• Title/Summary/Keyword: Carbon Arc

검색결과 287건 처리시간 0.028초

용접흄내 중금속분석시 전처리 방법별 효율비교 (A Comparison of Efficiency of Two Pretreatment Methods for Extracting Heavy Metals from Welding Fume Samples)

  • 손두영;김현욱
    • 한국산업보건학회지
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    • 제9권2호
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    • pp.135-144
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    • 1999
  • The purposes of this study were to survey types of pretreatment methods adopted by industrial hygiene laboratories in Korea for extracting heavy metals in welding fume samples and to compare performances of two pretreatment methods, the acid extraction and the microwave digestion, in extracting heavy metals contained in the real workplace samples from various welding jobs including arc, argon, and carbon dioxide. A total of 25 analytical chemists in the industrial hygiene laboratories participating the quality control program directed by the Korea Industrial Safety Corporation were interviewed by telephone. For the purpose of comparing performance of extracting heavy metals from real workplace samples, a total of 53 welders from 21 workplaces located in Anyang, Uiwang, and Kunpo areas were sampled from the period of March 22, 1999 to April 20, 1999. It was found that the most frequently adopted method for samples from the quality control program was the acid extraction method(40%) followed by the NIOSH 7300 method(36%). The NIOSH method, however, was the dominant method(36%) for samples from workplace followed by the acid extraction method(28%). In this study, two extraction methods, the acid extraction and the microwave digestion, were compared in terms of recovery rate, accuracy, and precision for both manganese and chromium. Both methods produced comparable results for the samples prepared for the quality control program. In contrast, concentrations of two heavy metals determined from real workplace samples pretreated with the microwave digestion method were statis tically significantly higher, manganese(166%) and chromium (200%), than those of utilizing the acid extraction method. These findings were consistent regardless of types of welding techniques used. The results of this study clearly show the importance of verifying the analytical performances of extraction methods for heavy metals not only for the samples from the quality control program but also from the real world samples collected from welding jobs.

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Purification of Si using Catalytic CVD

  • 조철기;이경섭;송민우;김영순;신형식
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2009년도 추계학술대회 논문집
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    • pp.383-383
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    • 2009
  • Silicon is commercially prepared by the reaction of high-purity silica with wood, charcoal, and coal, in an electric arc furnace using carbon electrodes, so called the metallurgical refining process, which produces ~98% pure Si (MG-Si). This can be further purified to solar grade silicon (SoG-Si) by various techniques. The most problematic impurity elements are B and P because of their high segregation coefficients. In this study, we explored the possibility of the using Cat-CVD for Si purification. The existing hot-wire CVD was modified to accommodate the catalyzer and the heating source. Mo boat (1.5 cm ${\times}$ 1 cm ${\times}$ 0.2 cm) was used as a heating source. Commercially available Si was purchased from Nilaco corporation (~99% pure). This powder was kept in the Mo-boat and heated to the purification temperature. In addition to the purification by cat-CVD technique, other methods such as thermal CVD, plasma enhanced CVD, vacuum annealing was also tried. It is found that the impurities are reduced to a great extent when treated with cat-CVD method.

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왕겨 연소기(燃燒機)를 이용(利用)한 온수(溫水)보일러 시스템 개발(開發) (I) -실험적(實驗的) 연구(硏究)- (Development of a Hot Water Boiler System with a Rice Hull Furnace)

  • 이용국;박승제;백풍기;노상하
    • Journal of Biosystems Engineering
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    • 제12권4호
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    • pp.31-43
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    • 1987
  • This study was performed to develop a hot water boiler system with small scale automatic rice hull furnace for the multi-purpose use in the farm. For the experiment a prototype hot water boiler system with rice hull furnace was fabricated, which was equipped with automatic hull feeder, igniter and ash removal device. Optimum operational conditions of the prototype: system were analyzed. The results arc summarized as follows. 1. The temperature measured right above the burning surface should be higher than $500^{\circ}C$ combustion. 2. The top zone of the combustion chamber was the most suitable location of the thermocouple to pick up the control temperature for the automatic operation of the rice hull furnace. 3. The content of carbon monoxide in the flue gas was increased with the filling height of burning material but it was less than 0.3 percent in volume in this experiment. When the filling height was expressed as the ratio of rice hull feed rate to the volume of the combustion chamber above the burning surface, the optimum ratio was about $150kg/m^3-h$. 4. The combustion efficiency of the prototype was higher than 95 percent when the feed rate was 1.1 to 2.3 kg/h and moisture content of rice hull was 22.4 percent (w.b.) or less. 5. It was estimated that the optimum operational conditions of the system were 1.3 to 2.0 kg/h in feed rate, 70 to 100 percent in excess air and 500 to $510^{\circ}C$ in control temperature. 6. The efficiency of coil heal exchanger increased with a decrease in feed rate of rice hull. When the rice hull feed rates were 1.1, 1.7 and 2.3 kg/h, the efficiencies of coil heat exchanger were about 34, 30 and 25 percent and heat transfer rates were 5.7, 7.6 and 8.8 MJ/h, respectively. When the flat plate heat exchanger was used in addition to the coil heat exchanger, the efficiency of the heat exchanger system increased to 48 percent.

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만성 성인형 아토피 피부염의 한방 치험 3례 (Three Cases of Chronic Adult Atopic Dermatitis)

  • 구영회;최인화
    • 한방안이비인후피부과학회지
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    • 제15권1호
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    • pp.140-150
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    • 2002
  • Introduction: Atopic dermatitis is chronic eczematous dermatosis which is related strongly to a family history of atopic disease and hereditary disposition. Its threshold of itching is low so that severe itching occurs and causes secondary eczema. Adult atopic dermatitis has mostly severe symptoms and progresses to chronic relapsing. Objective: The purpose of this study was to estimate the efficacy of oriental medical treatment and management on chronic adult atopic dermatitis. Subject: We studied 3 patients who visited Dongguk University Gangnam Oriental Hospital Dept. of Dermatol. with chronic adult atopic dermatitis from August 2001 to April 2002 and were observed for over 4 months. Methods: We treated them with herb-medication, acupuncture, negative therapy, aroma therapy, full spectrum visible ray therapy(by carbon arc) and external application(Jaun-go). We used the SCORAD index to assess the severity of atopic dermatitis. Results: There were 3 patients with chronic adult atopic dermatitis we could check for over 4 months by clinical scoring using the SCORAD system. 1. The grades of the severity of atopic dermatitis were lower only by the oriental medical treatments and management. 2. Intensities of relapse cases were lower then before the oriental medical treatments. 3. The secondary treatment term for relapse cases was shorter then the first treatment term after oriental remedies were used. Conclusion: Considering the above results, more study is needed on the chronic relapse cases with adult atopic dermatitis, the factors of increasing seventy of adult atopic dermatitis, the prognostic factors of adult atopic dermatitis, and the clinical interchange of chronic adult atopic dermatitis between oriental medicine and western medicine.

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Effect of Au-ionic Doping Treatment on SWNT Flexible Transparent Conducting Films

  • 민형섭;정명선;최원국;김상식;이전국
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2012년도 춘계학술발표대회
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    • pp.111.1-111.1
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    • 2012
  • Interest in flexible transparent conducting films (TCFs) has been growing recently mainly due to the demand for electrodes incorporated in flexible or wearable displays in the future. Indium tin oxide (ITO) thin films, which have been traditionally used as the TCFs, have a serious obstacle in TCFs applications. SWNTs are the most appropriate materials for conductive films for displays due to their excellent high mechanical strength and electrical conductivity. In this work, the fabrication by the spraying process of transparent SWNT films and reduction of its sheet resistance on PET substrates is researched Arc-discharge SWNTs were dispersed in deionized water by adding sodium dodecyl sulfate (SDS) as surfactant and sonicated, followed by the centrifugation. The dispersed SWNT was spray-coated on PET substrate and dried on a hotplate. When the spray process was terminated, the TCF was immersed into deionized water to remove the surfactant and then it was dried on hotplate. The TCF film was then was doped with Au-ionic doping treatment, rinsed with deionized water and dried. The surface morphology of TCF was characterized by field emission scanning electron microscopy. The sheet resistance and optical transmission properties of the TCF were measured with a four-point probe method and a UV-visible spectrometry, respectively. This was confirmed and discussed on the XPS and UPS studies. We show that 87 ${\Omega}/{\Box}$ sheet resistances with 81% transmittance at the wavelength of 550nm. The changes in electrical and optical conductivity of SWNT film before and after Au-ionic doping treatments were discussed. The effect of Au-ion treatment on the electronic structure change of SWNT films was investigated by Raman and XPS.

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고압 전력기기에서의 $SF_6$ Gas 사용단계별 배출특성에 관한 연구 ($SF_6$ Emission Characteristics at High Voltage Equipments in use-phase Stage)

  • 박정주;조연행
    • 전기학회논문지
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    • 제57권12호
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    • pp.2199-2201
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    • 2008
  • Sulfur hexafluoride($SF_6$) is a gaseous dielectric used in high voltage electrical equipment such as an insultor or arc quenching medium in the transmission and distribution of electricity. however, $SF_6$ is one of the greenhouse gases(GHG) with a global warming potential that is 23,900 times greater than that of carbon dioxide($CO_2$). for this reason, $SF_6$ emissions in electric equipment shall be controlled to reduce GHG and improve cost-effective use of $SF_6$ for economical benefits. Until recently there has not been any investigation on $SF_6$ emission characteristics and inventory in Korea. To understand emission characteristics during the use-phase, the scope of this study was limited to the following closed pressure system equipment from 10 substations in Korea. This study highlights (1) the investigation of sampling/analysis methodology for $SF_6$ emissions in high voltage equipment, (2) the estimation of $SF_6$ emissions in the use-phase, and (3) the comparison between the emission ratio and the mass-balance applied to inventory study. According to this study, the majority of emissions were related to electric equipment nameplates and the rest of the emissions were related to the handling of $SF_6$ during operations. from this result, emission ratios estimated from this study were similar; GIS was 14% and GCB was 13%, as maintenance process conditions were the same as manual process conditions for both equipment.

유한요소법을 이용한 용접열영향부의 균열진전 및 샤르피 흡수에너지 연구 (Study of Crack Propagation and Absorbed Energy in Heat Affected Zone Using a Finite Element Method)

  • 장윤찬;이영석
    • 한국전산구조공학회논문집
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    • 제22권6호
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    • pp.541-548
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    • 2009
  • 본 논문은 샤르피 충격실험과 유한요소법를 이용하여 노치위치에 따른 파괴거동과 흡수에너지의 영향을 평가하였다. 본 연구자는 쉴드메탈아크 용접방법으로 두께가 25mm인 압력용기용강(SA-516 Gr. 70)을 용접하였고, 이 용접된 평판으로 샤르피 시편을 제작하였다. 샤르피 충격실험에서는 용접열영향부(HAZ)에서 노치위치가 다른 시편이 사용되었다. 그리고 본 연구자는 유한요소법을 이용하여 샤르피 충격실험에서의 균열진전을 모사하였다. 용접열영향부(HAZ)의 기계적 물성을 유한요소해석에 적용하기 위해 HAZ를 2개 영역, 3개 영역 그리고 4개 영역으로 나누었다. 본 연구결과에서는 샤르피 충격실험의 흡수에너지가 노치위치에 의존적이라는 것을 보여주었다. 또한 샤르피 용접시편에서 신뢰성 있는 유한요소해석 결과를 얻기 위해서는 용접열영향부를 적어도 3개 이상의 영역으로 나누어야 한다는 결과를 얻었다.

초고속 카메라와 삼차원 표면 측정기를 이용한 삭마 재료의 정량적 표면 침식 분석 (Quantitative Analysis for Surface Recession of Ablative Materials Using High-speed Camera and 3D Profilometer)

  • 최화영;노경욱;천재희;신의섭
    • 한국항공우주학회지
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    • 제46권9호
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    • pp.735-741
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    • 2018
  • 본 논문에서는 초고속 카메라와 삼차원 표면 측정기를 이용하여 삭마 재료의 표면 침식량을 정량적으로 분석하였다. 대기권 재진입 환경을 모사하기 위해 0.4 MW 아크 가열 풍동을 이용하여 흑연과 탄소/페놀릭 복합재료의 삭마 실험을 수행하였다. 초고속 카메라를 이용하여 실시간 삭마 실험 영상을 획득하고, 이를 분석하여 침식량과 침식률을 산출하였다. 또한, 삼차원 표면 측정기를 이용하여 삭마 전후 시편의 표면 형상을 측정하였으며, 시편의 높이 차이로부터 침식량 분포를 정밀하게 산출하였다. 이를 통해 표면 침식 현상을 종합 분석하는데 있어서 두 측정 결과를 상호 보완하는 것이 유효함을 확인하였다.

Nanocomposite Coating with TiAlN and Amorphous Carbon Phases Synthesized by Reactive Magnetron Sputtering

  • Kim, Bom Sok;Kim, Dong Jun;La, Joung Hyun;Lee, Sang Yong;Lee, Sang Yul
    • 대한금속재료학회지
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    • 제50권11호
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    • pp.801-808
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    • 2012
  • TiAlCN coatings with various C contents were synthesized by unbalanced magnetron sputtering. The characteristics, the crystalline structure, surface morphology, hardness, and friction coefficient of the coatings as a function of the C content were investigated by X-ray diffraction (XRD), atomic force microscopy (AFM), a microhardness tester, and a wear test. In addition, their corrosion behaviors in a deaerated 3.5 wt% NaCl solution at $40^{\circ}C$ were investigated by potentiodynamic polarization tests. The results indicated that the $Ti_{14.9}Al_{15.5}C_{30.7}N_{38.9}$ coating had the highest hardness, elastic modulus, and a plastic deformation resistance of 39 GPa, 359 GPa, and 0.55, respectively, and it also had the lowest friction coefficient of approximately 0.26. Comparative evaluation of the TiAlCN coatings indicated that a wide range of coating properties, especially coating hardness, could be obtained by the synthesis methods and processing variables. The microhardness of the coatings was much higher than that from previously reported coating using similar magnetron sputtering processes. It was almost as high as the microhardness measured from the TiAlCN coatings (~41 GPa) synthesized using an arc ion plating process. The potentiodynamic test showed that the corrosion resistance of the TiAlCN coatings was significantly better than the TiAlN coatings, and their corrosion current density ($i_{corr}$), corrosion potentials ($E_{corr}$) and corrosion rate decreased with an increasing C content in the coatings. The much denser microstructure of the coatings due to the increased amount of amorphous phase with increasing C contents in the coatings could result in the the improved corrosion resistance of the coatings.

한포진에 대한 최근 한의학적 연구 동향 - 국내 학술지를 중심으로 - (An Overview of Korean Medicine Research for Pompholyx - Literature Review based on recently published studies in Korea -)

  • 정종민;오용택;김경한;이명선;송범용;김종욱;육태한
    • 대한예방한의학회지
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    • 제22권3호
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    • pp.61-72
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    • 2018
  • Objectives : This study was conducted to review the research trends in Korean Medicine of pompholyx based on publications in Korea. Methods : Literature published after 2000 were collected using OASIS, NDSL, KISS, and key words searched were "한포진" "발한이상" "pompholyx" "dyshidrotic eczema". Results : 10 case reports and 4 patient studies were selected for study. Conclusions : Korean medicine treatments included acupuncture, pharmacopuncture, venesection therapy, herbal medicine, ointments and carbon arc lamp therapy. The most commonly used diagnostic method for pompholyx was inspection along with pulse diagnosis, abdominal diagnosis, tongue diagnosis, culture test, and KOH smear screening. The most frequently used treatment evaluation method was Likert scale while VAS(Visual Analog Scale) and Visual&Subjective symptoms were each used in 4 studies. Among 29 patients in 14 papers who showed clinical manifestations of pompholyx, there were 15 male patients (52%), 14 female patients (48%), and the male to female ratio showed 1.07:1. Symptoms were improved using Korean Medicine treatments including acupuncture and herbal medicine. Concurrent treatment using special treatments such as pharmacopuncture, jiyang-go, bojungikgi-tang(ex), external applications showed higher treatment effects. Korean medical treatment of pompholyx was effective in all studies, but the lack of numbers of research on Korean medicine of pompholyx was witnessed compared to other diseases such as psoriasis. Also considering the number of patients suffering from pompholyx, further studies should be conducted.