• 제목/요약/키워드: Compound Ⅲ

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데칸술폰이 삽입된 니켈 화합물의 층상 구조의 열적 성질 (Thermal behavior of the layered structure of decanesulfonate intercalated into the hydrated nickel compound)

  • 허영덕;전태현;박용준
    • 한국결정성장학회지
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    • 제9권6호
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    • pp.580-584
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    • 1999
  • 수화된 니켈에 데칸술폰이 층간 삽입된 화합물을 합성한 후 성질을 확인하였다. 화합물의 층상구조는 고온 X-선 회절 데이터로 확인하였다. 온도가 증가하면 층간 삽입된 니켈화합물의 구조가 변하는 것과 동시에 화합물의 층 거리가 24.7 $\AA$에서 30.5 $\AA$가지 증가하였다. X-선 회절 데이터와 데칸술폰의 크기로부터 니켈 층에 결합된 데칸술폰의 공간배열을 결정하였다. 이중 층 구조를 가진 데칸술폰의 분자 축은 니켈 층에 경사진 각도로 수직하게 배열되어있다.

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Sn/Cu 및 Sn/Ni 계면에서 금속간화합물 형성 및 성장에 관한 연구(II) (A Study of Intermetallic Compound Growth in the Sn/Cu and Sn/Ni Couples (II) : Sheet Resistance and Solderability Changes)

  • 김홍석;이성래
    • 한국표면공학회지
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    • 제22권2호
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    • pp.47-54
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    • 1989
  • The effects of intermetallic compound growt on the sheet resistance and soldreability as functions of the aging time, the temperature, and the conditions of substrates have been investi-gated in the electroplallic compound (mainy Cu6Sn5and Ni3Sn4) and the number of phase interface increased, the sheet resistance increased. Spread tests showed that the solderability was dereased with the intermetallic compounds growth and increased with the thickness of electroplated Sn. The surface morphology or agin size of the compound layer singificantly affect the solderability. The solderability of Sn/Ni system was superiot to Sn/Ni system was sperior to that of Sn/Cu system and the intermetallic compounds growth was solwer in the former system.

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산국에서의 Terpenes 함량의 변이 (Variation of Concentration of Terpenes in Chrysanthemum boreale)

  • 김종희
    • The Korean Journal of Ecology
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    • 제20권6호
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    • pp.397-403
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    • 1997
  • The monoterpenes and sesquiterpenes are analysed in the leaf and stem of Chrysanthemum boreale using gas chromaltography-mass spectrometry (GC-MS). The total amount of sesquiterpenes are always higher than monoterpenes in both leaf (2.0-3.4 times) and stem (1.6-8.3 times). The mono- and sesquiterpenes yields of the leaf are higher than the stem. There was no significant difference among the leaf developmental stages, while those of stem were varied. Seventeen monoterpenes and 9 sesquiterpenes compound in this plants comprised more than 5% of the mean total monoterpenes and the total sesquiterpenes in each dates. Among leaf monoterpenes, the concentration of (+)-Limonene and unknown compound no. 13 (Retention time, R.T.=17.28) varied significantly during leaf growing season, and the concentrafion of unknown compound no. 7 (R.T.=35.04) and no. 9(R.T.=35.71) varied in the leaf sesquiterpenes. Similarly the results from the leaf, the concentration of five monoterpenes in stem also varied significantly during maturing period, and much varied in seven compounds of stem sesquiterpene. The major sesquiterpenes of leaf and stem were ${\alpha}-Humulene$ and compound no. 2(R.T.=26.19).

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이온질화 에 있어서 첨가탄소량 이 경도 및 마모특성 에 주는 영향 (The Added Carbon Content Effect on the Hardness And Wear Characteristics in Ion-Nitriding)

  • 김희송
    • 대한기계학회논문집
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    • 제7권1호
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    • pp.19-27
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    • 1983
  • This paper deals with hardness and wear characteristics of ion-nitrided metal, and with ion-nitride processing which is concerned with the effects of added carbon content in gas atmosphere. A small optimal amount of carbon content in gas atmosphere increase compound layer thickness, as well as to increase diffusion layer thickness and hardness, and reduces wear rate when the applied wear load is small. It is found in the analysis that under small applied wear load, the critical depth where voids and cracks may be created and propagated is located at the compound layer, so that the abrasive wear where hardness is an important factor, is created and the existence of compound layer reduces the amount of wear. When the load becomes large, the critical depth is located below nucleation and propagation, is created and the existence of compound layer increase wear rate.

자긴가공된 복합실린더의 기계가공해석 (Machining Analysis of the Autofrettaged Compound Cylinder)

  • 박재현;김재훈;차기업;홍석균;이영신
    • 대한기계학회논문집A
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    • 제31권7호
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    • pp.800-807
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    • 2007
  • Autofrettage process is used for internal forming and sizing of cylinder designed to withstand high internal pressures. Once the tube is autofrettaged, it needs to be machined to its final dimensions both at the bore and its outer surface. This paper presents an analytical analysis and numerical analysis of machined compound cylinder using finite element code, ANSYS10.0. An analytical model for predicting the level of autofrettage following either inner, outer, or combined machining of the compound cylinder is developed for the autofrettage residual stress field is simulated by an autofrettaged pressure. The autofrettaged pressures are obtained by using trying-error method. As autofrettage percentage is 20 % and 40 %, the numerical results are found to be in almost agreement with the analytical ones. However, as autofrettage percentage is 60 %, the numerical results have a little difference with the analytical ones.

이반응형 브리지 화합물을 이용한 폴리에스테르/면 복합소재의 단일분산염료염색 (I) (The Disperse Dyeing of Polyester/Cotton Blend Using a Hetero-bifunctional Bridge Compound (I))

  • 김태경;윤석한;김미경
    • 한국염색가공학회지
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    • 제18권3호
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    • pp.1-9
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    • 2006
  • In order to dye polyester/cotton blend fabric by one-bath dyeing process with single disperse dye, a novel hetero-bifunctional bridge compound(DBDCBS) was synthesized and utilized. The DBDCBS was designed to contain two different reactive groups such as ${\alpha},{\beta}$-dibromopropionylamido and dichloro-s-triazinyl groups. The ${\alpha},{\beta}$-dibromopropionylamido group shows considerable reactivity towards amines or amino groups at acidic condition and high temperature. In contrast, the dichloro-s-triazinyl group has reactivity towards hydroxyl groups at alkaline condition and room temperature. In order to examine whether as a bridge the compound could combine dyes containing amino groups with cellulosic substrates, disperse dyes containing amino group were tried to dye the cotton fibers pretreated with the DBDCBS compound. By the results, polyester/cotton blends were dyed by one-bath dyeing process with single disperse dye,1,4-diaminoanthraquinone.

Broiler저장의 온도 및 경시에 따른 Methionine 함량 변화에 관한 연구 (A Study on the Methionine Content of Cold Storage Broiler in the Cooking)

  • 홍종만
    • 한국식품영양학회지
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    • 제1권1호
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    • pp.7-12
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    • 1988
  • In the view of the fact that data are scare concerning the change of Methionine composition of poultry meat in function of storage temperature and cooking method. The present study was carried out to change in these compounds and the results were summarized as follows. 1. The result of measuring methionine compound of raw material stored under the condition of 5$^{\circ}C$, 1$0^{\circ}C$ for 6 weeks were increased as temperature increases. 2. The result of change in methionine compound of roasting were decreased than raw material It was greatly decreased in the storage for 42 days at 1$0^{\circ}C$ and slightly decreased in the storage for 14 days at 5$^{\circ}C$ 3. When the boiling in the water, methionine compound was decreased than roasting to compare with raw material 4. By the results of this study, one of the best cooking method is roasting, because of the change in methionine compound of roasting is slightly decrease.

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복합진동계의 진동 인텐시티 능동 제어 (Active Control of Vibrational Intensity in a Compound Vibratory System)

  • 김기만
    • 한국정밀공학회지
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    • 제19권6호
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    • pp.109-118
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    • 2002
  • The vibrational intensity and the dynamic response of a compound vibratory system had been controlled actively by means of a feedforward control method. A compound vibratory system consists of a flexible beam and two discrete systems - a vibrating source and a dynamic absorber. By considering the interactive motions between discrete systems and a flexible beam, the equations of motion for a compound vibratory system were derived using a method of variation of parameters. To define the optimal conditions of a controller the cost function, which denotes a time averaged power flow, was evaluated numerically. The possibility of reductions of both of vibrational intensity and dynamic response at a control point located at a distance from a source were fecund to depend on the positions of a source, a control point and a controller. Especially the presence of a dynamic absorber gives the more reduction on the dynamic response but the less on the vibrational intensity than those without a dynamic absorber.

2K-HI 형식 복합형 무단변속기의 성능실험 (Performance Analysis of Compound CVTs with a 2K-HI)

  • 박재민;김연수;이상희;최상훈
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2005년도 춘계학술대회 논문집
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    • pp.1345-1348
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    • 2005
  • We designed the compound CVT (Continuously Variable Transmissions) by combining power circulation mode CVT and power split mode CVT, which have been proposed for connecting 2K-H I differential gear to the V- belt type CVU (Continuously Variable Unit), as an input coupled type. With the designed compound CVT, we carried out theoretical analysis and performance experiments. We proved that the compound CVT had a better performance than either of the power circulation mode or power split mode.

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황기(黃芪) (Astragalus membranaceus Bunge.) 뿌리의 성분연구(I) (A Study on the Constituents from the Roots of Astragalus membranaceus (I))

  • 김진숙;김연태;김정숙
    • 생약학회지
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    • 제27권4호
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    • pp.336-341
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    • 1996
  • The roots of Korean Astragalus membranaceus Bunge. (Leguminosae), Astragali Radix, were extracted following general methods. During these extractions, first of all, 1,2-benzendicarboxylic acid diisononylester(compound A), ${\beta}-sitosterol(compound\;B)$, $3-0-{\beta}-D-galactopyranosyl-{\beta}-sitosterol(compound\;C)$ and $stigmast-4-en-6{\beta}-ol-3-one(compound\;D)$ were isolated. Three of these compounds were identified the first time isolation from the genus of Astragalus.

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