• Restorative Dentistry and Endodontics
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• v.29 no.5
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• pp.413-422
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• 2004

Established microleakage tests have their own disadvantages. In this study, 3D reconstruction method was tried to overcome these disadvantages. Four types of microleakage tests were used and relationships among them were estimated: penetrated dye volume: marginal adaptability: degree of dye penetration and relative penetrated length to cavity wall. Twenty-four Class V cavities were bulk filled with composite (Esthet X) following surface treatments: N group (no treatment): E group (etching only): T group (etching + Prime & Bond NT). 50% silver nitrate was used as a dye solution after thermocycling ($5^{\circ}C{\;}&{\;}55^{\circ}C$, 1.000 times). Teeth were serially ground with a thickness of 0.2 mm. Volume of dye penetration was estimated from a three-dimensionally reconstructed image with a software (3D-DOCTOR). Percentage of margin without gap was estimated from SEM and degree of dye penetration and the relative length of dye penetration to overall cavity wall were also estimated. ANOVA and Scheffe test for dye volume, Kruskal-Wallis and Mann-Whitney test for marginal quality, Spearman's rho test for checking of relationships among methods were used. The results were as follows: 1. Dye penetration could be seen from several directions, furthermore, its volumetric estimation was possible. 2. Reverse relationship was found between dye volume and marginal quality (r = -0.881/ p = 0.004). 3. Very low relationship was seen between dye volume and two-dimensional tests (degree of dye penetration and relative length). However, 2D evaluation methods showed high relationship (p = 0.002-0.054) each other. 4. Three times vertical section could be recommended as a 2D test.

• Journal of Periodontal and Implant Science
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• v.32 no.2
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• pp.325-338
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• 2002

Bone graft using growth factors and guided tissue regeneration have been used for the regeneration of infrabony defects which caused by periodontal disease. Calcium sulfate which is one of the resorbable barrier materials used for guided tissue regeneration. Platelet rich plasma which is a easy method to obtain the growth factors had many common points but, platelet rich plasma was still studying. This study was the comparative study between bone graft using platelet rich plasma and guided tissue regeneration using calcium sulfate barrier material in clinical view. For the study, 28 sites(2 or 3 wall infrabony defects) were treated. 14 infrabony defects were received surgical implantation of BBP-calcium sulfate composite with a calcium sulfate barrier and the others received BBP mixed with platelet rich plasma. Clinical outcome was accessed 3 and 6 months of postsurgery. 1. There was no statistical difference between CS group and PRP group in pocket depth, gingival recession, clinical attachment level, and probing bone level at baseline. 2. There was statistically significant reduction in probing depth, clinical attachment level, and probing bone level at 3 and 6 months postsurgery(p<0.05). 3. In the probing depth and clincial attachment level PPR group had less improvement than CS group, but there was no statistically difference at 3 and 6 months postsurgery. 4. In the recession PPR group had less recession than CS group, but there was no statistically difference at 3 and 6 months postsurgery. 5. In the probing bone level PPR group had less improvement than CS group, but there was no statistically difference at 6 months postsurgery. In conclusion bone graft using platelet rich plasma and guided tissue regeneration using calcium sulfate barrier showed similar clinical improvement for the treatment of 2 or 3 wall infrabony defects.

• Journal of the Korean Electrochemical Society
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• v.13 no.1
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• pp.50-56
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• 2010

The multi-wall carbon nano-tube composite mixed with carbon paste electrode presented more sensitive and selective amperometric signals in the oxidation of glucose than general screen-printed carbon electrodes(SPCEs). Redox mediators to transport electrodes from enzyme to electrodes are very important part in the biosensor. A novel osmium redox complex was synthesized by the coordinating pyridine group containing primary amines which were electrochemically immobilized onto the MWCNT-SPCEs surface. Electrochemical studies of osmium complexes were investigated by cyclic voltammetry, chronoamperometry. The surface coverage of osmium complexes on the modified carbon nano-tube electrodes were significantly increased at 100 time (${\tau}_0=2.0\;{\times}\;10^{-9}\;mole/cm^2$) compared to that of the unmodified carbon electrodes. It's practical application of the glucose biosensor demonstrated that it shows good linear response to the glucose concentration in the range of 0-10 mM.

• Archives of Reconstructive Microsurgery
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• v.1 no.1
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• pp.51-55
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• 1992

Problems of composite tissue transfer commonly arise when a single indispensable recipient vessel receives the graft vssel, and the graft vessel must be sutured in end-to-side fashion so as not todisturb the vascularity of the recipient vessel. The triangular flap in the recipient vessel wall gives an intact endothelial surface when the flow of blood stream is presented and may reduce the chance of anastomosis. We selected mature Wistar rats weighing over 450 grams to compare the conventional longitudinal slit from the triangular flap in the recipient carotid artery over bloood pressure and blood flow when the donor carotid artery was anastomosed in end-to-side fashion. In 30 minutes after anastomosis, maximum blood pressure measured in the donor carotid arterial side when the recipient arterial wall was fasioned with the longitudinal slit was recorded 114 mmHg and with the triangular flap 100mmHg. Minimum blood pressure with the longitudinal slit was 98mmHg and with the triangular flap 88mmHg. The amount of blood collected for 30 seconds in the conventional longitudinal slit was 1.18mg and in the triangular flap 0.78mg. Histology study in 30 minutes, the conventional longitudinal slit demonstrated the more hemorrhagic features around the suture material compared to that of the triangular. flap and, in the 7th day, the conventional longitudinal slit demonstrated the more prominent granulomatous reactions and vascular proliferations around the suture material compared to that of the triangular flap.

• Steel and Composite Structures
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• v.37 no.1
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• pp.91-98
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• 2020

Steel plate shear walls are recently used as efficient seismic lateral resisting systems. These lateral resistant structures are implemented to provide more strength, stiffness and ductility in limited space areas. In this study, the seismic behavior of the multi-story steel frames with steel plate shear walls are investigated for buildings with 4, 8, 12 and 16 stories using verified computational modeling platforms. Different number of steel moment bays with distinctive lengths are investigated to effectively determine the deflection amplification factor for low-rise and high-rise structures. Results showed that the dissipated energy in moment frames with steel plates are significantly related to the inside panel. It is shown that more than 50% of the dissipated energy under various ground motions is dissipated by the panel itself, and increasing the steel plate length leads to higher energy dissipation capability. The deflection amplification factor is studied in details for various verified parametric cases, and it is concluded that for a typical multi-story moment frame with steel plate shear walls, the amplification factor is 4.93 which is less than the recommended conservative values in the design codes. It is shown that the deflection amplification factor decreases if the height of the building increases, for which the frames with more than six stories would have less recommended deflection amplification factor. In addition, increasing the number of bays or decreasing the steel plate shear wall length leads to a reduction of the deflection amplification factor.

• Steel and Composite Structures
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• v.23 no.4
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• pp.409-420
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• 2017

This paper theoretically studies the cyclic behavior of hybrid connections between steel coupling beams and concrete shear walls with embedded steel columns. Finite element models of connections with long and short embedded steel columns are built in ABAQUS and validated against the test results in the companion paper. Parametric studies are carried out using the validated FE model to determine the key influencing factors on the load-bearing capacity of connections. A close-form solution of the load-bearing capacity of connections is proposed by considering the contributions from the compressive strength of concrete at the interface between the embedded beam and concrete, shear yielding of column web in the tensile region, and shear capacity of column web and concrete in joint zone. The results show that the bond slip between embedded steel members and concrete should be considered which can be simulated by defining contact boundary conditions. It is found that the loadbearing capacity of connections strongly depends on the section height, flange width and web thickness of the embedded column. The accuracy of the proposed calculation method is validated against test results and also verified against FE results (with differences within 10%). It is recommended that embedded steel columns should be placed along the entire height of shear walls to facilitate construction and enhance the ductility. The thickness and section height of embedded columns should be increased to enhance the load-bearing capacity of connections. The stirrups in the joint zone should be strengthened and embedded columns with very small section height should be avoided.

• Steel and Composite Structures
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• v.23 no.4
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• pp.473-481
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• 2017

Steel plate shear wall (SPSW) system has been increasingly used for lateral loads resisting system since 1980s when the utilization of post-buckling strength of SPSW was realized. The structural response of SPSWs largely depends on the behavior of the surrounded beams. The beams are normally required to behave in the elastic region when the SPSW fully buckled and formed the tension field action. However, most modern design codes do not specify how this requirement can be achieved. This paper presents theoretical investigation and design procedures of manually calculating the plastic flexural capacity of the beams of SPSWs and can be considered as an extension to the previous work by Qu and Bruneau (2011). The reduction in the plastic flexural capacity of beam was considered to account for the presence of shear stress that was altered towards flanges at the boundary region, which can be explained by Saint-Venant's principle. The reduction in beam web was introduced and modified based on the research by Qu and Bruneau (2011), while the shear stress in the web in this research is excluded due to the boundary effect. The plastic flexural capacity of the beams is given by the superposition of the contributions from the flanges and the web. The developed equations are capable of predicting the plastic moment of the beams subjected to combined shear force, axial force, bending moment, and tension fields induced by yielded infill panels. Good agreement was found between the theoretical results and the data from previous research for flexural capacity of beams.

• Transactions of the Korean hydrogen and new energy society
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• v.32 no.5
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• pp.365-373
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• 2021

In this study, evaporation of LN2 non-spreading pool on concrete plate was dealt with experimentally. The thermophysical properties of concrete, which is a composite material, were obtained by minimizing the difference between the numerical analysis results obtained from the assumed properties and the results from experiments. The thermal energy required for evaporation of the liquid pool is supplied from the concrete plate and the wall of the container. As a result of the measurement, the thermal energy flowing in from the wall was negligible compared to the one supplied from the concrete plate. It was found that the measured evaporation rate of the liquid pool by the heat energy supplied through the concrete plate agrees well with the PTC model except for the initial section of the experiment. The validity of the semi-infinite assumption and the one-dimensional assumption, which are the main conditions of the PTC model, was also verified through experiments. The evaporation rate model in the non-spreading pool discussed in this study can provide a basic frame for the one in the spreading pool, which is a meaningful result considering that the spreading pool is very realistic compared to the non-spreading pool.

• Steel and Composite Structures
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• v.29 no.6
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• pp.717-734
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• 2018

This paper presents the flexural performance of steel beam-to-column joints composed of hollow structural section beams and columns. A finite element (FE) model was developed incorporating geometrical and material nonlinearities to evaluate the behaviour of joints subjected to bending moments. The numerical outcomes were validated with experimental results and compared with EN1993-1-8. The demountability of the structure was discussed based on the tested specimen. A parametric analysis was carried out to investigate the effects of steel yield strength, end-plate thickness, beam thickness, column wall thickness, bolt diameter, number of bolts and location. Consequently, an analytical model was derived based on the component method to predict the moment-rotation relationships for the sub-assemblies with extended end-plates. The accuracy of the proposed model was calibrated by the experimental and numerical results. It is found that the FE model is fairly reliable to predict the initial stiffness and moment capacity of the joints, while EN1993-1-8 overestimates the initial stiffness extensively. The beam-to-column joints are shown to be demountable and reusable with a moment up to 53% of the ultimate moment capacity. The end-plate thickness and column wall thickness have a significant influence on the joint behaviour, and the layout of double bolt-rows in tension is recommended for joints with extended end-plates. The derived analytical model is capable of predicting the moment-rotation relationship of the structure.

• Applied Chemistry for Engineering
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• v.30 no.2
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• pp.178-185
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• 2019

Three spherical quaternary composites composed of metal/metal oxide/high explosive/oxidizer were prepared by a crystallization/agglomeration process. From the characteristics of composites by thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC), the shortening of the decomposition zone of high explosives in the quaternary composite was observed, which may be attributed to the autocatalytic reaction caused by $ClO_2$ or HCl which are ammonium perchlorate (AP) degradation products. The activation energy analysis showed that the activation energy abruptly decreases at the end of the decomposition zone of high explosives, and it was considered to be caused by $HNO_2$ which is common in decomposition products of high explosives. The activation energy predicted from complex pyrolysis results by the distributed activation energy model (DAEM) showed much better in accuracy than those by model-fitting methods such as Kissinger-Akahira-Sunose and Flynn-Wall-Ozawa models.