• Korean Journal of Pharmacognosy
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• v.35 no.1 s.136
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• pp.88-91
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• 2004

Abstract - The Evodiae Fructus is known for containing a number of indolquinazoline and quinoline type alkaloids. Evodiamine, evocarpine and rutaecarpine are the major constituents of alkaloids. These alkaloids were isolated and determined by forming complex compounds from Evodiae Fructus in O-Su-You-Tang. For the determination of these alkaloids, a new spectrophotometric method was developed with a simple and selective sample clean-up using thiocyanatocobaltate[II] compIεx compound ion. The absorbance of alkaloidal complex compounds in 1,2-dichloroethane solution was measured at 625 nm. The method proved to be rapid, simple and reliable for the isolation and the determination of the alkaloids in O-Su-You-Tang.

• Journal of the Korean Chemical Society
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• v.10 no.1
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• pp.4-10
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• 1966

A new method of cobalt determination has been developed by employing ethylenediamine tetrabutyl acetate(EDTA-butyl ester) synthesized from EDTA and Butyl alcohol. The synthesized EDTA ester dissolved in butyl alcohol extracts various metal ions from aqueous solutions. Cobaltous ion extracted into organic phase containing EDTA ester to form Co (II)-EDTA butyl ester complex is back extracted into alkaline aqueous phase forming a stable pink colored complex of Co (III). The optimum condition for spectrophotometric determination of cobalt via the new complex has been established. The absorption peak occurs at 540$m{\mu}$ and Beer's law was obeyed over the concentration range of 0∼50 ${\mu}g/ml$ of cobalt.

• Proceedings of the KWS Conference
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• v.43
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• pp.150-152
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• 2004

This study was aimed at evaluation of residual stress of steel pipe structures. The production process of pipes was complex (at first bending was done by roll forming or press forming and welding was final process of making of steel pipes). So there could be effected high residual stresses in steel pipes. In order to evaluate the changes of residual stress the locations of measurement were selected carefully. Measurements of residual stress were done for various kinds of pipes (shapes in circular and square). For the evaluation of residual stress, hole-drilling method (ASTM E837 was applied. The results showed that along the weld Eine high tensile stress were measured as effected, and high tensile stresses were measured where large plastic deformation developed. Through these efforts, experimental results could be more effectively assisted by numerical method.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.3 s.174
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• pp.550-559
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• 2000

One of the most important factor to be considered for the analysis of sheet metal forming processes is the tool surface description for arbitrarily- shaped sheet metal parts. In the present study , finite element approach is used to describe the arbitrarily shaped tool surface. In finite element mesh approach, tool surfaces ar, described by finite elements. The finite elements mesh description of the tool surface, which is originally described by CAD data, needs much time and time-consuming graphic operation. The method, however, has been widely used to describe a complex tool surface. In the present study, the contact searching algorithm for the finite element mesh approach is developed based on cell strategy method and sheet surface normal scheme. For the verification purpose, a clover cup drawing, Baden-Baden oilpan problem and a trunk floor drawing were investigated. The computational results based on the finite element approach were compared with the results of available parametric patch approach and experiments.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1995.03a
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• pp.196-202
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• 1995

Drawbead formulation is the first process together with a binder wrap process in a sheet metal forming process. The purpose of a drawbead is to control the flow of the metal into the die in panel press forming. To simulate the drawbead formation process, an elasto-plastic finite element formulation is derived from the equilibrium equation an drelated boundary conditions considering the proper contact conditons. The developed finite element program is applied to drawbead formation in the plane strain condition. The simulation of drawbead formation produces the distribution fo stress and strain along the bead and the resultant elongation of the sheet in the cavity region with respect to various cavity dimensions of the sheet as well as the punch force of a drawbead and the amount of draw-in with respect to the stroke fo a drawbead. The numerical resutls provides the fundamental information as a boundary condition to analyze the complex binder wrap phenomena and panel press forming in simple way.

• Journal of the Korean Society for Precision Engineering
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• v.14 no.8
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• pp.57-64
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• 1997

The process design of backward and forward extrusion of axisymmetric part has been studied in this paper. The important factors of cold forging process with complex geometry are the design of initial billet shape, the possibility of forming by one-stage operation and the determination of preform shapes, etc. Based on the systematic procedure of process sequence design, the forming operation of cold forged part is analyzed by the commercial finite element program, DEFORM. The design criteria are forming load, geo- metrical filling without defect and a sound distribution of effective strain in final product. It is noted that one step of preform operation is required to obtain the final product. Numerical result is compared with experi- mental one. It is found that the analyzed result is in good agreement with actual forming result.

• Korean Journal of Pharmacognosy
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• v.33 no.3 s.130
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• pp.182-186
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• 2002

The Coptidis rhizoma is known for containing protoberberine alkaloids. Berberine, coptisine and palmatine are the major constituents of protoberberine alkaloids. The alkaloids were isolated and determined by forming complex compounds from Coptidis rhizoma in preparation I(Sam-Hwang-Sa-Sim-Tang) and II(Hwang-Ryen-Tang). For the determination of these alkaloids, a new spectrophotometric method was developed with a simple and selective sample clean-up using thiocyanatocobaltate[II] complex compound ion. The absorbance of alkaloidal complex compounds in l.2-dichloroethane solution was measured at 625 nm. Calibration curve for the alkaloids isolated from Coptidis rhizoma was linear over the concentration range of 0.2-0.3 mg/ml. The method was proved to be rapid, simple and reliable for the isolation and the determination of the alkaloids in Coptidis rhizoma preparation I and II.

• Journal of Korean Society of Industrial and Systems Engineering
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• v.39 no.4
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• pp.90-96
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• 2016

Incremental sheet forming (ISF) is a highly versatile and flexible process for rapid manufacturing of complex sheet metal parts. Compared to conventional sheet forming processes, ISF is of a clear advantage in manufacturing small batch or customized parts. ISF needs die-less machine alone, while conventional sheet forming requires highly expensive facilities like dies, molds, and presses. This equipment takes long time to get preparation for manufacturing. However, ISF does not need the full facilities nor much cost and time. Because of the facts, ISF is continuously being used for small batch or prototyping manufacturing in current industries. However, spring-back induced in the process of incremental forming becomes a critical drawback on precision manufacturing. Since sheet metal, being a raw material for ISF, has property to resilience, spring-back would come in the case. It is the research objective to investigate how geometrical shaping parameters make effect on shape dimensional errors. In order to analyze the spring-back occurred in the process, this study experimented on Al 1015 material in the ISF. The statistical tool employed experimental design with factors. The table of orthogonal arrays of $L_8(2^7)$ are used to design the experiments and ANOVA method are employed to statistically analyze the collected data. The results of the analysis from this study shows that the type of shape and the slope of bottom are the significant, whereas the shape size, the shape height, and the side angle are not significant factors on dimensional errors. More error incurred on the pyramid than on the circular type in the experiments. The sloped bottom showed higher errors than the flat one.

• Transactions of Materials Processing
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• v.7 no.5
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• pp.489-495
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• 1998

Spinning is a chipless forming method for producing axially symmetric parts by using axial-radial motions of a spinning roller. This process has still some advantages in such a view point that a variety of complex shapes which can not be formed in a press can be easily spun at a low cost although it is one of the oldest forming methods for spinning mainly cookware parts for a long time. This study is to investigate the optimum roller path in order to obtain the maximum spinnability in producing cylindrical cups of Aluminum(A1050-H16) sheet metal. Working conditions applicable to any size of blank were predetermined through preliminary spinning tests. 9 types of roller path were proposed and experiments were carried out. The modified involute curve was shown to give the maximum drawing ration and more uniform quality of spun cups as compared with other results of this study. in addition thickness distribution and dimensional accuracy of spun cups were examined and discussed.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.03a
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• pp.18-21
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• 1999

The wrinkling of thin sheet metal induced by compressive instability is one of major defects in sheet metal forming processes. compressive instability is influence by many factors such as mechanical properties of the sheet material geometry of the sheet contact conditions and plastic anisotropy. The analysis of compressive instability in a plastically deforming body is rather difficult because the effects of the above-mentioned factors are rather complex and the instability behavior may show swide variations even for small deviations of the factors. in this work the bifurcation theory is introduced for the finite elemental analysis of the instability behavior of a thin sheet with initially sound geometry and property. All the above-mentioned factors are conveniently considered by the finite element method. The instability limit is found by introducing a criterion scheme into the incremental analysis and the post-bifurcation behavior is analyzed by introducing the branching scheme. Wrinkling initiation and growth in the deep drawing process are analyzed.