• Title/Summary/Keyword: Co-PET extraction

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A Study on Extraction Condition of Co-PET from PET/Co-PET Sea-Island Type Microfiber Fabric (PET/Co-PET 해도사 직물의 Co-PET 추출 조건에 관한 연구)

  • Park, Myeong Su;Yun, Jong Ho;Jo, Dae Hyeon
    • Textile Coloration and Finishing
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    • v.13 no.2
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    • pp.34-34
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    • 2001
  • In order to make a microfiber fabric with PET/Co-PET Sea-Island Type microfiber, the optimum condition of extraction and elimination of Co-PET from the microfiber was examined. At the same time, the physical property change of the fabric with respect to the change of the relative amount of the Co-PET in the microfiber was also examined to provide a directly applicable data set to the industry. The sample fabric used was warp 75/36(DTY) and weft 0.05d(PET/Co-PET, Sea Island Type Microfiber) twill fabric of 36 separated yarns+40/24(high shrinking yarn) with 130/48 ITY. The data set was made at various NaOH concentrations and steam temperatures with time as a main variable. The physical properties examined were the tensile properties. The results obtained were the tensile properties. The results obtained were 1. For a proper extraction of Co-PET (13.5%)from the microfiber with wet curing, it takes more than 5 min. in 8 and 12% of NaOH solutions but it takes only 3 min. in 18% of NaOH solution at 120℃. 2. For a proper extraction of Co-PET (13.5%) from the microfiber with wet curing, it takes 3∼5 min. in 12 and 14% of NaOH solution and it takes less than 3 min. in 18% of NaOH solution at 130℃. 3. The increasing ratio of WT increased with increasing NaOH concentrations and the equilibrium point reached was 3 min. at 120℃. 4. The WT increasing ratio was greater in 14 and 18% NaOH solutions than in 8 and 12% of NaOH solutions at 130℃. 5. The RT ratio changes at 120℃ in 8 and 12% of NaOH solutions were indifferent from that at 130℃ in 12% of NaOH solution. However, the RT was apparently decreased with increasing NaOH concentration.

A Study on Extraction Condition of Co-PET from PET/Co-PET Sea-Island Type Microfiber Fabric (PET/Co-PET해도사 직물의 Co-PET추출 조건에 관한 연구)

  • 박명수;윤종호;조대현
    • Textile Coloration and Finishing
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    • v.13 no.2
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    • pp.120-127
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    • 2001
  • In order to make a microfiber fabric with PET/Co-PET Sea-Island Type microfiber, the optimum condition of extraction and elimination of Co-PET from the mocrofiber was examined. At the same time, the physical property change of the fabric with respect to the change of the relative amount of the Co-PET in the microfiber was also examined to provide a directly applicable data set to the industry. The sample fabric used was warp 75/36(DTY) and weft 0.05d(PET/Co-PET, Sea Island Type Microfiber) twill fabric of 36 separated yarns+40/24(high shrinking yarn) with 130/48 ITY. The data set was made at various NaOH concentrations and steam temperatures with time as a main variable. The physical properties examined were the tensile properties. The results obtained were the tensile. The results obtained were 1. For a proper extraction of Co-PET (13.5%)from the microfiber with wet curing, it takes more than 5 min. in 8 and 12% of NaOH solutions but it takes only 3 min. in 18% of NaOH solution at 12$0^{\circ}C$. 2. For a proper extraction of Co-PET (13.5%) from the microfiber with wet curing, ti takes 3~5min. in 12 and 14% of NaOH solution and it takes less than 3 min. in 18% of NaOH solution at $130^\circ{C}$. 3. The increasing ratio of WT increased with increasing NaOH concentrations and the equilibrium point reached was 3 min. at $120^\circ{C}$. 4. The WT increasing ratio was greater in 14 and 18% NaOH solutions than in 8 and 12% of NaOH solutions at $130^\circ{C}$5. The RT ratio changes at $120^\circ{C}$ in 8 and 12% of NaOH solutions were indifferent from that at $130^\circ{C}$ in 12% of NaOH solution. However, the RT was apparently decreased with increasing NaOH concentration.

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The Extraction of Co-PET from Non-Woven Fabrics of Nylon/Co-PET Sea-island Type Composite Microfiber

  • Park, Myung-Soo;Yoon, Jong-Ho;Cho, Dae-Hyun
    • Fashion & Textile Research Journal
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    • v.3 no.5
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    • pp.466-472
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    • 2001
  • To find a suitable condition in this process examined, we investigated the main control factors, such as, the NaOH concentrations, such as, the NaOH concentrations, the heat treating times, and the heating temperatures. The resulting mechanical properties of the fabrics also studied. The samples used were Nylon/Co-PET sea-island type composite microfiber (Co-PET content: 35%) non-woven fabric. The conclusions obtained were as follows. 1. For the complete extraction of Co-PET from the sample non-woven fabric in the dry hot air process, $160^{\circ}C$ of air temperature, 15 min. of treatment time, and around 30% of NaOH concentration were required. On the other hand, in the wet hot air process, $140^{\circ}C$ of air temperature, 3.5 min. of treatment time, and around 30% of NaOH concentration were required. 2. The mechanical properties of the continuous processed samples showed that the WT, B, and WC increased with increasing the weight reduction ratio. However, the G, decreased with increasing the weight loss ratio. Note that, particularly in B, it increased drastically when the weight deduction ratios exceeded 30%. 3. As increasing the wet hot air temperature from 130 to $140^{\circ}C$, B appeared to increase, however, WT, G, and WC appeared to decrease. 4. The best condition found in this continuous process to extract Co-PET is the wet hot air temperature of 140, NaOH concentration of 28% or above, and the treatment time 2-4 min.

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Multimodality Image Registration and Fusion using Feature Extraction (특징 추출을 이용한 다중 영상 정합 및 융합 연구)

  • Woo, Sang-Keun;Kim, Jee-Hyun
    • Journal of the Korea Society of Computer and Information
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    • v.12 no.2 s.46
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    • pp.123-130
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    • 2007
  • The aim of this study was to propose a fusion and registration method with heterogeneous small animal acquisition system in small animal in-vivo study. After an intravenous injection of $^{18}F$-FDG through tail vain and 60 min delay for uptake, mouse was placed on an acryl plate with fiducial markers that were made for fusion between small animal PET (microPET R4, Concorde Microsystems, Knoxville TN) and Discovery LS CT images. The acquired emission list-mode data was sorted to temporally framed sinograms and reconstructed using FORE rebining and 2D-OSEM algorithms without correction of attenuation and scatter. After PET imaging, CT images were acquired by mean of a clinical PET/CT with high-resolution mode. The microPET and CT images were fusion and co-registered using the fiducial markers and segmented lung region in both data sets to perform a point-based rigid co-registration. This method improves the quantitative accuracy and interpretation of the tracer.

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Quantitative Extraction Analysis of Brominated Flame Retardant Substances Using Supercritical-Fluid Method for Environmental Assessment (초임계추출법을 이용한 브롬계 난연제 화합물 환경성 평가 추출효율 분석 연구)

  • Oh, Min-Kyung;Yoon, Sang-Hwa;Lee, Young-Kwan;Han, Jae-Sung;Won, Sung-Ho;Nam, Jae-Do
    • Polymer(Korea)
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    • v.32 no.1
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    • pp.13-18
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    • 2008
  • For the evaluation of brominated flame retardants included in polymeric electronic devices, we investigated the extraction methods and solvent systems for four different types of polymers of PC (polycarbonate), PP (polyropylene), PET (poly(ethylene terephthalate)) and PBT (poly(butylene terephthalate)) using different solvent systems of hexane/acetone, THF, toluene, and THF/toluene. In order to compare the extraction efficiency of different methods and solvent systems, the deca-BDE (decabromo diphenyl ether) flame retardant was included in PC, PP, PET and PBT systems and subsequently extracted by soxhlet, ultrasonic, accelerated solvent, microwave and supercritical fluid extraction methods. The amount of the extracted flame retardant was monitored to evaluate the extraction efficiency. The ultrasonic extraction method was found not to be acceptable as an extraction method for the polymer systems mainly due to a low salvation efficiency of the organic solvents. Soxhlet, accelerated solvent and microwave extraction methods exhibited over 80% of extraction efficiency for toluene. The supercritical fluid extraction method, which has been used as an extraction method for flame retardants in polymers, showed the extraction efficiencies of ca. 100% for PC and PP in the optimal extraction conditions of $60^{\circ}C$ and 120 bar.

Co-registration of PET-CT Brain Images using a Gaussian Weighted Distance Map (가우시안 가중치 거리지도를 이용한 PET-CT 뇌 영상정합)

  • Lee, Ho;Hong, Helen;Shin, Yeong-Gil
    • Journal of KIISE:Software and Applications
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    • v.32 no.7
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    • pp.612-624
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    • 2005
  • In this paper, we propose a surface-based registration using a gaussian weighted distance map for PET-CT brain image fusion. Our method is composed of three main steps: the extraction of feature points, the generation of gaussian weighted distance map, and the measure of similarities based on weight. First, we segment head using the inverse region growing and remove noise segmented with head using region growing-based labeling in PET and CT images, respectively. And then, we extract the feature points of the head using sharpening filter. Second, a gaussian weighted distance map is generated from the feature points in CT images. Thus it leads feature points to robustly converge on the optimal location in a large geometrical displacement. Third, weight-based cross-correlation searches for the optimal location using a gaussian weighted distance map of CT images corresponding to the feature points extracted from PET images. In our experiment, we generate software phantom dataset for evaluating accuracy and robustness of our method, and use clinical dataset for computation time and visual inspection. The accuracy test is performed by evaluating root-mean-square-error using arbitrary transformed software phantom dataset. The robustness test is evaluated whether weight-based cross-correlation achieves maximum at optimal location in software phantom dataset with a large geometrical displacement and noise. Experimental results showed that our method gives more accuracy and robust convergence than the conventional surface-based registration.

The development of a fully automated homemade system for [11C] acetate synthesis using an open source PLC

  • Kang, Se Hun;Hong, Sung Tack;Park, Kwangseo;Kim, Seok-ki
    • Journal of Radiopharmaceuticals and Molecular Probes
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    • v.2 no.2
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    • pp.103-107
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    • 2016
  • Solid phase extraction (SPE) purification method is the efficient and well-known tool for automated [$^{11}C$]acetate synthesis. A fully automated homemade module adopting the SPE method and 'pinch' valves was developed very economically with a universal interface board, a relay card and an open source programmable logic controller. The radiochemical yield of the optimized [$^{11}C$]acetate synthesis by this system was $58.8{\pm}2.1%$ (n=10, decay-corrected) from $15.5{\pm}0.19GBq$ of $[^{11}C]CO_2$ as starting activity, and total synthetic time was 15 minutes. HPLC analysis showed its high radiochemical purity as $97.4{\pm}1.1%$ without possible by-products.

Phenolics Content and Browning Capacity during the White Winemaking (백포도주 양조중 페놀류의 함량과 갈변도)

  • Song, Dong-Hun;Kim, Chan-Jo;Rho, Tae-Wook;Lee, Jong-Soo
    • Korean Journal of Food Science and Technology
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    • v.20 no.6
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    • pp.787-793
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    • 1988
  • Juices of Golden Queen, Neo-Muscat and Seibell-9110 were prepared with the addition of $SO_2(100ppm)$ in must and juice, of $SO_2(100ppm)$ and pectinase (40mg/l) in must, respectively and then 300mg/1 of Polyclar AT were added on different white wines from grape juices. Phenolics content in grape juices and white wines were determined. and also changes of browning capacity of white wines during the storage periods at $45^{\circ}C$ were investigated by accelerated method. Extraction of total phenol into grape juices was increased significantly in $SO_2-pectinase$ addition lot and content of total phenol of Seibell-9110 juice was two or three times higher than the others. Yield of grape juices was highest in $SO_2-pectinase$ addition lot. Ethanol content of white wines were 11.4-12.0 v/v% , and total acid, fusel oil and methanol content of Neo-Muscat white wine was lower than that of the other white wines. Total phenol content of white wines was 25-50% lower than that of grape juices and 50-80% lower in colour. Browning capacity of white wines was decreased by 25-40% for 18 days at $45^{\circ}C$ with addition of Polyclar AT, but Seibell-9110 white wine prepared from $SO_2-pectinase$ addition lot was not available commercially because of severe browning.

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