• Title/Summary/Keyword: Coating structure

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Uniform Coating of Organic-Capped Ba-Ti-O Nanolayers on Spherical Ni Particles

  • Lee, Yong-Kyun;Choi, Jae-Young;Yoon, Seon-Mi;Lee, Jong-Heun
    • Korean Journal of Materials Research
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    • v.17 no.2
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    • pp.86-90
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    • 2007
  • The organic-capped Ba-Ti-O nanolayers were coated uniformly on spherical Ni particles for multilayer ceramic capacitor (MLCC) applications via the formation of Ti-hydroxide nano-coating layers and their subsequent reaction with Ba-stearate at $180^{\circ}C$. The capping of organic shell on oxide coating layer changed the hydrophilic surface structure into hydrophobic one, which significantly improved the dispersion behavior in hydrophobic solvents such as terpineol and butanol. In addition, the uniform coating of Ba-Ti-O layer was advantageous to prevent Ni oxidation. This method provides a useful chemical route to fabricate organic-soluble Ba-Ti-O coated Ni particles for a highly integrated passive component.

Sintering of Nd-Fe-B Magnets from Dy Coated Powder

  • Kim, Jin Woo;Kim, Young Do
    • Journal of Powder Materials
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    • v.20 no.3
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    • pp.169-173
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    • 2013
  • High-coercive (Nd,Dy)-Fe-B magnets were fabricated via dysprosium coating on Nd-Fe-B powder. The sputtering coating process of Nd-Fe-B powder yielded samples with densities greater than 98%. $(Nd,Dy)_2Fe_{14}B$ phases may have effectively penetrated into the boundaries between neighboring $Nd_2Fe_{14}B$ grains during the sputtering coating process, thereby forming a $(Nd,Dy)_2Fe_{14}B$ phase at the grain boundary. The maximum thickness of the Dy shell was approximately 70 nm. The maximum coercivity of the Dy sputter coated samples(sintered samples) increased from 1162.42 to 2020.70 kA/m. The microstructures of the $(Nd,Dy)_2Fe_{14}B$ phases were effectively controlled, resulting in improved magnetic properties. The increase in coercivity of the Nd-Fe-B sintered magnet is discussed from a microstructural point of view.

Effects of Curing Agent on the Corrosion Protection of Diglycidyl Ether Bisphenol-A Based Epoxy Coating

  • Shon, MinYoung;Kwon, HyukSang
    • Corrosion Science and Technology
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    • v.7 no.6
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    • pp.344-349
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    • 2008
  • Epoxy coatings were prepared to give a different corrosion protection by reacting it with two different kinds of curing agent, and then effects of the curing agents on the structure, surface hydrophobic tendency, water transport behavior and hence corrosion protection of epoxy coatings were examined using hygrothermal cyclic test, and impedance analysis. In the results of EIS, the corrosion protection of epoxy coating cured by polyamide shows better than epoxy coating cured by polyamide epoxy adduct. It was well agreed with its water transport behavior and hydrophobic tendency.

Deposition Behavior and Properties of Carbon Nanotube Aluminum Composite Coatings in Kinetic Spraying Process (탄소 나노튜브 알루미늄 복합재료 저온 분사 코팅의 적층 거동 및 특성)

  • Kang, Ki-Cheol;Xiong, Yuming;Lee, Chang-Hee
    • Journal of Welding and Joining
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    • v.26 no.5
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    • pp.36-42
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    • 2008
  • Carbon nanotube (CNT) aluminum composite coatings were built up through kinetic spraying process. Deposition behavior of CNT aluminum composite on an aluminum 1050 alloy substrate was analyzed based on deposition mechanism of kinetic spraying. The microstructure of CNT aluminum composite coating were observed and analyzed. Also, the electrical resistivity, bond strength and micro-hardness of the CNT aluminum composite coatings were measured and compared to kinetic sprayed aluminum coatings. The CNT aluminum composite coatings have a dense structure with low porosity. Compared to kinetic sprayed aluminum coating, the CNT aluminum composite coatings present lower electrical resistivity and higher micro-hardness due to high electrical conductivity and dispersion hardening effects of CNTs.

Preparation and Characteristics of Anti-Corrosive Coatings for Steel Structures using Polyaniline (폴리아닐린을 이용한 강 구조물용 방청도료의 제조 및 특성)

  • Kim, Tae-Ok;Kong, Seung-Dae;Park, Jin-U;Hahm, Hyun-Sik
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.3
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    • pp.230-237
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    • 2006
  • Anti-corrosive coatings for steel structures with an alternative anti-corrosive pigment, polyaniline was prepared and anti-corrosive characteristics of the prepared coatings were investigated. The structure of the polyaniline was identified by using FT-IR, UV/Vis. and TGA analysis, and the anti-corrosive properties were analyzed from the results of the salt spray experiment. We found that the anti-corrosion properties of the prepared coatings varied in accordance with the types of primer coating resins as well as with the existence and nonexistence of the top coating. In this condition, the properties of adhesion, chemical resistance, and water resistance were found to be very satisfactory when using the single-packaged urethane resin as the primer coating resin and the urethane resin as the top coating resin.

A study of hydroxyapatite coating on Ti-6Al-4V dental implant alloy with different surface treatments using a sol-gel derived precursor (Sol-Gel 성형체에 의해 다르게 표면 처리된 치과 Implant용 Ti-6Al-4V합금의 Hydroxyapatite 코팅에 관한 연구)

  • Han, Sok-Yoon
    • Journal of Technologic Dentistry
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    • v.26 no.1
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    • pp.139-144
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    • 2004
  • In the present study, a simple method was successfully used for hydroxyapatite coatings on Ti-6Al-4V substrates deposited by using a sol-gel derived precursor. Prior to hydroxyapatite coating the samples were micropolished (0.1 micron) and divided into three sets. The first set,were the micropolished samples kept as such. The second set were coated with titania sol and the third set was treated with 5M NaOH. After three repetitions of hydroxyapatite coating procedures on each set and heat treatment at 600 $^{\circ}\Delta C$, the formation of hydroxyapatite has been confirmed by XRD analyses and the substrate material was found to be oxidized with negligible amount of CaO in the coating. The SEM studies revealed surface morphology. Hydroxyapatite, calcined at 600$^{\circ}\Delta C$, displaying a porous structure arisen from heating of the bulk. But, it is very meaningful in trying to approach morale management plans with an object of dental technicians. It is necessary that dental technicians should make efforts to control themselves.

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A Research on DLC Thin Film Coating of a SiC Core for Aspheric Glass Lens Molding (비구면 유리렌즈 성형용 SiC 코어의 DLC 코팅에 관한 연구)

  • Park, Soon-Sub;Won, Jong-Ho
    • Journal of the Korean Society for Precision Engineering
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    • v.27 no.12
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    • pp.28-32
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    • 2010
  • Technical demands for aspheric glass lens formed in market increases its application from simple camera lens module to fiber optics connection module in optical engineering. WC is often used as a metal core of the aspheric glass lens, but the long life time is issued because it fabricated in high temperature and high pressure environment. High hard thin film coating of lens core increases the core life time critically. Diamond Like Carbon(DLC) thin film coating shows very high hardness and low surface roughness, i.e. low friction between a glass lens and a metal core, and thus draw interests from an optical manufacturing industry. In addition, DLC thin film coating can removed by etching process and deposit the film again, which makes the core renewable. In this study, DLC films were deposited on the SiC ceramic core. The process variable in FVA(Filtered Vacuum Arc) method was the substrate bias-voltage. Deposited thin film was evaluated by raman spectroscopy, AFM and nano indenter and measured its crystal structure, surface roughness, and hardness. After applying optimum thin film condition, the life time and crystal structure transition of DLC thin film was monitored.

Characterization of the Morphology and Corrosion Resistance in Electroless Ni-P-TiO2 Composite Coating Prepared by TiO2 Contents (TiO2 함량에 따르는 무전해 Ni-P-TiO2 복합도금층 특성 연구)

  • Byoun, Young-Min;Kim, Ho-Young;lee, Jae-Woong;Hwang, Hwan-il
    • Journal of the Korean institute of surface engineering
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    • v.52 no.4
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    • pp.187-193
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    • 2019
  • Electroless Ni-P coatings are widely used in the chemical, mechanical, and electronic industries because of their excellent wear and abrasion resistance. In this study, the effect of $TiO_2$ particles of composite coating was investigated. To improve the corrosion resistance, electroless $Ni-P-TiO_2$composite coating was studied by varying the $TiO_2$ content. The morphology and phase structure of $Ni-P-TiO_2$ composite coatings were analyzed by scanning electron microscopy(SEM), X-ray diffractometry(XRD) and X-ray photoelectron spectroscopy(XPS). The result showed that $Ni-P-TiO_2$composite coating is composed of Ni, P, Ti and O. It exhibits an amorphous structure, high hardness and good corrosion resistance to the substrate. $Ni-P-TiO_2$ composite coatings have higher open circuit potential than that of the substrate, which obtained at $TiO_2$ content of 5.0 g/L optimal integrated properties.

Image Tracking Interference Minimize of Electro Optical Tracking System by MgF2 Nano Structure Antireflective Coating Films (MgF2 나노구조 반사방지막을 통한 함정용 전자광학추적장비 영상추적간섭 최소화)

  • Shim, Bo-Hyun;Jo, Hee-Jin
    • Journal of the Institute of Electronics and Information Engineers
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    • v.52 no.5
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    • pp.206-213
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    • 2015
  • An omni-directional, graded-index and textured ZnO nanorods with $MgF_2$ anti-reflective(AR) coating films for the electro optical tracking system(EOTS) by e-beam evaporation method are presented. we achieved that the graded index structure can minimize image tracking interference of EOTS which is comparable to a general AR coating films. Optimized ZnO nanorods with $MgF_2$ AR coating films lead to decreasing Fresnel reflection by gradient refractive index. According to our experiment results, ZnO nanorods with $MgF_2$ AR coating films can be used for various electro optical system to improve the optical performance.

Changes in the Process Efficiency and Product Properties of Pulp Mold by the Application of Oil Palm EFB (오일팜 EFB 섬유 적용에 따른 펄프몰드 공정효율 및 제품품질 변화)

  • Kim, Dong-Seop;Sung, Yong Joo;Kim, Chul-Hwan;Kim, Se-Bin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.48 no.1
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    • pp.67-74
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    • 2016
  • The demand of environmental friendly packaging materials such as pulp mold has been increased. The application of the oil palm biomass, EFB (Empty Fruit Bunch) fiber as natural raw materials to the pulp mold could increase the usability of the pulp mold by the reduced production cost brought from the relatively low cost of EFB. The effects of the EFB(Empty Fruit Bunch) fibers on the properties of pulp mold and on the process efficiency were evaluated in this study. The pulp mold samples were prepared with mixture ONP (Old news paper) and EFB by using laboratory wet pulp molder. The changes in the drying efficiency were measured with the changes in the solid contents of pulp mold samples during drying process. The efficiency of the surface coating treatment on the pulp mold depending on the condition of the pulp mold samples were also evaluated in order to improve the water resistance properties of pulp mold. The addition of EFB increased the drying efficiency by providing the bulkier structure and the higher water contact angle, which indicated the better water resistance properties. The water resistance were improved by the surface coating treatments and the application of surface coating on the pulp mold at the higher moisture contents resulted in the higher improvement in the water resistance. The bulkier structure originated from the application of EFB fiber reduced the effects of the surface coating, which could be overcome by the control of surface coating process.