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A STUDY ON THE BONDING BEHAVIOR OF PALLADIUM-BASED ALLOYS FOR CERAMO-MENTAL RESTORATION (도재 소부용 팔라디움계 합금의 도재 결합양상에 관한 연구)

  • Chang, Hoon;Lim, Ho-Nam;Choi, Boo-Byung
    • The Journal of Korean Academy of Prosthodontics
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    • v.27 no.1
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    • pp.143-179
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    • 1989
  • To observe the bonding behavior of palladium-based alloys to porcelain; 1. Pd-Co binary alloy with the higher cobalt content, 2. Pd-Co binary alloy with the lower cobalt content, 3. Pd-Ag-Sn ternary alloy, 4. Pd-Ag binary alloy, 5. Pd-Cu-Au ternary alloy and 6. Pd-Cu binary alloy were made as 6 groups of experimental alloys. Each group of alloy was divided into 4 sub-groups such as one sub-group that was not degassed and three sub-groups that degassed for 5 minutes, 10 minutes and 15 minutes. On each specimen, weight changes after degassing, morphological changes of oxide layer by changing the degassing time, compositional changes at metal-ceramic interface and bond strength of metal-ceramic measured with planar shear test were observed and compared. The results of the present study allow the following conclusions to be drawn: 1. The alloy showing the greatest bond strength was Pd-Cu alloy without gold and bond strength was decreased by alloying gold to them. 2. Although Pd-Co alloy showed the most prominent oxidation behavior, bond strength of them to porcelain was not greatly high by the formation of porosities at metal-ceramic interfaces. 3. Likewise tin, cobalt formed the peaks on line profiles at metal-ceramic interface, however copper did not exhibit such peaks on line profiles. 4. Mainly, oxide layer on Pd-Co alloy was composed with cobalt, and for Pd-Co alloy with higher cobalt content the rise of bond strength was not significant by increased degassing time. 5. On Pd-Ag alloy not containing tin, during degassing for 15 minutes silver content was increased at metal-ceramic interface. 6. As an oxidized element, tin formed the oxide layers that widen their area by increasing the degassing time, while cobalt and copper showed the morphological changes of particle or crystal on oxide layer.

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The Characteristics of Compound Layers Formed during Plasma Nitrocarburising in Pure Iron (플라즈마 침질탄화처리된 순철의 화합물층 특성)

  • Cho, H.S.;Lee, S.Y.;Bell, T.
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.3
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    • pp.143-150
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    • 2000
  • Ferritic plasma nitrocarburising was performed on pure iron using a modified DC plasma unit. This investigation was carried out with various gas compositions which consisted of nitrogen, hydrogen and carbon monoxide gases, and various gas pressures for 3 hours at $570^{\circ}C$. After treatment, the different cooling rates(slow cooling and fast cooling) were used to investigate its effect on the structure of the compound layer. The ${\varepsilon}$ phase occupied the outer part of the compound layer and ${\gamma}^{\prime}$ phase existed between the ${\varepsilon}$ phase and the diffusion zone. The gas composition of the atmosphere influenced the constitution of the compound layer produced, i.e. high nitrogen contents were essential for the production of ${\varepsilon}$ phase compound layer. It was found that with increasing carbon content in the gas mixture the compound layer thickness increased up to 10%. In the gas pressure around 3 mbar, the compound layer characteristics were slightly effected by gas pressure. However, in the low gas pressure and high gas pressure, the compound layer characteristics were significantly changed. The constitution of the compound layer was altered by varying the cooling rate. A large amount of ${\gamma}^{\prime}$ phase was transformed from the ${\varepsilon}$ phase during slow cooling.

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Properties and Provenance of Loess-paleosol Sequence at the Daebo Granite Area of Buan, Jeonbuk Province, South Korea (전북 부안 화강암지역 뢰스-고토양 연속층의 퇴적물 특성과 기원지)

  • Park, Chung-Sun;Hwang, Sang-Ill;Yoon, Soon-Ock
    • Journal of the Korean Geographical Society
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    • v.42 no.6
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    • pp.898-913
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    • 2007
  • We examined soil properties and provenance of loess-paleosol sequences at the Daebo Granite area of Buan, Jeonbuk Province, South Korea. The section consists of the surface layer, Layer 1(paleosol), Layer 2(loess), Layer 3(paleosol), Layer 4(loess), and Layer 5(paleosol), from top to bottom and thickness of the exposed section is approximately 280cm. The magnetic susceptibility values show the distinct variations between the loess- and the paleosol layer. Even though pH, ORP, water content, and soil hardness do not display the obvious differences in the section, the organic content indicates the variation similar to those of the magnetic susceptibility. In the respect of the soil colors measured under 3 conditions, although the variations of the wet soil color exceedingly reflect the difference of the layers, these variations are obscure in some points in the section due to the characteristics of the Munsell color system. Based on the geomorphological properties, sedimentary structure, the difference of the major element composition and the condrite-normalized rare earth element(REE) patterns showing the clear difference from the adjacent bedrocks and stream sediments and the similarity to those of the Chinese Loess Plateau, it is suggested that the section was formed by the material originated from the Chinese Loess Plateau and peripheral areas. However, because the material experienced the alteration after sedimentation under the environment of the sediment area, it has the properties different from the material in the provenance areas. This phenomenon may result in the climatic condition of Korea, especially in precipitation.

Three-Dimensional Analysis on Drying Process of a Cylindrical Thin Film Layer of Sludge under Uniform Heating (일정온도로 가열되는 원통 형상 슬러지 박막의 건조에 대한 3차원 해석)

  • Lee, Kong-Hoon;Kim, Ook-Joong
    • Proceedings of the SAREK Conference
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    • 2009.06a
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    • pp.1326-1331
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    • 2009
  • Drying process in the cylindrical thin film layer of sludge with the thickness less than a few millimeters has been investigated. Thin film drying is specially designed and used to dry the viscous materials like sewage sludge. The thin film layer of sludge is dried on the metallic cylindrical surface through which thermal energy is supplied to the layer during drying. The wall temperature is assumed to be constant during drying in the present study for the simplification. In order to solve the equations, the mass transfer rate on the drying surface should be determined. The mass flux of evaporated water vapor on the surface is estimated with the formulation given in the literature. The effect of some physical parameters on drying has been examined to figure out the drying characteristics of the sludge layer.

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Determination of Thermal Conductivity and Numerical Analysis of Al-Cr-N-O Composites Layer Formed by Hydro-thermal Process (수열합성된 Al-Cr-N-O계 도포층의 열전도 측정과 수학적 해석)

  • Kim, Ma-Ro;Yang, So-Eun;Lee, Jong-Jae;Kim, Byeong-Du;Choe, Yong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2014.11a
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    • pp.215-215
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    • 2014
  • Composites layer of Al-Cr-Ni-O system was prepared on a steel plate by hydro-thermal process at $700^{\circ}C$ for 12 hours, which phase identification and thermal conductivity were determined. The composites layer consisted of aluminum nitride, alumina, chromium carbide and aluminium, which density was $3.7kg/m^3$. The thermal conductivity of the coating layer determined by thermal data acquisition system was about 98.0 W/m/ which depended on the AlN content. Numerical modelling of the heat transfer behavior of the coating layer was well agreement with the empirical data.

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Analysis on the Drying Characteristics for the Drying Process of a Thin Film Layer of Sludge (슬러지 박막의 건조과정에 대한 건조 특성 해석)

  • Lee, Kong-Hoon;Kim, Ook-Joong
    • Proceedings of the SAREK Conference
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    • 2008.06a
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    • pp.1128-1133
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    • 2008
  • Drying process in the thin film layer of sludge with the thickness less than a few millimeters has been investigated using the simple one-dimensional model. Thin film drying is usually used to dry the viscous materials like sewage sludge. The thin film layer of sludge is dried on the metallic surface through which thermal energy is supplied to the layer during drying. In order to solve the equations, the mass transfer rate on the drying surface should be determined. The mass flux of evaporated water vapor on the surface is estimated with the formulation given in the literature. The effect of heating temperature, film thickness, and air velocity on drying has been examined to figure out the drying characteristics of the sludge layer.

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Content production method based on OLED film and dual layer display system

  • Lee, Sang-Hyun
    • International Journal of Internet, Broadcasting and Communication
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    • v.10 no.3
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    • pp.81-87
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    • 2018
  • It is common practice to display high-quality video images on the large display among the methods of developing tourist attractions and culture in the region as experience contents differentiation is required. This paper combines the local attractions with the OLED dual layer display system and the extended image implementation and augmented interaction technique to give the experiencer a realistic space, such as directing to new experiences and beautiful sights. In this paper, we added UI layer to additional layers of images to enable users to experience sightseeing information, weather, maps, accommodation, festivals and photo materials with images. It is implemented to add fun through interlocking. We also developed transparent OLED and dual layer panel and 3-channel multi-image playback technique.

Study on Gaseous Nitrocarburizing Treatment (가스침질탄화법(浸窒炭化法)에 관한 연구(硏究))

  • Lee, S.Y.;Bell, T.
    • Journal of the Korean Society for Heat Treatment
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    • v.1 no.1
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    • pp.8-12
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    • 1988
  • This study has been carried out to evaluate gaseous nitrocarburizing treatment undertaken for pure iron at $570^{\circ}C$ in an atmosphere containing 50% endothermic gas, generated from natural gas, and 50% ammonia. The results obtained from the experiment are as follows ; 1) The microstructure of gaseous nitrocarburized pure iron consists of the compound layer on the surface and the diffusion zone beneath it. The compound layer progresses uniformly into ferrite with a thickness of $20{\mu}$ obtained after treating for 3 hours. 2) Chemical analysis has shown that the compound layer has a C/N ratio of 0.19 and that the average combined interstitial content of the compound layer is about 30 atomic percent, which is close to the lower limit of the ${\varepsilon}$-carbonitride phase field in Fe-C-N phase diagram. 3) X-ray diffraction analysis has revealed that the compound layer consists mainly of the c.p.h. phase, ${\varepsilon}-Fe_3$(C.N) and a small amount of $Fe_4N$ and traces of ferrite are also present in the compound layer. 4) The microhardness of the compound layer is about 600 V.H.N and shows a relatively sharp fall-off at the compound layer/diffusion zome interface. 5) The average actual degree of ammonia dissociation is calculated to be 27% for a gaseous nitrocarburizing treatment carried out at $570^{\circ}C$.

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The Study on Experimental Method of Smoldering Ground Fire in Forest Fire (뒷불 특성에 관한 실험방법 연구)

  • Kim, Dong-Hyun;Kim, Jang-Hwan;Kim, Eung-Sik
    • Fire Science and Engineering
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    • v.24 no.6
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    • pp.1-6
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    • 2010
  • A smoldering ground fire can be a probable cause of reignition of surface fire when transmitted from Fermentation layer to Humus layer with temperature higher than that of ignition. Purpose of this paper is to identify experimental methodology on the potential risk of a smoldering ground fire, which is similar to the real surface fuel bed, and its combustion characteristics. The fuel model designed in this study is composed of 3 layers such as Litter layer, Fermentation layer and Humus layer and 8 Thermocouples are set through 3 layer at each boundary and in between to detect the temperature change and duration of smoldering and propagation velocity. As a result, it was observed that ignition conditions in the boundary between L layer and F layer determined transmission and non-transmisstion to F-H layer. In addition, range of critical humidity at which a smoldering ground fire was transmitted in a material layer was 33~44% and when temperature exceeds $350^{\circ}C$, likelihood of transmission of a smoldering ground fire was high. In the research, the experimental model for multi-layer smoldering ground fire is suggested and information about propagation of smoldering fire, possibility of reignition according to moisture content, propagation velocity and temperature change are obtained, Also, the built-up methods were established to help analyze basic characteristics of smoldering ground fire.

Effects of Sodium Tripolyphosphate and Canola Oil on the Quality of Chicken Nuggets Made from Old Layer Meat (Sodium Tripolyphosphate와 카놀라유 첨가가 산란 성계육으로 제조한 치킨너깃의 품질에 미치는 영향)

  • Kim, Juntae;Utama, Dicky Tri;Jeong, Hae Seong;An, Byoung Ki;Lee, Sung Ki
    • Korean Journal of Poultry Science
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    • v.45 no.2
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    • pp.89-96
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    • 2018
  • This study aimed to investigate the effect of adding sodium tripolyphosphate (STPP) and canola oil on the quality traits of chicken nuggets. The nuggets were prepared from the breast meat of 75-week-old Hy-line old layer. Experiment 1 was conducted to evaluate the effect of adding different levels (0%, 0.1%, 0.2%, and 0.3%) of STPP addition (w/w). It was found that moisture content and cooking yield were significantly increased by the addition of STPP (P<0.05). STPP addition significantly increased hardness and Warner-Bratzler shear force (WBSF) value (P<0.05). Thereafter, STPP addition was fixed at 0.3% (w/w) and another experiment was performed to investigate the effect of canola oil addition (w/w) at different levels (5%, 10%, and 15%). There was no difference in pH depending on canola oil content. However, emulsion capacity, fat loss, and total water loss increased with the increase in canola oil content (P<0.05). Hardness and WBSF value showed significant decreases as canola oil content increased (P<0.05). Texture and overall acceptance were significantly increased with the increase in canola oil content in a test based sensory evaluation. In conclusion, adding 0.3% STPP and 15% canola oil to chicken nuggets made from the old layer could produce a product with an acceptable quality.