}\leq5.0$) Materials ($\textrm{BaCo}_{x}\textrm{Ti}_{x}\textrm{Fe}_{12-2x}\textrm{O}_{19}$($1.0\leq\textrm{x}\leq5.0$)재료의 Microwave 유전특성)

  • Kim, Chan-Uk;Jo, Nam-Ung
    • Korean Journal of Materials Research
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    • v.8 no.8
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    • pp.775-779
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    • 1998
  • The resonant frequency fo and unloaded quality factor Qu of CoTi-substituted Barium ferrites($\textrm{BaCo}_{x}\textrm{Ti}_{x}\textrm{Fe}_{12-2x}\textrm{O}_{19}$, $1.0\leq\textrm{x}\leq5.0$) were measured at frequencies between 5 to 10GHz using the paralleled copper-plate wave guide method. The measurements showed that the permittivities of CoTi-substituted Barium ferrites(CoTi-BF) increased from 14.7 to 23.4 with the contents of CoTi, x, and the loss tangents had values of $\textrm{10}^{-3}$ order. From these results, CoTi-BF are considered to be very promising materials in microwave devices such as dielctric resonator antennas.

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Electro-chemical properties of $Li_{2}O=P_{2}O_{5}-V_{2}O_{5}$ Glass-ceramics for Cathode Materials (정극재료용 $Li_{2}O=P_{2}O_{5}-V_{2}O_{5}$ 계 결정화 유리의 전기화학적 특성)

  • 손명모;이헌수;구할본;김윤선
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.11a
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    • pp.295-298
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    • 2000
  • Vanadate glasses in the Li$_2$O-P$_2$O$_{5}$-V$_2$O$_{5}$ system containing 10~20mo1% glass former, P$_2$O$_{5}$ were prepared by melting the batch in pt. crucible followed by quenching on the copper plate. We found that Li$_2$O-P$_2$O$_{5}$-V$_2$O$_{5}$ g1ass-ceramics obtained from crystallization of glass showed significantly higher capacity and longer cycle life than Li$_2$O-P$_2$O$_{5}$-V$_2$O$_{5}$ g1ass. In the present paper, we describe electro-chemical properties during crystallization process and find the best crystallization condition of Li$_2$O-P$_2$O$_{5}$-V$_2$O$_{5}$ g1ass as cathod material. Li$_2$O-P$_2$O$_{5}$-V$_2$O$_{5}$ glass-ceramics shows superior rechargeable capacity of 220 mAh/g in the cycling between 2.0 and 3.9V. between 2.0 and 3.9V.

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Focusing effect of a Metallic Layer according to the Cooling Condition and Height in a Severe Accident (중대사고시 금속용융물층의 냉각 조건과 높이가 열속 집중 현상에 미치는 영향)

  • Moon, Je-Young;Chung, Bum-Jin
    • Journal of Energy Engineering
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    • v.24 no.1
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    • pp.78-87
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    • 2015
  • Focusing effect of a metallic layer in a severe accident depending on the aspect ratios and cooling conditions of top plate and side wall was investigated. Experiments were carried out for Rayleigh numbers and aspect ratio in the range of $8.49{\times}10^7{\sim}5.43{\times}10^9$, 0.135~0.541 respectively. In order to achieve high Rayleigh numbers, the heat transfer experiments were replaced by mass transfer experiments based on the heat and mass transfer analogy. A sulfuric acid-copper sulfate ($H_2SO4-CuSO_4$) electroplating system was adopted as the mass transfer system. The experimental results agreed well with the Rayleigh-Benard natural convection correlations of Dropkin and Somerscales and Globe and Dropkin. When compared with the standard Rayleigh-Benard problem, the cooling by the side wall is even higher than the top. For a shorter height, the interaction between the heated and cooled plumes increases due to decrease of the height. Thus, the heat transfer increases.