• 제목/요약/키워드: Content Standard

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담배 중 멘톨 분석에 대한 불확도 측정 (Uncertainty in Determination of Menthol from Mentholated Cigarette)

  • 장기철;이운철;백순옥;한상빈
    • 한국연초학회지
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    • 제22권1호
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    • pp.91-98
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    • 2000
  • This study was carried out to evaluate the uncertainty in the analysis of menthol content from the mentholated cigarette. Menthol in the sample cigarette was extracted with methanol containing an anethole as an internal standard, and then analyzed by gas chromatography. As the sources of uncertainty associated with the analysis of menthol, were the following points tested, such as the weighing of sample, the preparation of extracting solution, the pipetting of extracting solution into the sample, the preparation of standard solution, the precision of GC injections for standard & sample solution, the GC response factor of standard solution, the reproducibility of menthol analysis, and the determination of water content in tobacco, etc. For calculating the uncertainties, type A of uncertainty was evaluated by the statistical analysis of a series of observation, and type B by the information based on supplier's catalogue and/or certificated of calibration. Sources of uncertainty were subsequently included and mathematically combined with the uncertainty arising from the assessment of accuracy to provide the overall uncertainty. It was shown that the main source of uncertainty came from the errors in the reproducibility of menthol and water determination, the purity of menthol reference material in the preparation of standard solution, and the precision of GC injections for sample solution. The errors in sample weighing and volume measurement contributed relatively little to the overall uncertainty. The expanded uncertainty in the mentholated cigarettes, Korean and American brand, at 0.95 level of statistical confidence was $\pm$0.06 and $\pm$0.07 mg/g for a menthol content of 1.89 and 2.32 mg/g, respectively.

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Alcohol과 쌀 곰팡이의 Toxicity가 간(肝)의 지방(脂肪) 축적(蓄積)에 미치는 영향(影響) (Effects of Alcohol Intoxication and Moldy Rice Consumption on the Liver Lipid Content in Rat)

  • 정진은;김숙희
    • Journal of Nutrition and Health
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    • 제6권4호
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    • pp.37-53
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    • 1973
  • For the elucidation of the metabolic effects due to alcoholic drink and moldy rice intake author designed two experiments as follows. In the first experiment, sixty male and female rats, divided into six groups, 10 rats each in both sexes, were given 7.5% sucrose-30% alcohol solution (Jinro-Soju) and diets varied of fat content (2%, 7%, 30% of diet) and protein quality (casein, bean, anchovy) for 6 weeks. In the Second experiment, six groups of rats, 10 male rats each, were fed the diets containing zero, 5%, 10%, 25%, 50%, and 100% moldy rice contaminated Penicillium Islandicum and the experimental periods were 4 weeks and 6 weeks. The results of these studies due to the toxicity of alcohol consumption and moldy rice ingestion of the fatty liver production and the other effects are as follows. 1. Food intake of alcohol consumed groups decreased to 50%-70% of that of standard group. In the second study, there was no significant differences on food intake due to the different contents of moldy rice and experimental period. 2. On the view paint of body weight gain, the body weight of alcohol consumed groups gained much less than that of standard group, because food consumption was decreased due to alcohol ingestion. 3. In comparison of F.E.R. and P.E.R. between standard and experimental groups, there was no significant differences in this study. 4. As a matter of fact, there was no significance on the nitrogen balance in both studies. 5. From the result of hematology, R.B.C. counts, W.B.C. counts, hemoglobin, and hematocrit showed normal values in all groups including in this study. So we might conclude that the toxicity of alcohol and moldy rice do not effect significantly on blood picture. 6. The larger organs shrank on the range of 20%-70% of that against standard group in this study. The major reason for the shrinkage of organs might be account of decreased food consumption due to alcoholic drink. There was no great changes on the organ weight due to the ingestion of moldy rice. 7. The nitrogen content in various organs in both experiments was revealed at the normal level for the worst condition in terms of the least food intake. In other word, it was noteworthy that the concentration of nitrogen in various organs was kept at the normal ratio as standard groups under the circumstances of this study. 8. The lipid content in the liver of rats fed alcohol and diets containing either various lipid contents or protein quality did not increase. Hepatic lipids accumulation due to the dietary fat content was observed, but there wvas no significances among the compared groups. In the second experiment, the difference of hepatic lipid content between the moldy rice groups and standard group was not showed. In addition to the result of total lipid, hepatic free cholesterol, free fatty acid, and triglyceride did not change in both studies, we might conclude that the toxicity of alcohol and moldy rice could not effect on the hepatic lipid contents. 9. There was no significant differences on the serum glucose level between alcohol groups and standard group. In the second experiment, serum glucose level increase in 6th week compared with in 4th week, but there was no significant differences.

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지리교육내용의 표준설정 방법 - 지적영역을 중심으로 - (A Study on Content Standard of Geographical Education)

  • 조성욱
    • 대한지리학회지
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    • 제37권3호
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    • pp.276-291
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    • 2002
  • 현행 교육과정의 지리교육내용은 포괄적이고 추상적으로 제시되고 있다. 또한 전체 교육의 일부분으로 설정되기 때문에, 지리교육 자체의 교육 내용 체계화를 이루기 어렵다. 본 연구에서는 현행 교육과정을 보완하고 지리교육 내용을 체계화하는 방법으로, 지리학에 기반을 둔 지리교육 내용의 표준 설정 방법을 제안한다. 지리교육의 표준 설정 방안으로 대주제, 기본 주제, 주요 표준, 표준, 상세 표준을 제시하였다. 대주제는 지리교육 전반을 통찰하는 대개념으로서 '인간과 환경의 상호작용 이해', '장소 또는 지역에 대한 이해', '인간과 장소의 상호작용 이해'의 3개를 선정하였다. 기본 주제는 '지리적 기능', '자연 환경' '인문 환경', '장소 및 지역', '인간과 장소의 상호작용'의 5개를 선정하였다. 표준은 구체적이고 측정 가능한 지리교육내용을 제시하는 단계로서 '주요 표준'표준', '상세 표준'의 3단계로 상세화했다.

저소성 실트질흙의 흙 시멘트에 관한 연구 (A Study on the Cement Mixture With Low Plasticity Silty Soil)

  • 김주범;박완순류기송김성교
    • 한국농공학회지
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    • 제17권2호
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    • pp.3778-3783
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    • 1975
  • The objective of this study is to determine an appropriate cement of soil-cement in which silty soil of salty tidal flat with low plasticity was used. Physical, chemical and mechanical tests were conducted to find out the standard properties of the soil to be used. Various cement contents used in this test were 8%, 10%, 12%, and 14%, and the compressive strength was tested after 7 days and 28 days of standard curing in the above each cement content respectively. The results obtaind are summarized as follows. 1. As the cement content was increased from 8% to 14%, Maximum dry density (M.D.D.) and optimum moisture content (O.M.C.) were not changed remarkably. 2. Density of soil-cement was directly proportional to cement content and inversely proportional to water content. 3. OMC was generally decreased in proportion to the increase of cement content. 4. Compressive stranth was directly proportional to centent and inversely proportional to water content. 5. In freezing and thawing test, maximum loss of 10% in the total Weight was found on the 8% cement mixture. and This loss was rapidly decreased to 2% when the Cement content of the mixture was more than 10%.

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융합시대의 이러닝 콘텐츠 개발용역의 표준계약서 적용 실태 분석 (An Analysis on Application Status of Standard Contract on the e-Learning Content Development Project in Era of Convergence)

  • 이주연;노규성
    • 디지털융복합연구
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    • 제13권3호
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    • pp.11-18
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    • 2015
  • 융복합 시대로 들어서면서 정부가 이러닝 콘텐츠 개발용역 표준계약서를 제정 고시 후 1년 8개월이 지났다. 그럼에도 불구하고 여전히 관련 업계에서는 부당하고 불합리한 관행이 개선되지 않고 있다는 문제 제기가 지속되어 왔다. 본 연구는 이러닝 융합 콘텐츠 개발용역 현장에서의 표준계약서 적용 실태를 설문 등을 통해 조사하고 이의 개선방안을 제언하고자 한다. 본 연구 결과, 이 표준계약서가 콘텐츠 개발용역 수발주 현장에 전혀 뿌리를 내리지 못해 실효를 거두지 못한 것으로 분석되었다. 이에 본 연구는 이러닝 콘텐츠 개발용역 표준계약서가 정부의 의도와 목적대로 수발주 현장에서 착근됨과 동시에 관행으로 정착되도록 하기 위한 대안으로 표준계약서 적용 의무화, 교육 및 홍보 실시, 모니터링 체계 도입, 인증제도 시행, 기관 및 기관장 평가시의 가점 부여 등의 정책을 제언하였다.

황색종 담배중 전알카로이드와 환원당 분석에 대한 불확도 측정 (Uncertainty of Total Alkaloids and Reducing Sugar Determination in Flue-cured Tobacco)

  • 백순옥;장기철;이운철;한상빈
    • 한국연초학회지
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    • 제23권1호
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    • pp.45-52
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    • 2001
  • This study was carried out to evaluate the uncertainty in the analysis of total alkaloids and reducing sugar content in flue-cured tobacco. The sources of uncertainty associated with the analysis of total alkaloids and reducing sugar were the weighing of sample, the preparation of extracting solution, the addition of extracting solution into the sample, the preparation of standard solution, the precision of calibration curve for standard solution, the reproducibility of analysis, and the determination of water content in tobacco, etc. For the calculating uncertainties, Type A of uncertainty was evaluated by the statistical analysis of a series of observation, and Type B by the information based on supplier’s catalogue and/or certificated of calibration. It was shown that the main source of uncertainty was caused by the calibration curve of standard solution, the reproducibility of analysis, the volume measurement of 1$m\ell$, and the purity of nicotine reference material in the preparation of standard solution. The uncertainty in the addition of extracting solution, the sample weighing, the volume measurement of 100$m\ell$, and the determination of water content of tobacco contributed relatively little to the overall uncertainty. The expanded uncertainty of total alkaloids and reducing sugar in flue-cured tobacco at 95% level of confidence was $\pm$0.12% and $\pm$0.54%, respectively.

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Determination of Protein Content in Pea by Near Infrared Spectroscopy

  • Lee, Jin-Hwan;Choung, Myoung-Gun
    • Food Science and Biotechnology
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    • 제18권1호
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    • pp.60-65
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    • 2009
  • Near infrared reflectance spectroscopy (NIRS) was used as a rapid and non-destructive method to determine the protein content in intact and ground seeds of pea (Pisum sativum L.) germplasms grown in Korea. A total of 115 samples were scanned in the reflectance mode of a scanning monochromator at intact seed and flour condition, and the reference values for the protein content was measured by auto-Kjeldahl system. In the developed ground and intact NIRS equations for analysis of protein, the most accurate equation were obtained at 2, 8, 6, 1 math treatment conditions with standard normal variate and detrend scatter correction method and entire spectrum (400-2,500 nm) by using modified partial least squares regression (n=78). External validation (n=34) of these NIRS equations showed significant correlation between reference values and NIRS estimated values based on the standard error of prediction (SEP), $R^2$, and the ratio of standard deviation of reference data to SEP. Therefore, these ground and intact NIRS equations can be applicable and reliable for determination of protein content in pea seeds, and non-destructive NIRS method could be used as a mass analysis technique for selection of high protein pea in breeding program and for quality control in food industry.

한식 메뉴 명명 기준에 대한 내용분석 (The Content Analysis of the Korean Food Menu Naming Standard)

  • 한경수;이진용
    • 한국식생활문화학회지
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    • 제26권6호
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    • pp.629-640
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    • 2011
  • This research analyzed the naming standard of Korea menu names divided into two groups, main dish and side dish. The research was conducted by contents analysis of selected literature articles and multiple-response cross tabulation analysis. The result demonstrated that the naming standard of Korea food consisted of the main ingredient name - sub ingredient name - main condiment name and main recipe. On the other hand, the menu name that is in native language or has a historical origin is exempt from this classification. Therefore, this study proposes a new standard, 'Hansik Menu Naming', to assist the food service industry and correct the names of unknown foreign dishes.

모발의 아연과 납 합량 : 학령 전 아동의 영양소 섭취 상태와 신장 및 체중과의 관계 (Hair Zinc and Lead: Relationship to Nutrient Intake and Height and Body Weight in Korean Preschool Children)

  • 박현서;신경옥
    • Journal of Nutrition and Health
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    • 제37권3호
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    • pp.193-201
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    • 2004
  • The objective was to evaluate the factors influencing on the growth of children aged 3 - 6 years by mini dietary assessment and anthropometric indices in 556 children and by analyzing mineral contents of hair from 273 children by inductively coupled plasma mass spectrometry (ICP-MS). The mean concentration of zinc (Zn) in hair was 68.9 $\pm$ 31.1 ppm and the zinc level of 91 % children was less than 60% of the reference value of 180 ppm. The mean content of lead (Pb) in hair was 1.76 $\pm$ 1.20 ppm, but only 67% of 273 children was within the reference value of 2 ppm and the lead level of 33% of children was 2 - 4 times higher than the reference value. The level of Zn was negatively correlated with Pb content (r = -0.305, p 〈 0.01). Hair Zn content, regardless of age, was significantly positively correlated with height (r = 0.214) and body weight (r = 0.159). The height of 95.3% children was belonged to the normal range of 90 - 109.9% of standard value and the body weight of 49.8% children was in the range of 90 - 109.9% of standard value. However, 8.1 % children was overweighted (110 - 119.9% of standard) and 9.4% children was obese (120 - 149.9% of standard) and 0.9% children was severe obese (〉 150%) which resulted in total 10.3% obese. Contrary to our expectation, 32.8% children was underweight (70 - 89.9% of standard) and 36% of the underweight children showed the low content of zinc (10 - 49 ppm) in hair. There was no significant correlation between dietary intake of Zn and hair Zn content. Hair Zn content was low even though children consumed greater than 75% of their requirement for zinc. Regardless of dietary intake of Zn, hair Zn level was rather negatively correlated to the content of Pb in hair. 38.8% children had an unbalanced diet which resulted in lower intake of calorie, Ca, Zn, vitamin B$_2$ compared with those consuming variety of foods. Therefore, it would be needed that new approach for nutrition education to improve eating habit having the unbalanced diet in preschool children. It might be also suggested to develop new food products to complement the nutrients of Zn, Ca, Fe as snacks or dietary supplement for Korean preschool children.

익산지역 수원지의 불소함량에 관한 조사연구 (A Study on Fluoride Content in the Reservoirs Of Iksan Region)

  • 이인규
    • 대한치과기공학회지
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    • 제20권1호
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    • pp.139-143
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    • 1998
  • This study was carried out to collect basic dates on fluoride intake from drinking water, and the apperance of mottled teeth after taking samples form 5 selected waterways from Iksan region's reservoir to the filtration plant for examination of the fluoride content. The results are as follows. 1. It indicatied that from Hoojung reservoir $2.17{\pm}0.95ppm$, Bulsan reservoir $1.93{\pm}0.23ppm$ and Yoolso reservoir $2.19{\pm}0.10ppm$. 2. Significances were found between Shinhung reservoir $2.57{\pm}1.22ppm$ and Uhwoo reservoir $0.80{\pm}0.55ppm$. 3. Except for the Uhwoo reservoir, the remaining 4 reservoir exceeded the standard fluoride content of 0.50-1.00ppm. For the residents in the region where they use natural water with fluoride content exceeding the standard 1.00ppm as their drinking water and the apperance of mottled teeth should be carried out.

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