• Title/Summary/Keyword: Capillary method

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A acupuncture therapy literature study on the hemorrhoids and hemorrhoids complicated by anal fistula (치창(痔瘡)과 치루(痔漏)에 대한 침구학적(鍼灸學的) 문헌고찰(文獻考察))

  • Song, Won-sub;Lee, Byung-ryul;Lee, Hyun;Chae, Sang-jin
    • Journal of Acupuncture Research
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    • v.20 no.1
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    • pp.131-143
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    • 2003
  • Objective : The purpose of this study is to arrange the literature about acupuncture therapy on the hemorrhoids and hemorrhoid complicated by anal fistula. Methods : We arrange Huang Di Nei Jing and fifteen kinds of literature about the hemorrhoids and hemorrhoid complicated by anal fistula. Results : 1. The cause of hemorrhoids are overfatigue, overeating, imbalance of stool(const-ipation or diarrhea), uncontrol sexual excess or abstinence, pathgenic factors of wetness, heat, wind, dry, fire, chronical hemorrhoids that has not been treated, and general weakness. 2. Symptom of hemorrhoids is that skin is projected form the nine holes or varicose extension to become hemorrhoid. Hemorrhoids is small nodosity that projected on the anal inter or outer region, and hemorrhoid complicated by anal fistula is pus which comes out form one or some fistula on the anal around inter and outer region. 3. Therapy method of hemorrhoid and hemorrhoid complicated by anal fistula are elimination pathological heat from blood, promote blood flow to remove blood stasis, cold in nature and purge away fire, remove heat form the blood, promote blood flow to remove blood stasis, cold in nature and purge away fire, remove heat from the blood and eliminate dampness, tonify the spleen and replenish Ki, dispel wind and alleviate pain and so forth. Therapy method of hemorrhoid is to give the first consideration to relieve blood: eliminating pathological heat form blood complicated by anal fistula is to tonify the blood first, than after that eliminating pathological heat form blood. About external method are method of fumigation, method of ointment, method of close with medicine, necrotizing method and also operation(injection, bind etc.)was used for treatment. 4. The prescription are Gurgak-hwan, Wypi-hwan, Gunggyi-tang, Jingyochangchul-tang, Jingyobangpung-tang, Mokhyangbinrang-hwan, Ochi-san, Gamihyanso-san, Jojang-hwan, Sinyung-hwan used frequently. 5. food taboo on patient's diet of the hemorrhoid and hemorrhoid complicated by anal fistula are raw grain, cold or dampness food, alcohol, hot food, Singiberis rhizoma recens, Cinnamomi ramulus. 6. Acupuncture therapy on the hemorrhoid and hemorrhoid complicated by anal fistula are, in the first stage eliminating pathological heat form blood and eliminate dampness, and in the long term eliminate dampness, promote and remove meridian energy, remove that form the intestines, dispel channels and collaterals. 7. Acupuncture points at B2, CV1, B58, B36, B56, Sp5, S30, B25, B54, GV1, GV20, L6, B40 used frequently for the acupuncture therapy, and acupuncture point at GV4, GV1, B30, hemorrhoidal point used form moxibustion. Reduction blood at B40 and blue capillary of Sp9 and acupuncture Chungbaek, Ki-gack, Ki-jung, Ki-mun(Dongsh Kihyel) makes the treatment very effective.

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Diffusion Characteristics of Fatty Acid using Supercritical Fluid Chromatographic Method (초임계유체 크로마토그래피를 이용한 지방산의 확산특성 해석)

  • Lee, Seung Bum;Seong, Dae Hyung;Kim, Hyung Su;Hong, In Kwon
    • Applied Chemistry for Engineering
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    • v.7 no.6
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    • pp.1043-1052
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    • 1996
  • Supercritical fluid chromatographic method was recommended as an alternative separation method of fatty acids of the conventional method such as distillation or extraction. Although diffusion characteristics are varied by the carbon numbers and the degree of unsaturation of fatty acids, the quantitative data were so rare that the commercialization of supercritical fluid chromatographic method has been hindered. In this study, diffusion coefficients of fatty acids which are differently unsaturated are measured by CPB method in the range of 308.15K to 328.15K and 13MPa to 17MPa in supercritical carbon dioxide. A decrease in the binary diffusion coefficient was observed with an increase in temperature and pressure. Also, the decrease in the binary diffusion coefficient with increasing fluid density and viscosity. Wilke-Chang equation, Funazukuri empirical equation, and Matthews-Akgerman equation are used to correlate the experimental diffusion coefficients of fatty acids in supercritical carbon dioxide. Among the various theoretical equations, Matthews-Akgerman equation based on RHS theory was suggested as a more successful correlation model with experimental data.

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A Study on Delineation of Groundwater Recharge Rate Using Water-Table Fluctuation and Unsaturate Zone Soil Water Content Model (지하수위 변동 예측 및 비포화대 함수모델을 이용한 지하수 함양율 산정 연구)

  • Cho, Jin-Wook;Park, Eun-Gyu
    • Journal of Soil and Groundwater Environment
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    • v.13 no.1
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    • pp.67-76
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    • 2008
  • In this study, a combined model of a water-table fluctuation and a soil moisture content model is proposed for the estimation of groundwater recharge rate at a given location. To evaluate the model, groundwater level data from 4 monitoring wells (Pohang Yeonil, Pohang Kibuk, Suncheon Oeseo, Hongcheon Hongcheon) of National Groundwater Monitoring Network from 1996 to 2005 and precipitation data of corresponding years are used. From the proposed methodology, the groundwater recharge rates are estimated to be from 0.5 to 61.4% for Hongcheon Hongcheon, from 1.1 to 27.4% for Pohang Yeonil, from 5.1 to 41.4% for Pohang Kibuk, and from 1.1 to 8.3% for Suncheon Oeseo. The magnitude of variation of the estimated recharge rate depends on the soil type observed near the stations. The groundwater fluctuation model used in this study includes precipitation as a unique source of water-table perturbation and there may exist corollary limitations. To improve the applicability of the proposed method, a capillary-water content constitutive model for unsaturated fractured rock media may be considered. The proposed recharge rate delineation method is physically based and uses minimum numbers of assumptions. The method may be used as a better substitute for the previous tools for delineating recharge rate of a location using water-table fluctuation method and contribute to national groundwater management plan. Further research on the spatial interpolation of the method is under progress.

Effects of Hataedock with Douchi on 2,4-dinitrofluorobenzene-induced Atopic Dermatitis-like Skin Lesion in NC/Nga Mice (두시를 이용한 하태독법의 NC/Nga 생쥐에서 DNFB로 유발된 피부손상 완화 효과)

  • Song, Ji-hoon;Ahn, Sang-Hyun;Cheon, Jin-Hong;Park, Sun-young;Kim, Ho-Hyun;Kim, Ki-Bong
    • Journal of Physiology & Pathology in Korean Medicine
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    • v.30 no.2
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    • pp.109-115
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    • 2016
  • Hataedock is a Korean medical treatment that administers herbal extracts orally to newborn infants. This method is used for alleviating harmful heat and excreting fetal wastes by meconium. The purpose of this study was to evaluate anti-inflammatory effect of Hataedock method with Douchi on 2,4-dinitrofluorobenzene (DNFB)-induced atopic dermatitis (AD). The 3-week-old NC/Nga mice were divided into 3 groups: the control group (Ctrl), the AD-induced group (AE), and the Hataedock-treated group (GT). Only the GT group was treated with Hataedock at the 3rd week. After 28 days from Hataedock treatment, we induced AD-like dermatitis to the AE and GT group by DNFB. The effects of Hataedock were evaluated by immunohistochemical method. In the epithelium, PKC-positive reaction of the GT group was decreased by 57%. In the dermal papillae, IL-4-positive reaction was decreased by 34%. In the dermis, the distribution of degranulated mast cells was decreased and substance P-positive reaction was decreased by 49%. In the skin tissue, edema was decreased and MMP-9-positive reaction was decreased by 71%. Tissue damage such as epithelial cell hyperplasia, infiltration of granulocyte and lymphocyte, and capillary distribution were also decreased. The Hataedock method with Douchi maintained skin barrier and inhibited skin-damaging factors via regulating Th2 differentiation. In conclusion, Hataedock has a potential for preventative treatment of AD. Further studies are necessary to investigate the immune-regulating mechanism and verify the safety and efficacy of the Hataedock method.

Development of Analytical Method for Fipronil Residues in Agricultural Commodities Using GC-ECD/MS (GC-ECD/MS를 이용한 농산물 중 Fipronil의 잔류 분석법 개발)

  • Ahn, Kyung-Geun;Kim, Gyeong-Ha;Kim, Gi-Ppeum;Hwang, Young-Sun;Kang, In-Kyu;Lee, Young Deuk;Choung, Myoung-Gun
    • Korean Journal of Environmental Agriculture
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    • v.34 no.4
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    • pp.309-317
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    • 2015
  • BACKGROUND: An analytical method was developed using GC-ECD/MS to precisely determine the residue of fipronil, a phenylpyrazole insecticide used to control a wide range of foliar and soil-borne pests.METHOD AND RESULTS: Fipronil residue was extracted with acetone from representative samples of five raw products which comprised hulled rice, soybean, Kimchi cabbage, green pepper, and apple. The extract was diluted with saline water, and fipronil was partitioned into n-hexane/dichloromethane (20/80, v/v) to remove polar co-extractives in the aqueous phase. Florisil column chromatography was additionally employed for final purification of the extract. Fipronil was separated and quantitated by GC-ECD using a DB-17 capillary column. Accuracy of the proposed method was validated by the recovery from crop samples fortified with fipronil at 3 levels per crop in each triplication.CONCLUSION: Mean recoveries ranged from 86.6% to 106.0% in five representative agricultural commodities. The coefficients of variation were less than 10%. Limit of quantitation of fipronil was 0.004 mg/kg as verified by the recovery experiment. A confirmatory technique using GC/MS with selected-ion monitoring was also provided to clearly identify the suspected residue. Therefore, this analytical method was reproducible and sensitive enough to determine the residue of fipronil in agricultural commodities.

Solvent-free determination of BTEX in water using repetitive membrane extraction followed by GC-MS (반복적인 막 추출과 GC-MS를 이용한 물 중 BTEX의 분석)

  • Kim, He-Kap;Kim, Se-Young;Lee, Soo-Hyung
    • Analytical Science and Technology
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    • v.24 no.5
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    • pp.352-359
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    • 2011
  • An analytical method for solvent-free determination of benzene, toluene, ethylbenzene, and xylenes (BTEX) in water using repetitive membrane extractions coupled to cryofocusing and GC-MS was derived. BTEX compounds that permeated through a nonporous silicone membrane from the aqueous phase and evaporated into the acceptor phase were purged into a cryofocusing trap ($-100^{\circ}C$) with helium gas. The BTEX compounds, thus enriched in the trap, were thermally desorbed into a capillary column GC and detected using an MS. The flow rate of the donor phase (30 mL water) was set at 10 mL/min, and membrane extractions, accomplished by returning the water drained from the extraction module to the sample container, were repeated three times at $20{\pm}2^{\circ}C$. Although recoveries (%) were variable, from the highest for benzene (approximately 80%) to the lowest for ethylbenzene and xylenes (3.5-10%), the method showed satisfactory precision (RSD 2.2-10%) with good-linearity calibration curves ($r^2$ 0.9976-0.9997 in 1-100 ${\mu}g$/L range) for all of the compounds. The method detection limits (MDLs) ranged from 0.16 to 1.8 ${\mu}g$/L. The results showed the method's advantages such as short analysis time and overall simplicity without solvent compared to the conventional techniques.

Development of Analytical Method for Propylene Glycol in Foods (식품 중 프로필렌글리콜의 분석법 개발)

  • Kim, Hee-Yun;Hong, Ki-Hyoung;Choi, Jang-Duck;Park, Sung-Kwan;Jung, Si-Sub;Choi, Woo-Jeong;Lee, Shin-Ho;Moon, Dong-Chul
    • Korean Journal of Food Science and Technology
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    • v.37 no.6
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    • pp.889-892
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    • 2005
  • Standardized method based on extraction, filtration, and gas chromatography (GC) was developed far propylene glycol analysis to set hygienic norm of safety measure for foods under governmental control. Various columns were tested fur propylene glycol analysis by GC with flame ionization detector. Known amount of propylene glycol was spiked into wheat flour dough and analyzed by developed method. Results showed 101.60% recovery rate for propylene glycol with HP-5 column. Reproducibility test of standards recorded 0.30 for standard variation and 0,42% for relative variation. Using analytical method established, contents of propylene glycol in more than hundred different foods were monitored. Propylene glycol was detected in most foods, indicating propylene glycol is not only commonly added during food preparation, but also is contained naturally in food.

Effect of Heat Treatment on the Gas Permeability, Sound Absorption Coefficient, and Sound Transmission Loss of Paulownia tomentosa Wood (참오동나무의 열처리가 기체투과성, 흡음율과 음향투과손실에 미치는 영향)

  • KANG, Chun-Won;JANG, Eun-Suk;JANG, Sang-Sik;Cho, Jae-Ik;KIM, Nam-Hun
    • Journal of the Korean Wood Science and Technology
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    • v.47 no.5
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    • pp.644-654
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    • 2019
  • In this study, the gas permeability, sound absorption coefficient, and sound transmission loss of the Paulownia tomentosa wood were estimated using capillary flow porometry, transfer function method, and transfer matrix method, respectively. The longitudinal specific permeability constant of the Paulownia tomentosa wood with a thickness of 20 mm was 0.254 for the control sample and 0.279, 0.314, and 0.452 after being subjected to heat treatments at $100^{\circ}C$, $160^{\circ}C$, and $200^{\circ}C$, respectively. The gas permeability was observed to be slightly increased by the heat treatment. The mean sound absorption coefficients of 20-mm thick Paulownia tomentosa log cross-section for the control sample and after being subjected to heat treatments at $100^{\circ}C$, $160^{\circ}C$, and $200^{\circ}C$ were 0.101, 0.109, 0.096 and 0.106, respectively. Further, the noise reduction coefficients of 20-mm thick Paulownia tomentosa log cross-section of the control sample and after being subjected to heat treatment at temperatures of $100^{\circ}C$, $160^{\circ}C$, and $200^{\circ}C$ were 0.060, 0.067, 0.062 and 0.071, respectively. The mean of sound transmission loss of the 20-mm thick Paulownia tomentosa log cross-section was approximately 36.93 dB. Furthermore, the gas permeability and sound absorption coefficient of the heat-treated Paulownia tomentosa discs slightly increased depending on the heat treatment temperature; however, the rate of increase was insignificant.

Improvement of Analysis Methods for Fatty Acids in Infant Formula by Gas Chromatography Flame-Ionization Detector (GC-FID를 이용한 조제유류 중 지방산 분석법 개선 연구)

  • Hwang, Keum Hee;Choi, Won Hee;Hu, Soo Jung;Lee, Hye young;Hwang, Kyung Mi
    • Journal of Food Hygiene and Safety
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    • v.36 no.1
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    • pp.34-41
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    • 2021
  • The purpose of this research is to improve analysis methods of determining the contents of fatty acids in infant formulas and follow-up formulas. A gas chromatography (GC) method was performed on a GC system coupled to flame ionization detector, with a fused silica capillary column (SP2560, 100 m×0.25 mm, 0.20 ㎛). The method was validated using standard reference material (SRM, NIST 1849a). Performance parameters for method validation such as specificity, linearity, limits of detection (LOD) and quantification (LOQ), accuracy and precision were examined. The linearity of standard solution with correlation coefficient was higher than 0.999 in the range of 0.1-5 mg/mL. The LOD and LOQ were 0.01-0.06 mg/mL and 0.03-0.2 mg/mL, respectively. The recovery using standard reference material was confirmed and the precision was found to be between 0.8% and 2.9% relative standard deviation (RSD). Optimized methods were applied in sample analysis to verify the reliability. All the tested products had acceptable contents of fatty acids compared with component specification for nutrition labeling. The result of this research will provide efficient experimental information and strengthen the management of nutrients in infant formula and follow-up formula.

Effect of irradiation on the dental pulp tissues in streptozotocin-induced diabetic rats (방사선조사가 당뇨 백서의 치수조직에 미치는 영향)

  • Kang Ho-Duk;Hwang Eui-Hwan;Lee Sang-Rae
    • Imaging Science in Dentistry
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    • v.35 no.1
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    • pp.9-14
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    • 2005
  • Purpose : To observe the histopathological changes in the pulp tissues of mandibular molars in streptozotocin-induced diabetic rats after irradiation. Materials and Methods : The male Sprague-Dawley rats weighing approximately 250 gm were divided into four groups: control, diabetes, irradiation, and diabetes-irradiation groups. Diabetes mellitus was induced in the rats by injecting streptozotocin. Rats in control and irradiation groups were injected with citrate buffer only. After 5 days, the head and neck region of the rats in irradiation and diabetes-irradiation groups were irradiated with a single absorbed dose of 10 Gy. All the rats were sacrificed at 3, 7, 14, 21, and 28 days after irradiation. The specimen including the mandibular molars were sectioned and observed using a histopathological method. Results : In the diabetes group, capillary dilatation was observed. However, there was no obvious morphologic alteration of the odontoblasts. In the irradiation group, generalized necrosis of the dental pulp tissues was observed. Vacuolation of the odontoblasts and dilatation of the capillaries were noted in the early experimental phases. In the diabetes-irradiation group, generalized degeneration of the dental pulp tissues was observed. Vacuolation of the dental pulp cells and the odontoblasts was noted in the late experimental phases. Conclusion : This experiment suggests that dilatation of the capillaries in the dental pulp tissues is induced by diabetic state, and generalized degeneration of the dental pulp tissues is induced by irradiation of the diabetic group.

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