• Journal of Korea Foundry Society
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• v.27 no.4
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• pp.179-183
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• 2007

The TiC layer was formed on Ti and Ti alloys by plasma carburizing method. The main experimental parameters for plasma car boozing were temperature and time. XRD, EDX, hardness test and corrosion test were employed to analyze the evolution and material properties of the layer. The preferred orientation of TiC layers is (220) at treated temperature of $700^{\circ}C\;and\;880^{\circ}C$ However, it is changed to (200) at temperature of $800^{\circ}C$ The thickness of carbide layer increase with increasing carburizing temperature. Highest hardness of hardened layer formed on CP-Ti was obtained at the carburizing condition of processing temperature $880^{\circ}C$ and processing time 1080min. The corrosion potential of carburizing specimen was higher than untreated CP-titanium, and corrosion potential increased as carburizing temperature and time increased. Thus the corrosion resistance of CP-Ti was greatly enhanced after plasma carburizing treatment.

• Journal of the Korean Society for Heat Treatment
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• v.5 no.1
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• pp.32-40
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• 1992

This content is a part of the results of the study on the development of the vacuum carburizing technology. In this study the vacuum carburizing furnace being used was the furnace that developed through the joint project between KIMM and Kyung-Pook Heat Treating Co. from June 1988 to Nov. 1990. And the used carburizing gas was the propane gas and the introducing methods of the gas applied two methods such as pulse and constant pressure. By this study we established the basis of the furnace manufacturing technology and of the processing technology in the vacuum carburizing. Above all in this work there are notable meanings in a viewpoint of the foremost research in home. Hereafter, we are going to industrialize the vacuum carburizing technology by improving the results of the present work and by developing the process for the mass production.

• Korean Journal of Metals and Materials
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• v.46 no.6
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• pp.357-362
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• 2008

The 2-step low temperature plasma processes (the combined carburizing and post-nitriding) were carried out for improving both the surface hardness and corrosion resistance of AISI 316L stainless steel. The effects of processing time and temperature on the surface properties during nitriding step were investigated. The expanded austenite (${\gamma}_N$) was formed on all of the treated surface. The thickness of ${\gamma}_N$ was increased up to about $20{\mu}m$ and the thickness of entire hardened layer was determined to be about $40{\mu}m$. The surface hardness reached up to $1,200HV_{0.1}$ which is about 5 times higher than that of untreated sample ($250HV_{0.1}$). The thickness of ${\gamma}_N$ and concentration of N on the surface were increased with increasing processing time and temperature. The corrosion resistance in 2-step low temperature plasma processed austenitic stainless steels was enhanced more than that in the untreated austenitic stainless steels due to a high concentration of N on the surface.

• Journal of Ocean Engineering and Technology
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• v.25 no.1
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• pp.56-60
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• 2011

A low temperature plasma carburizing process was performed to AISI 304L austenitic stainless steel to achieve the enhancement of surface hardness without a compromise in their corrosion resistance. Attempts were made to investigate the influence of the processing temperatures on the surface-hardened layer during low temperature plasma carburizng in order to obtain the optimum processing conditions. The expanded austenite (${\gamma}C$) was formed on all the treated surfaces. Precipitates of chromium carbides were detected in the hardened layer (C-enriched layer) only for the specimen treated at $500^{\circ}C$. The hardened layer thickness of ${\gamma}C$ increased up to about $35\;{\mu}m$, with increasing treatment temperature. The surface hardness reached about 1000 $HK_{0.05}$, which is about 4 times higher than that of the untreated sample (250 $HK_{0.05}$). Minor loss in corrosion resistance was observed for the specimens treated at temperatures of $310^{\circ}C-450^{\circ}C$ compared with untreated austenitic stainless steel. Particularly, the precipitation of chromium carbides at $500^{\circ}C$ led to a significant decrease in the corrosion resistance.

• Journal of Ocean Engineering and Technology
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• v.25 no.6
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• pp.60-65
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• 2011

A low temperature plasma carburizing process was performed on AISI 316L austenitic stainless steel to achieve an enhancement of the surface hardness without degradation of its corrosion resistance. Attempts were made to investigate the influence of the processing temperatures on the surface hardened layer during low temperature plasma carburizing in order to obtain the optimum processing conditions. The expanded austenite (${\gamma}_c$) phase, which contains a high saturation of carbon (S phase), was formed on all of the treated surfaces. Precipitates of chromium carbides were detected in the hardened layer (C-enriched layer) only for the specimen treated at $550^{\circ}C$. The hardened layer thickness of ${\gamma}_c$ increased up to about $65{\mu}m$ with increasing treatment temperature. The surface hardness reached about 900 $HK_{0.05}$, which is about 4 times higher than that of the untreated sample (250 $HK_{0.05}$). A minor loss in corrosion resistance was observed for the specimens treated at temperatures of $300^{\circ}C{\sim}450^{\circ}C$ compared with untreated austenitic stainless steel. In particular, the precipitation of chromium carbides at $550^{\circ}C$ led to a significant decrease in the corrosion resistance. A diamond-like carbon (DLC) film coating was applied to improve the wear and friction properties of the S phase layer. The DLC film showed a low and stable friction coefficient value of about 0.1 compared with that of the carburized surface (about 0.45). The hardness and corrosion resistance of the S phase layer were further improved by the application of such a DLC film.

• Korean Journal of Heritage: History & Science
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• v.52 no.3
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• pp.240-251
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• 2019

This study examined the manufacturing technology used for the flat iron axes excavated from Ulsan Hadae. Their microstructures were analyzed using metallurgical methods. In addition, a variety of manufacturing technologies were examined and compared using existing research materials on flat iron axes. As a result of analyzing ten flat iron axes, which were excavated in the order that they were laid out in a row in one of the wooden coffin tombs at Ulsan Hadae, Tomb No. 44, it was possible to classify the flat iron axe manufacturing technology and system into three types: 'pure iron - shape processing', 'pure iron - shape processing - carburizing', and 'pure iron - shape processing - carburizing - decarburizing.' All of the flat iron axes were produced by forging, and most of them were made by beating the pure iron into their shapes. In particular, a number of the flat iron axes were reinforced through a carburizing process after shaping the iron. This appears as steel products forming the basis of the steel industry at the time were commonly used as an intermediary material or currency. On the other hand, it was commonly found in all samples that the hardening was not performed after shaping or carburizing. Since the microstructure of the flat iron axes made of pure iron contained a large number of impure inclusions and the result of analyzing the components of the non-metal inclusions showed characteristics of slag which contains a mixture of glass phase and wustite, it is possible that low-temperature reduction was used in the refining process.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.10 no.2
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• pp.84-89
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• 2011

This paper studied the carburizing of chromium molybdenum steel which the heat treatment effect of gear geometric tolerance, OPD, Runout, the surface hardness, the maximum hardness, the core hardness and the bending fatigue strength were investigated. Firstly, the deformation is observed, and the results of circularity, squareness, OPD and Runout of SCM822, SCM425, and SCM415 are obtained in order. Secondly, in order to investigate the gear hardness, the surface hardness, the maximum hardness and the core hardness of SCM822, SCM425, and SCM415 are obtained; and the surface hardness of SCM822 is about 10% higher than SCM415's, and about 3% higher than SCM425's. Thirdly, the fatigue strength of SCM822 is about 10% higher than SCM415's, and about 7% higher than SCM425's in the fatigue test results. At last, for the purpose of the minimum deformation of heat treatment, and also the improvement of fatigue strength, the best gear material is SCM822 in this test.

• Proceedings of the Korean Institute of Surface Engineering Conference
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• 2013.05a
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• pp.92-94
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• 2013

우수한 기계적 강도 및 내식성을 가지고 있는 F51(Duplex Stainless Steel)에 저온 plasma Carburizing처리를 적용하여 온도 및 Ar농도에 따른 표면특성을 조사하였다. 플라즈마 처리된 시편은 표면에 탄소가 과포화된 S-phase 또는 Expanded austenite가 형성되어 미처리 시편에 비해 경도 및 내식성 모두 증가하였다.

• Proceedings of the KSME Conference
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• 2007.05a
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• pp.1601-1606
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• 2007

In order for high strength aluminum alloys to be used in transportation systems and the aerospace industry, excellent mechanical and physical properties are required. In particular, excellent anti-abrasion property is indispensable for parts that require driving force. In general, surface treatment technologies such as high frequency heat treatment, gas solid carburizing, surface rolling, shot peening are used as ways of improving anti-abrasion property. Among various surface treatment technologies, this research chose shot peening processing for Al7075-T6, which is well known as representative high-strength alloy steel. Wear characteristics were compared and analyzed after shot peening processing with shot ball velocities of 40m/s and 70m/s in order to investigate the effects of shot peening processing on wear characteristics.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2003.11a
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• pp.299-306
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• 2003

The SCM420 used mainly to automobile transmission gear has problems that it costs transmission gear maker much money in carburizing treatment. For this, it needs to alternate the existing material and heat treatment to new gear material and surface modification. For this, friction and wear experiment according to sliding speed and applied load was carried out to evaluate the wear resistance of two transmission gear materials with oxidation nitrocarburising and non-oxidation nitrocarburising NT100, The presumed wear volume was calculated with the image processing for evaluation of wear resistance of two transmission gear materials. The results show that the oxidation nitrocarburising has a distinguished wear resistance than non-oxidation nitrocarburising.