• Title/Summary/Keyword: Capillary method

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The Role of Pulmonary Capillary Pressure in the Oxygen Free Radical-Induced Acute Lung Injury (산소기에 의한 급성 폐손상에서 폐모세혈관압의 역할에 관한 연구)

  • Yoo, Chul-Gyu;Kim, Young-Whan;Han, Sung-Koo;Shim, Young-Soo;Kim, Keun-Youl;Han, Yong-Chol
    • Tuberculosis and Respiratory Diseases
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    • v.39 no.6
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    • pp.474-483
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    • 1992
  • Background: Regardless of its causes, acute lung injury is characterized pathophysiologically by increased pulmonary arterial pressure and the protein-rich edema. Many inflammatory mediators are known to be involved in the pathogenesis of acute lung injury, including oxygen free radicals (OFR). But the changes in pulmonary capillary pressure in the OFR-induced acute lung injury is not clear. While the pulmonary edema characterized by the movement of fluid and solutes is dependent on the pressure gradient and the alveolar-capillary permeability, the role of pulmonary capillary pressure in the development of pulmonary edema is also not well understood. Method: Male Sprague-Dawley rats were divided into 5 groups: normal control (n=5), xanthine/xanthine oxidase (X/XO)-treated group (n=7), catalase-pretreated group (n=5), papaverine-pretreated group (n=7), and indomethacin-pretreated group (n=5). In isolated perfused rat lungs, the sequential changes in pulmonary arterial pressure, pulmonary capillary pressure by double occlusion method, and lung weight as a parameter of pulmonary edema were determined. Results: Pulmonary arterial pressure and pulmonary capillary pressure were increased by X/XO. This increase was significantly attenuated by catalase and papaverine, but indomethacin did not prevent the X/XO-induced increase. Lung weight gain was also observed by X/XO perfusion. It was prevented by catalase. Papaverine did not completely block the increase, but significantly delayed the onset. Indomethacin had no effect on the increase in lung weight. Conclusion: These data suggest that increased pulmonary capillary pressure by OFR may aggravate pulmonary edema in the presence of increased alveolar-capillary permeability and this may not be mediated by cyclooxygenase metabolites.

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Improvement of Motion Accuracy Using Active Controlled Capillary in Hydrostatic Table (능동제어모세관을 이용한 유정압테이블의 운동정도 향상)

  • Park, C.H.;Song, Y.C.;Lee, H.S.
    • Journal of the Korean Society for Precision Engineering
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    • v.14 no.12
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    • pp.114-120
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    • 1997
  • For compensating the error motion of hydrostatic tables, we have introduced a way that the clearance of table is controlled corresponding to the amount of eror with the actively controlled variable capillary, named as ACC. In previous paper, through the basic test, it was confirmed that by the use of ACC, the error motion within 2.7$\mu$ m of a hydrostatic table could be compensated with the resolution of 27nm, 1/100 contollable range, and with the frequency bandwidth of 5.5Hz, structurally. In this paper, we performed practical compensation of the linear and angular motion error of hydrostatic table using ACC. For improving the compensated motion accuracy, iterative control method is put into the control system. The experimental results show that by the simultaneous compensation of error, the linear and angular motion error are improved upto 0.25$\mu$ m and 0.4arcsec, which are about 1/10 and 1/3 of the non-compensated motion errors respectively.

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Volatile Components of Pinenut (잣의 향기성분(香氣成分)에 관한 연구(硏究))

  • Kim, Yong-Kap;Chung, Kyu-Neung;Ishi, Hirosh;Muraki, Shigeru
    • Korean Journal of Food Science and Technology
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    • v.18 no.2
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    • pp.105-109
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    • 1986
  • Volatile components of pinenut were identified. Pinenut was extracted by simultaneous distillation and extraction method after Soxhlet extraction. The odor profile of the extract was very similar to that of pinenut. This extract was then fractionated into four fractions by Preparative TLC. These all fractions were analyzed by a combination of glass capillary gas chromatography (FTD, FID capillary GC) and mass spectrometry. One hundred and nine components, including 26 hydrocarbons,17 esters,16 aldehydes,12 ketones,31 alcohols, 11 bases, 2 acids and 3 miscellaneous components were identified.

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Development of Infiltration Model Considering Temporal Variation of Soil Physical Properties Under Rainfalls (토양의 물리적 특성의 변화를 고려한 강우의 침투모형 개발)

  • 정하우;김성준
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.35 no.3
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    • pp.36-46
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    • 1993
  • The purposes of this study are to develop three-layered Green-Ampt infiltration model considering temporal variation of physical properties of soil and to evaluate the model with field experiment on bare-tilled and soybean-growing soil plots under natural rainfalls. Infiltration tests were conducted on a sandy loam soil. The model has three-layered soil profile including a surface crust, a tilled layer, a subsoil and considers temporal variation of porosity, hydraulic conductivity, capillary pressure head on a tilled layer by natural rainfalls and canopy density variation of crop. Field measurement of porosity, average hydraulic conductivity and average capillary presure head on a tilled layer were conducted by soil sampler and air-entry permeameter at regular intervals-after tillage. It was found that temporal variation of porosity and average hydraulic conductivity might be expressed as a function of cumulative rainfall energy and average capillary pressure head might be expressed as a function of porosity of a tilled soil. The model was calibrated by an optimization technique, Hooke and Jeeves method using hourly surface runoff data. With the calibrated parameters, the model was verified satisfactorily.

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A Study on the Separation and Determination of Organochlorine Pesticides by Capillary Column Gas-liquid Chromatography (모세관 컬럼 기체크로마토그래피에 의한 유기염소제 농약의 분리 정량에 관한 연구)

  • Taek-Jae Kim;Yun-Woo Eo;Young-Sang Kim
    • Journal of the Korean Chemical Society
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    • v.31 no.5
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    • pp.425-433
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    • 1987
  • The separation of 19 organochlorine pesticides was studied by capillary column gas chromatography. The applicability of this method to the fresh rice was investigated. Comparison of the resolution of pesticides by OV-17 and SE-30 capillary columns revealed that OV-17 column (25m ${\times}$ 0.20mm, 0.27${\mu}$m thickness) showed better resolution. The relative standard deviations (RSD) for their retention times and peak areas obtained by splitless injection mode were within 0.16% and 8.2%, respectively. The recoveries of pesticides spiked in fresh rice were mostly over 85% and their RSDS did not exceed 11.4%.

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Fabrication of Microstructures with Nanocomposites by Capillary Effect (모세관법을 이용한 나노 복합재료 마이크로 구조 제작)

  • Han, Soo-Ho;Hwang, Hui-Yun
    • Composites Research
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    • v.31 no.4
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    • pp.171-176
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    • 2018
  • We proposed new and easy fabrication method of micro-nano hierarchical structures for synthetic dry adhesives and conducted feasibility tests of alignment characteristics of nano-materials in the microstructures by capillary effect. Candidates of fabrication conditions were selected based on the degree of cure and viscosity of mixtures of multiwall carbon nanotubes (MWCNTs) and polydimethylsiloxane (PDMS), which were measured with respect to the fabrication conditions. Scanning electron microscopy images of cross sections of MWCNT-PDMS microstructures were analyzed. MWCNT alignment in microstructures was better when fabrication temperature and degree of cure at fabricating start were lower, but areal density of MWCNTs was little affected by fabrication conditions.

Performance Evaluations of a Residential Small Multi-Refrigeration System Considering the Adiabatic Characteristics (단열 특성을 고려한 가정용 소형 멀티 냉동시스템의 성능에 관한 연구)

  • Lee, Moo-Yeon;Lee, Dong-Yeon;Joo, Young-Ju;Kim, Sang-Uk;Kim, Yong-Chan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.31 no.10
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    • pp.868-875
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    • 2007
  • In this paper, performance characteristics of a domestic kim-chi refrigerator are predicted by using the theoretical calculation and experimental method. The objective of this study is to find out the best design points of the refrigeration system and to calculate an adiabatic characteristic with variation to outdoor temperatures. The best design points such as refrigerant charge amount and capillary length were experimentally investigated. And the theoretical calculation is conducted as a function of calculation parameters and outdoor temperatures. According to this study results, the best design points of a refrigeration system with 2 rooms are 95 g of a refrigerant charge amount and 3500 / 3500 mm of capillary lengths and the best design points of a refrigeration system with 3 rooms are 100 g of a refrigerant charge amount and 3000/3000/6000mm of capillary lengths. And the power consumptions of both systems are 13.57 and 18.2 kWh/month. The worst part of heat loss is a front side of a domestic kim-chi refrigerator body.

Determination of Terbutaline Enantiomers in Human Urine by Capillary Electrophoresis Using $Hydroxypropyl-{\beta}-cyclodextrin$ as a Chiral Selector

  • Kim, Kyeong-Ho;Seo, Sang-Hun;Kim, Hyun-Ju;Jeun, Eun-Young;Kang, Jong-Seong;Mar, Woong-Chon;Youm, Jeong-Rok
    • Archives of Pharmacal Research
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    • v.26 no.2
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    • pp.120-123
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    • 2003
  • A method for the determination of terbutaline enantiomers in human urine by capillary elctrophoresis has been developed. Optimum resolution was achieved using 50 mM phosphate buffer, pH 2.5, containing 15 mM of hydroxypropyl-$\beta$-cyclodextrin as a chiral selector. Urine samples were prepared by solid-phase extraction with Sep-pak silica, followed by CE. The assay was linear between 2-250 ng/mL (R = 0.9998 for (S)-(+)-terbutaline and R = 0.9999 for (R)-(-)-terbutaline) and detection limit was 0.8 ng/mL. The intra-day variation ranged between 6.3 and 14.5% in relation to the measured concentration and the inter-day variation was 8.2-20.1%. It has been applied to the determination of (S)-(+)-terbutaline and (R)-(-)-terbutaline in urine from healthy volunteer dosed with racemic terbutaline sulfate.

Multivariate Optimization of a Sulfated- β-Cyclodextrin-Modified Capillary Zone Electrophoretic Method for the Separation of Chiral Arylalcohols

  • Zhang, Yu-Ping;Noh, Hyun-Joo;Choi, Seong-Ho;Ryoo, Jae-Jeong;Lee, kwang-Pill;Ohta, Kazutoku;Fujimoto, Chuzo;Jin, Ji-Ye;Takeuchi, Toyohide
    • Bulletin of the Korean Chemical Society
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    • v.25 no.3
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    • pp.377-381
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    • 2004
  • Chiral separation of aryalcohols such as 1-phenyl-propanol, 1-phenyl-2-proanol, and 2-phenyl-1-propanol by capillary electrophoresis has been optimized using the overlapping resolution mapping (ORM) scheme. Three critical parameters of the electrophoretic media, i.e. phosphate concentration, sulfated ${\beta}$-cyclodextrin (CD) concentration and pH, were chosen for optimization. The working ranges were initially presumed by 7 preexperiments. Further optimization was carried out by another seven experiments within the narrow working ranges. From the final overlapping resolution mapping all peak pairs, the area of maximum separations were located. Using the conditions of a point in this area, we found that the target compounds were a baseline separated within 30 min. The maximum separation conditions of arylalcohols were a chiral selector concentration of 5.4%, a phosphate concentration of 28 mM, and a pH of 5.0.

Capillary Electrochromatography with Liquid Crystal Crown Ether Modified Hybrid Silica Monolith for Analysis of Imidacloprid and Carbendazim in Tomatoes

  • Wang, Mingming;Feng, Rui;Shen, Jing;Chen, Hao;Zeng, Zhaorui
    • Bulletin of the Korean Chemical Society
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    • v.33 no.7
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    • pp.2224-2228
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    • 2012
  • This study describes the ability of capillary electrochromatography (CEC) for the determination of imidacloprid and carbendazim in tomato samples. A novel liquid crystal crown ether modified hybrid silica monolithic column was synthesized, characterized and developed as separation column for the first time. Baseline separation of imidacloprid and carbendazim could be achieved using a mobile phase containing 90% (v/v) 20 mmol/L phosphate buffer (pH 7.0) and 10% (v/v) acetonitrile. The matrix matched calibration curves were linear with correlation coefficient $r^2$ > 0.9998 in the range of 0.20-10.00 mg/L. The limits of detection for imidacloprid and carbendazim were 0.061 and 0.15 mg/kg, respectively, which were below the maximum residue limits established by the European Union as well as Codex Alimentarius. Average recoveries for imidacloprid and carbendazim varied from 101.6-108.0% with relative standard deviations lower than 6.3%. This method was applied to the analysis of tomatoes collected from local markets.