• 제목/요약/키워드: Constant temperature bath

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MODELING AND OPTIMIZATION Of A FIXED-BED CATALYTIC REACTOR FOR PARTIAL OXIDATION OF PROPYLENE TO ACROLEIN

  • Lee, Ho-Woo;Ha, Kyoung-Su;Rhee, Hyun-Ku
    • 제어로봇시스템학회:학술대회논문집
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    • 2000.10a
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    • pp.451-451
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    • 2000
  • This study aims for the optimization of process conditions in a fixed-bed catalytic reactor system with a circulating molten salt bath, in which partial oxidation of propylene to acrolein takes place. Two-dimensional pseudo-homogeneous model is adopted with estimation of suitable parameters and its validity is corroborated by comparing simulation result with experimental data. The temperature of the molten salt and the feed composition are found to exercise significant influence on the yield of acrolein and the magnitude of hot spot. The temperature of the molten salt is usually kept constant. This study, however, suggests that the temperature of the molten salt must be axially adjusted so that the abrupt peak of hot spot should not appear near the reactor entrance. The yield of acrolein is maximized and the position and the magnitude of hot spot are optimized by the method of the iterative dynamic programming (IDP).

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A Basic Study of the Snow Melting System for the Anti-Freezing Road using the Pulsating Heat Pipe (PHP를 이용한 도로융설 시스템에 관한 기초연구)

  • Kim, J.S.;Ha, S.J.;Son, K.J.
    • Journal of Power System Engineering
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    • v.14 no.3
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    • pp.19-24
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    • 2010
  • The purpose of this study is to develop a snow melting system using the pulsating heat pipe(PHP). The experimental apparatus is consisted of a PHP, a concrete structure, a constant water thermostatic bath and a flowmeter. The experiment was performed at the outdoor air temperature of $-8^{\circ}C$ and inlet temperature of hot water of $75^{\circ}C$. PHP is the closed and non-loop type heat exchanger which is charging R-410A as an operating fluid. As experimental results, the temperature profile of vertical and horizontal orientation of concrete structure was measured with operating time. The heat flux of the snow melting was required more than 300 $W/m^2$. We confirmed that the snow melting system using the PHP was useful for anti-freezing road.

Enhancement of bent transfer in the liquid bath by ultrasound (액상용기에서 초음파에 의한 열전달촉진)

  • Kang Won-Jong;Oh Yool-Kwon
    • Proceedings of the KSME Conference
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    • 2002.08a
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    • pp.655-658
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    • 2002
  • The present paper investigated the effect of ultrasonic vibrations on the melting process of a phase-change material (PCM). Furthermore, the present study considered constant heat-flux boundary conditions unlike many of the previous researches, which had adopted constant wall-temperature conditions. Therefore in the study, modified dimensionless numbers such as Stefan and Rayleigh were adopted to represent heat transfer results. The experimental results revealed that ultrasonic vibrations accompanied the effects like agitation, acoustic streaming, cavitation, and oscillating fluid motion, accelerating the melting process as much as 2.5 times, compared with the result of natural melting (i. e., the case without ultrasonic vibration). Such effects are believed to be a prime mechanism in the overall melting process when ultrasonic vibrations were applied. Subsequently, energy could be saved by applying the ultrasonic vibrations to the natural melting In addition, various time-wise dimensionless numbers provided a conclusive evidence of the important role of the ultrasonic vibrations on the melting phenomena of the PCM.

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An Investigation of Preferred Orientation and Microhardness of Nickel-Tin and Tin-Zinc Alloy Electrodeposits on Mild Steel (연강에서의 닉켈-주석과 주석-아연합금 전착층의 우성배향와 미소경도에 관한 연구)

  • Ahn, Deog-Su;Pyun, Su-Il
    • Journal of Surface Science and Engineering
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    • v.13 no.3
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    • pp.146-154
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    • 1980
  • The effects of various electrodeposition conditions (deposition temperature and cathode current density) on preferred orientation and microhardness of electrodeposited Ni-Sn and Sn-Zn alloys were studied. At deposition temperatures from 25$^{\circ}$ to 95$^{\circ}C$ and constant cathode current density of 270 and 530 A/$m^2$ Ni-Sn and Sn-Zn were codeposited in chloride-fluoride acid and stannate-cyanide alkaline electrolyte bath respectively. Ni-Sn alloy deposited at temperatures from 25$^{\circ}$ to 35$^{\circ}C$ was composed of single phase of $Ni_3Sn_4$ with 73 wt.% Sn and the one deposited at temperatures from 45$^{\circ}$ to 95$^{\circ}C$ was made of multiphase mixture of NiSn, $Ni_3Sn_2$ and $Ni_3Sn_4$ with nearly equiatomic composition (65.5 wt.% Sn). The random orientation of thermody-namically metastable NiSn phase (hexagonal structure) predominated at deposition temperature range 25$^{\circ}$-45$^{\circ}C$, and the strong (110) preferred orientation was found at 65$^{\circ}$-85$^{\circ}C$ and then disappeared again at 95$^{\circ}C$. The microhardness of Ni-Sn deposits increased with deposition temperature up to 85$^{\circ}C$, and then decreased at constant cathode current density. The preferred orientation and the maximum microhardness were discussed in terms of lattice contractile stress which result from desorption of hydrogen atom absorbed in deposit lattice. The Sn content of Sn-Zn alloy deposits increased with deposition temperature up to 75$^{\circ}C$, and then decreased at constant cathode current density of 530 A/$m^2$. It also decreased with cathode current density up to 530 A/$m^2$, and then increased at constant deposition temperature of 25$^{\circ}C$. Sn-Zn alloy deposits were composed of two-phase mixture of ${beta}$-Sn and Zn. The preferred orientations of ${beta}$-Sn (tetragonal structure) changed with deposition temperature. The microhardness of Sn-Zn deposits decreased with deposition temperature. It also increased with cathode density up to 530 A/$m^2$, and then decreased at constant deposition temperature of 25$^{\circ}C$. The microhardness of Sn-Zn deposits was observed to be determinded more by the Sn content than by the preferred orientation.

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Evaluation of Life Span for Al2O3 Nano Tube Formed by Anodizing with Current Density

  • Lee, Seung-Jun;Kim, Seong-Jong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.148-148
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    • 2017
  • Surface modification is a type of mechanical manipulation skills to achieve extensive aims including corrosion control, exterior appearance, abrasion resistance, electrical insulation and electrical conductivity of substrate materials by generating a protective surface using electrical, physical and chemical treatment on the surface of parts made from metallic materials. Such surface modification includes plating, anodizing, chemical conversion treatment, painting, lining, coating and surface hardening; this study conducted cavitation experiment to assess improvement of durability using anodizing. In order to observe surface characteristics with applied current density, the electrolyte temperature, concentration was maintained at constant condition. To prevent hindrance of stable growth of oxide layer due to local temperature increase during the experiment, stirring was maintained at constant speed. In addition, using galvanostatic method, it was maintained at processing time of 40minutes for 10 to $30mA/cm^2$. The cavitation experiment was carried out with an ultra sonic vibratory apparatus using piezo-electric effect with modified ASTM-G32. The peak-to-peak amplitude was $30{\mu}m$ and the distance between the horn tip and specimen was 1mm. The specimen after the experiment was cleaned in an ultrasonic bath, dried in a vacuum oven for more than 24 hours, and weighed with an electric balance. The surface damage morphology was observed with 3D analysis microscope. As a result of the study, differences were observed surface hardness and anti-cavitation characteristics depending on the development of oxide film with the anodizing process time.

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Electro-deposition and Crystallization Behaviors of Cr-C and Cr-C-P Alloy Deposits Prepared by Trivalent Chromium Sulfate Bath (황화물계 3가 크롬도금욕에서 크롬-탄소 및 크롬-탄소-인 합금도금의 전착과 결정화거동)

  • Kim, Man;Kim, Dae-Young;Park, Sang-Eon;Kwon, Sik-Chul;Choi, Yong
    • Journal of Surface Science and Engineering
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    • v.37 no.2
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    • pp.80-85
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    • 2004
  • Chromium-carbon (Cr-C) and chromium-carbon-phosphorus (Cr-C-P) alloy deposits using trivalent chromium sulfate baths containing potassium formate were prepared to study their current efficiency, hardness change and phase transformations behavior with heat treatment, respectively. The current efficiencies of Cr-C and Cr-C-P alloy deposits increase with increasing current density in the range of 15-35 A/dm$^2$. Carbon content of Cr-C and phosphorous of Cr-C-P layers decreases with increasing current density, whereas, the carbon content of Cr-C-P layer is almost constant with the current density. Cr-C deposit shows crystallization at $400^{\circ}C$ and has (Cr+Cr$_{ 23}$$C_{6}$) phases at $800^{\circ}C$. Cr-C-P deposit shows crystallization at $600^{\circ}C$ and has (Cr+Cr$_{23}$ $C_{6}$$+Cr_3$P) phases at $800^{\circ}C$. The hardness of Cr-C and Cr-C-P deposits after heating treatment for one hour increase up to Hv 1640 and Hv 1540 and decrease about Hv 820 and Hv 1270 with increasing annealing temperature in the range of $400~^{\circ}C$, respectively. The hardness change with annealing is due to the order of occurring of chromium crystallization, precipitation hardening effect, softening and grain growth with temperature. Less decrease of hardness of Cr-C-P deposit after annealing above $700^{\circ}C$ is related to continuous precipitation of $Cr_{23}$ $C_{6}$ and $Cr_3$P phases which retard grain growth at the temperature.

Experimental Investigations on the Temperature Characteristics of Oscillating Heat Pipe with Various Filling Ratio

  • Jeong, Hyo-Min;Chung, Han-Shik;Lee, Kwang-Sung;Tanshen, Md.Riyad;Lee, Tae-Jin;Lee, Sin-Il
    • Journal of Power System Engineering
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    • v.17 no.6
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    • pp.47-53
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    • 2013
  • The article focuses on the Temperature characteristics inside single loop oscillating heat pipe (OHPs). In this paper, heat pipe is experimentally studied thereby providing vital information on the parameter dependency of their thermal performance. The impact depiction has been done for the variation of tube model of the device. OHPs are made of copper capillary tubes of outer diameter 6.25 mm, inner diameter 4 mm heated by constant temperature water bath cooled by ambient temperature. Using four types of OHPs of copper capillary tubes length of 1500mm and HP length 650mm inside tubes working fluid is R-22 Pressure 8 bar and mass 34g,32g,28g,16g. The results indicate a strong influence of filling ratio on the performance.

Estimation of the thermal performance on the double slab floor with supplying air (급기가 되는 이중바닥 구조체의 열 성능 평가)

  • Cha, Kwang-Seok;Park, Myung-Sig;Lee, Dae-Woo;Nam, Woo-Dong
    • Proceedings of the SAREK Conference
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    • 2006.06a
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    • pp.866-871
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    • 2006
  • Recently according to the fashion of well-being, the case study of under floor heating system type for residential space is increasing. Specially double slab floor system can make several roles as reducing the acoustic noises and also supplying fresh air through the gap. So in present study floor heating performance was examined with various location of the space in the case of floor supply air and ceiling supply air. In both cases return air went out through ceiling opening. As one of the result is that when using the heat pipe type floor heating system the temperature difference between supply and return water was $15.2^{\circ}C$, but in case of commercial type floor heating system the temperature difference was $5.3^{\circ}C$ when the supply water temperature was $50^{\circ}C$.

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Study on long-term monitoring of heat exchanger installed in the tunnel lining (터널 라이닝 내부에 설치한 열교환기의 현장모니터링 연구)

  • Lee, Chulho;Park, Moonseo;Choi, Hangseok;Sohn, Byunghu;Jeoung, Jaehyeung
    • 한국신재생에너지학회:학술대회논문집
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    • 2011.05a
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    • pp.195.1-195.1
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    • 2011
  • This paper presents an experimental study on a new potential geothermal energy source obtained from tunnel structures. An "energy textile", which is a textile-type ground heat exchanger, was fabricated between a shotcrete layer and a guided drainage geotextile in the tunnel lining system. To examine the long-term thermal behavior of the energy textile, the difference in temperatures of the inlet and outlet fluid circulating through the heat exchange pipe within the energy textile was monitored using a constant-temperature water bath. Daily heat exchange rate of the energy textile during cooling operation was estimated from the measured temperatures of the inlet and outlet fluid through the energy textile. The air and ground temperature was also continuously monitored. The operation of the energy textile as a ground heat exchanger was simulated using a 3D numerical CFD model (Fluent). The thermal conductivity of shotcrete and concrete lining components and temperature variation of air in the tunnel were incorporated in the model. The numerical analysis shows a good agreement with the long-term monitoring result.

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The Study on the Structure and Performance of Heat Pump Calorimeter (열펌프 열량계 구조 및 성능 특성 연구)

  • Park, Seung Byung;Lee, Sang-Hyeok;Choi, Jinnil;Choi, Jong Min
    • Journal of the Korean Society for Geothermal and Hydrothermal Energy
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    • v.11 no.4
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    • pp.7-13
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    • 2015
  • The efficiency, reliability and performance of any heat pump unit can only be ascertained after it has been tested and rated. For this reason, specific facilities, equiped with testing plants are built. Heat pump calorimeter is the facilities used by most of these testing facilities in their rating and certification process. The ultimate function of calorimeters is to, control and maintain the constant standard test conditions (indoor/outdoor entering temperatures and flow rate etc) during testing period. In this study, the test standards of heat pump unit and the structure of the calorimeter are surveyed. In addition, this study analyzes the total energy consumption of a water to water heat pump calorimeter. Heat pump calorimeter consumed much energy to excute the heat pump tests. The energy consumption of the calorimeter was higher than the heat pump unit, and it was increased as the heat pump unit capacity decreased.