• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2001.10a
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• pp.138-141
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• 2001

The evolution of lectures and microstructure during the warm-rolling and subsequent annealing in aluminum 3004 alloy sheets was investigated by employing X-ray texture measurements and microstructure observations. Whereas the typical $\beta$-fiber orientations with the strong Bs-orientation $\{112\}<110>$ formed in the normally cold-rolled specimen, the warm-rolling at $250^{\circ}C$ led to the development of a strong through thickness texture gradient which was characterized by shear texture at the surface layer and rolling textures at the center layer After warm rolling, ultra-fine grains formed in the thickness layer with shear texture components. Upon recrystallization annealing, the $\{001\}<100>$ Cube-texture developed at the expense of normal rolling texture components the rise to the formation of corase recrystallized grains. However, in the layer with shear texture components the continuous recrystallization took place and the fine grain size persisted even after recrystallization annealing.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2002.05a
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• pp.184-186
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• 2002

The evolution of texture and microstructure during warm rolling and subsequent annealing in aluminium 3004 alloy sheet was investigated by X-ray texture measurements and microstructure observations. Warm rolling at 250$^{\circ}C$ led to the development of strong through thickness texture gradients with shear textures at the surface layer and a regular rolling texture in the center of the sheets. FEM simulations indicated that these texture gradients are caused by pronounced strain gradients throughout the sheet thickness. Upon recrystallization annealing, in the sheet center the characteristic cube-recrystallization texture developed, while in the surface layers with a pronounced shear texture continuous recrystallization took place which led to the formation of a very fine grained microstructure. It is concluded that the very complex strain history in the near-surface layers together with the resulting high work-hardening rate gave rise to the formation of the ultra-fine grains with an average size smaller than 2$\mu\textrm{m}$.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.42-45
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• 2007

Recrystallization behavior during ingot-breakdown process of Alloy 718 was investigated with finite element analysis and experimental approaches. In order to analyze microstructural changes during the cogging process of an Alloy 718 ingot, the side-pressing and heat treatment tests were performed at different temperatures and ram speed. From the side-pressing and heat treatment test results, it was found that microstructural changes during hot forging of Alloy 718 ingot greatly influenced on a close interaction between dynamic and static-recrystallization behaviors. A recrystallization model of Alloy 718 was used to predict the complex microstructural variation during continuous heating and forging processes of the cogging, and the predicted grain size and its distribution were compared with the actual cogged Alloy 718 billet.

• Journal of the Korean Society for Heat Treatment
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• v.13 no.5
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• pp.346-354
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• 2000

Effect of Nb addition on the phase transformation behavior was studied through continuous cooling transformation tests after reheating(reheating CCT) and deforming(deforming CCT) the 0.07%C-1.3%Mn-0.015%Ti-(0~0.08)% Nb steels. Transformation temperatures for deforming CCT were lower than those for reheating CCT, and the critical cooling rate for bainite transformation during deforming CCT was lower than that during reheating CCT. These enhanced hardenability for deforming CCT was considered to come from the sufficient solid solution of Nb in austenite during high temperature reheating before deformation. With Nb addition, the phase transformation temperature decreased, the bainite formation was enhanced, and the hardness of steel increased. Furthermore, these phenomena were more remarkable for deforming CCT than for reheating CCT. From the results, Nb-Ti bearing low carbon steel was considered to be a very favorable alloy system with good strength/toughness balance by recrystallization control rolling process.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2000.04a
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• pp.179-182
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• 2000

The dynamic softening behavior of type 430 ferritic stainless steel could be characterized by the hot torsion test in the temperature range of 900-110$0^{\circ}C$ and the strain rate range of 0.05-5/sec. It is found that the continuous dynamic recrystallization (CDRX) was a major dynamic softening mechanism. The effects of process variables strain ($\varepsilon$) stain rate($\varepsilon$)and temperature (T) on CDRX could be individually established from the analysis of flow stress curves and microstructure. The effect of CDRX individually established from the analysis of flow stress curves and microstructure. The effect of CDRX increased with increasing strain rate and decreasing temperature in continuous deformation. The multipass deformation processes were performed with 10 pass deformations. The CDRX effect occurred in multipass deformatioon. The grain refinement could be achieved from multipass deformation The grain refinement increased with increasing strain rate and decreasing temperature. Also the CDRX in multipass deformation was affected by interpass time and pass strain. The total strain was to be found key parameter to occur CDRX.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.03b
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• pp.135-139
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• 1999

The static softening behavior of AISI 4140 could be characterized by the hot torsion test in the temperature ranges of 10$0^{\circ}C$~120$0^{\circ}C$ and strain rate ranges of 0.05/sec~5/sec. Deformation efficiency which was based on dynamic materials model was calculated from flow stress curves obtained continuous deformation. Interrupted deformation was performed with 2 pass deformation in the pass strain ranges of 0.25{{{{ epsilon _p}}}} ~3{{{{ epsilon _p}}}} and interrupted time ranges of 0.5~100sec. The dependences of process variables pass strain ({{{{ epsilon _i}}}}) stain rate ({{{{ {. } atop {$\varepsilon$ } }}}}) temperature (T) and interpass time ({{{{ {t }_{i } }}}}) on static recrystallization (SRX) and metadynamic recrystallization .(MDRX) could be indicidually predicted from the modified Avrami's equations. Comparison of the softening kinetics between MDRX and SRX showed that the rate of MDRX was more rapid than that of SRX for the same deformation variables. Controlled multipass deformations were performed using deformation efficiency static and metadynamic recrystallization of AISI 4140.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2001.10a
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• pp.293-296
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• 2001

The dynamic softening mechanisms of AISI 316, AISI 304 and AISI 430 stainless steels were studied with torsion test in the temperature range of $900 - 1200^{\circ}C$ and the strain rate range of $5.0x10^{-2}-5.0x10^0/sec$. The austenitic stainless steels, such as AISI 316 and AISI 304 were softened by dynamic recrystallization (DRX) during hot deformation. Also, the evolutions of flow stress and microstructure of AISI 430 ferritic stainless steel show the characteristics of continuous dynamic recrystallization (CDRX). To establish the quantitative equations for DRX of AISI 316 stainless steel, the evolution of flow stress curve with strain was analyzed. The critical strain (${\varepsilon}_c$) and strain for maximum softening rate (${\varepsilon}^{*}$) could be confirmed by the analysis of work hardening rate ($d{\sigma}/d{\varepsilon}={\theta}$). The volume fraction of dynamic recrystallization ($X_{DRX}$) as a function of processing variables, such as strain rate ( $\varepsilon$ ), temperature (T), and strain ( $\varepsilon$ ) were established using the ${\epsilon}_c$ and ${\varepsilon}^{*}$. For the exact prediction the ${\varepsilon}_c,\;{\varepsilon}^{*}$ and Avrami' exponent (m') were quantitatively expressed by dimensionless parameter, Z/A, respectively. It was found that the calculated results were agreed with the experimental data for the steels at my deformation conditions. Also, we can reasonably conclude that the DRX, CDRX and grain refinement of stainless steels can be achieved by large strain deformation at high Z parameter condition.

• Journal of the Korean Ceramic Society
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• v.28 no.10
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• pp.751-756
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• 1991

Continuous microstructural changes on heating of hardened paste prepared from primary clinker of CA2 composition was studied. On heating period, several characteristic shrinkages and microstructural changes took place in the specimen due to the dehydration and recrystallization of calcium aluminates without regard to the accelerative shrinkage resulted from sintering. Though micropores formed by dehydration decreased with recrystallization of calcium aluminates, micropores formed by plate-type gibbsite in the hydrates were maintained up to the temperature at which CA2 becomes main phase and had influence to the microstructure of the final clinker.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.11
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• pp.1844-1853
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• 2001

In the present investigation, it was attempted to design the rolling pass schedule fur a clean steel of 0.1C-1.5Mn-0.25Si with the objective of the austenite grain refinement. As the method of approach, a coupled mathematical modeling technique was proposed which consists of a recrystallization model and a flow stress modes. The validity of the coupled model was examined through comparison with results of continuous and discontinuous compression tests at various temperatures, strains and strain rates. The coupled model was incorporated with the finite element method to set up a systematic design methodology far the rolling path schedule for austenite grain refinement. Two path schedules were obtained and discussed in the paper with regard to rolling path time, average grain size, grain size deviation in thickness, etc.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1996.03b
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• pp.48-54
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• 1996

The continuous deformation , multistage deformation and stress relaxation were carried out to investigate the strain induced procipitation by torsion tests in the range of 1000∼800$^{\circ}C$, 0.05/sec∼5/sec for V-microalloyed steel. The starting temperature and time for the initiation of precipitation were determined by stress relaxation tests and the distribution of percipitates increased at higher strain rate and the mean size of precipitates was found to be about 50nm. The precipitation starting time decreased with increasing strain rate from 0.05/sec to 5 /sec and pre-strain. The effect of deformation conditions on the no-recrystallization temperature(Tnr) was determined in the multistage deformation with declining temerature. The Tnr decreased with increasing strain and strain rae. In the controlled rolling, grain refinement and precpitation hardening effects could be achieved by the alternative large pass strain at the latter half pass stage under the condition of low temperature and high strain rate.