• Title/Summary/Keyword: Complex Samples Analysis

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Cardiac Disease Detection Using Modified Pan-Tompkins Algorithm

  • Rana, Amrita;Kim, Kyung Ki
    • Journal of Sensor Science and Technology
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    • v.28 no.1
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    • pp.13-16
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    • 2019
  • The analysis of electrocardiogram (ECG) signals facilitates the detection of various abnormal conditions of the human heart. The QRS complex is the most critical part of the ECG waveform. Further, different diseases can be identified based on the QRS complex. In this paper, a new algorithm based on the well-known Pan-Tompkins algorithm has been proposed. In the proposed scheme, the QRS complex is initially extracted by removing the background noise. Subsequently, the R-R interval and heart rate are calculated to detect whether the ECG is normal or has some abnormalities such as tachycardia and bradycardia. The accuracy of the proposed algorithm is found to be almost the same as the Pan-Tompkins algorithm and increases the R peak detection processing speed. For this work, samples are used from the MIT-BIH Arrhythmia Database, and the simulation is carried out using MATLAB 2016a.

A Free-Space Method for Measurement and Analysis of Dielectric Characteristics of Electromagnetic Absorbing Materials at Microwave Frequencies (자유공간 기법을 적응한 마이크로파 대역 전파흡수재의 유전 특성 분석)

  • 배근식
    • Journal of the Korea Institute of Military Science and Technology
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    • v.6 no.2
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    • pp.73-82
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    • 2003
  • For measurements and analysis of dielectric characteristics of planar slabs of microwave absorbing materials, I have applied a free-space method in the frequency range of 8~14 GHz. The measurement system for free-space method consists of transmit and receive antennas, mode transitions, precision coaxal cables, the network analyzer, and a computer Special Spot-focused horn lens antenna was used to eliminate diffraction effects. Diffraction effects at the edges of the sample are minimized by satisfying the condition for minimum transverse dimension of the plate and the beamwidth of the antennas at the focus. The time-domain gating feature of the network analyzer and the thru, reflect, and line(TRL) calibration technique were used to eliminate the effects of undesirable multiple reflections. The complex coefficients of reflection and transmission, $S_{11}$ and $S_{21}$, of planar samples were measured for standard materials such as Teflon, Rexolite$\textregistered$ 2200. The results were compared with existing measurement method. And I applied a free-space method for measurement to measure dielectric constants of some electromagnetic absorbing materials. Dielectric properties for the same samples were also measured with a 7mm coxial transmission line method for purposes of comparison with the free-space method.

Application of stoichiometric method in the assessment of groundwater chemistry in a coastal region having complex contaminant sources

  • Rajmohan Natarajan;Kim, Kang-Joo;Hwang, Gab-Soo;Kim, Hyun-Jung;Cho, Min-Joe
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2004.04a
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    • pp.499-502
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    • 2004
  • Groundwater chemistry in a coastal region having complex contaminant sources was investigated. Water analysis data for 197 groundwater samples collected from the uniformly distributed sixty-six wells were used. Chemical analysis rand results indicate that groundwaters show wide concentration ranges in major inorganic ions, reflecting complex hydrochemical processes of pollutants. Due to the complexity of groundwater chemistry, Results illustrate that thirty five percent of the wells do not fit for drinking based on nitrate and chloride concentration in the study area. the samples were classified into four groups based on Cl and NO$_3$ concentrations and the processes controlling water chemistry were evaluated based on the reaction stoichiometry. The results explained the importance of mineral weathering, anthropogenic activities (nitrification and oxidation of organic matters), and Cl-salt inputs (seawater, deicer, NaCl, etc.) on groundwater chemistry. It was revealed that mineral dissolution is the major process controlling the water chemistry of the low Cl and NO$_3$ group (Group 1). Groundwaters high in NO$_3$ (Groups 2 and 4) are acidic in nature, and their chemistry is largely influenced by nitrification, oxidation of organic matters and mineral dissolution. In the case of chloride rich waters (Group 3), groundwater chemistry is highly influenced by mineral weathering and seawater intrusion associated with cation-exchange reactions.

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The Evaluation Functional Activity and Indicator Component Analysis and According to the Extraction Method of Eleuthrococcus Gracilistylus (섬오갈피 추출물 중 acanthoic acid 및 Kaurenoic acid 함량 분석 및 기능성 활성 평가)

  • Hyun Kyoung Kim
    • The Journal of the Convergence on Culture Technology
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    • v.10 no.2
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    • pp.73-80
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    • 2024
  • To determinate the content of acanthoic acid and kaurenoic acid in 70% EtOH and hot water extracts of Eleutherococcus gracilistylus, quantitative analysis of each compound in samples was carried out by a HPLC-UVD. Also, the identification of each acompound in samples was successfully assigned by LC-MS analysis. In result, the contents of acanthoic acid and kaurenoic acid in 70% ethanoic extracts were 28.84±0.21 mg/g (2.88%), 26.38±1.63 mg/g (2.64%), respectively. However, the content of two compounds in hot-water extracts was not observed. In conclusion, it shows that 70% ethanol as a best extraction solvent to extract the acanthoic acid and its metabolite from Eleutherococcus gracilistylus was better than hot-water solvent. The 70% ethanol complex extract of Allium Hookeri and Eleutherococcus gracilistylus showed better effectiveness. In addition, the 70% ethanol extract complex of Allium Hookeri and Eleutherococcus gracilistylus showed better effects than the hot water solvent of DPPH radical scavenging ability, total polyphenols, and flavonoids content. The anti-inflammatory activity were significantly or partially reduced by treatment with ethanol extract complex(SEC) by Allium Hookeri and Eleutherococcus gracilistylus.

Analysis of formaldehyde using DNPH cartridge/LC-MS in the Ban-Woll.Shi-Hwa Industrial Complex (DNPH cartridge/LC-MS 방법에 의한 반월.시화산업단지의 폼알데하이드 분석에 관한 연구)

  • Cho Deok-Hee;Song Il-Seok;Kim In-Gu;Kim Woong-Soo;Kim Jong-Bo;Kim Tae-Hyun;Hwang Sun-Min;Nam Woo-Kyong
    • Journal of environmental and Sanitary engineering
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    • v.21 no.1 s.59
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    • pp.35-43
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    • 2006
  • Formaldehyde is important because of their irritant and toxic properties, mutagenicity and carcinogenicity. In this study, liquid chromatography-mass spectrometry (LC-MS) is used for the analysis of formaldehyde after derivatization with 2,4-dinitrophenylhydrazine (DNPH) cartridge. Analytical parameters such as linearity, repeatability and minimum detection limit were evaluated. The linearity ($r^2$) was 0.9997 when analyte concentration ranges from 25 to $200{\mu}g/l$. The relative standard deviation (%RSD) was 1.25 % for concentration of $200{\mu}g/l$. The minimum detection limit (MDL) was 0.73 ppbv. It was shown that LC-MS method has a great potential for formaldehyde analysis. The results of formaldehyde from the survey of Ban-Woll and Shi-Hwa Industrial Complex samples, the highest level was 6.20, 3.93 ppb, respectively. The highest emission level of formaldehyde at chemical plants in the Ban-Woll' Shi-Hwa Industrial Complex was 5421.25 ppb.

Characteristics of Respirable Particulate Matter from the Third and Fourth Industrial Complex Area of Daejeon City Using Instrumental Neutron Activation Analysis (기기중성자방사화분석을 이용한 대전 3, 4 공단지역의 호흡성입자의 특성)

  • Lim, Joung-Myoung;Lee, Jin-Hong
    • Journal of Environmental Impact Assessment
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    • v.15 no.6
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    • pp.425-433
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    • 2006
  • Instrumental neutron activation analysis was used to measure the concentrations of 27 elements associated with respirable particulate matter (PM10) that were collected from the Third and Fourth Industrial Complex Area of Daejeon City. The distribution patterns of elements were clearly distinguished with their concentrations varying across more than four orders of magnitude. The mean for Al were recorded to be the highest value of 1,527 $ng/m^3$, while that for In showed the lowest value of 0.1 $ng/m^3$. If compared in terms of enrichment factors, it was found that certain elements (e.g., As, Br, Cl, Cr, I, In, Sb, Se, and Zn) are enriched in PM10 samples of the study site. The results of factor analysis indicated six factors with statistical significance, which may exert dominant controls on regulating the elemental concentration levels in the study area.

Similarity Analysis of Chemical Profiles of Scrophularia buergeriana Based on HPLC-DAD

  • Kim, Dae-Hyun;Park, Jin-Ho;Kim, Young-Choong;Sung, Sang-Hyun;Kim, Seung-Hyun
    • Natural Product Sciences
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    • v.17 no.3
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    • pp.225-229
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    • 2011
  • A new approach for similarity analysis of chemical profiles of Scrophularia buergeriana was developed. The roots of S. buergeriana collected in Andong, Korea were analyzed using HPLC-DAD and the peak areas of the chromatograms were used to construct the chemical profiles of S. buergeriana. The analytical conditions were validated for specificity, precision and repeatability. The standard chemical profiles were established from the chromatograms of nine standard analytical extracts from three batches. The correlation coefficients of peak areas of characteristic compounds between the chromatograms of the standard and test samples were calculated for quantitative expression of the chemical profiles. The results showed that the HPLC chemical profiles of the samples of same geographic origin were relatively consistent. This new approach could be applied to the quality assessment of herbal medicines with complex chemical compositions.

Spectrophotofluorometric analysis of 2-[[3-(Trifluoromethyl) pheny 1] amino]-3-pyridine carboxylic acid in urine

  • Lee, Kang-Choon;Min, Shin-Hong;Rhee, Shang-Hi;Lee, Yoon-Joong
    • Archives of Pharmacal Research
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    • v.3 no.1
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    • pp.17-21
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    • 1980
  • A sensitive spectrophotofluorometric method was developed for the analysis of 2[[3-(trifluoromethyl)phenyl]amino]-3-phridine carboxylic acid (I) in urine. The method is based on the fluoroscence behavior of the I-aluminum complex in absolute ethanol. This fluorophore has activation and emission wavelengths of 355 and 450 nm, respectively. Optimum conditions for the reaction were investigated. The fluorescence was linear in the range of 0.25 3.0 ug of I/ml. Replicate studies of spiked urine samples, each containing 2.5 ug of I/ml showed good precision with a relative standard deviation of 0.019. Overall recovery percent from five spiked urine samples was 99.4 $\pm$1.32%.

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Stability and Environmental Safety of a Nanosized Agroformulation by Using Gamma-irradiation Technique (감마선을 이용하여 제조한 농업용 나노제제의 보존성 및 환경안전성)

  • Park, Hae-Jun;Kim, Hwa-Jung;Choi, Jin-Su
    • Journal of Radiation Industry
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    • v.7 no.2_3
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    • pp.171-176
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    • 2013
  • In previous study, the novel nanosized curdlan-silica complex for a sustain-releasing effect was developed by using gamma-irradiation. It can be applicable to use in various sustainr-eleasing formulation in agriculture industry. This study was conducted to investigate its storage stability and environmental toxicity in an accelerated condition. The complex samples were treated with high temperature condition ($65^{\circ}C$) during 3 weeks, and then sustain-releasing property of complex was verified thereby using Ion Chromatography on a weekly basis. The morphology of the complex was characterized using scanning electron microscopy (SEM). Results of Ion Chromatography analysis showed that sample treated for 3 weeks was similar to sustain-releasing pattern of non-treatment sample. We verify concluded that the complex is able to keep its sustain-releasing property and sustained-releasing in 3 years. Also the formulation has no environmental toxicity.

Analysis of EM Wave Absorption Properties in W-band using $TiO_2$ (W-대역에서 유전손실재료인 $TiO_2$의 전파흡수 특성 분석)

  • Choi, Chang-Mook;Kim, Dong-Il;Ko, Kwang-Soobl
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2007.06a
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    • pp.95-98
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    • 2007
  • In this paper, we make an analysis of electromagnetic wave absorption properties of $TiO_2$ in W-band. Therefore, we fabricated some samples in different composition ratio of $TiO_2$ and CPE. And the material properties of samples are calculated from S-parameter of samples using $\ell-2\ell$ method. We analyze absorption properties and complex relative permittivitis of samples. As a result, it has verified that absorption properties of sample containing $TiO_2:CPE=70:30wt.%$ have been excelled in W-band.

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