• Title/Summary/Keyword: Calibration Method

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Examination of GC-TD sensitivity for reduced sulfur compounds in relation to temporal stability and reproducibility (환원 황화합물의 열탈착 분석기법에 대한 감도의 경시변화 및 재현성에 대한 연구)

  • Hong, One-Feel;Kim, Ki-Hyun
    • Analytical Science and Technology
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    • v.23 no.1
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    • pp.24-35
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    • 2010
  • To learn more about the calibration properties of reduced sulfur compounds (RSCs) by the combination of gas chromatography(GC)-pulsed flame photometric detector (PFPD) and thermal desorption method, a series of calibration experiments were conducted on the basis of both internal and external calibration approaches. For these experiments, gaseous standards of 4 RSCs ($H_2S$, $CH_3SH$, DMS, and DMDS) were prepared at two different concentration levels of both low (10, 20, 50,and 100 ppb) and high ranges (100, 200, 500, and 1000 ppb) along with $CS_2$ as an internal standard. First, the external calibration results were compared between fixed standard volume (FSV) and fixed standard concentration (FSC) method. Secondly, FSV-based calibration results were compared between external and internal calibration results. As FSV method suffers from sensitivity variations less significantly than FSC, the former is recommended to maintain the consistency in GC-TD sensitivity for RSC analysis. In addition, when the calibration data were examined in terms of RSE between external and internal calibration data, the results were not consistent enough to show improvements in internal method. Hence, diverse efforts are desirable to optimize the reproducibility in terms of GC-TD sensitivity for RSC analysis.

Calibration of Portable Particulate Mattere-Monitoring Device using Web Query and Machine Learning

  • Loh, Byoung Gook;Choi, Gi Heung
    • Safety and Health at Work
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    • v.10 no.4
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    • pp.452-460
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    • 2019
  • Background: Monitoring and control of PM2.5 are being recognized as key to address health issues attributed to PM2.5. Availability of low-cost PM2.5 sensors made it possible to introduce a number of portable PM2.5 monitors based on light scattering to the consumer market at an affordable price. Accuracy of light scatteringe-based PM2.5 monitors significantly depends on the method of calibration. Static calibration curve is used as the most popular calibration method for low-cost PM2.5 sensors particularly because of ease of application. Drawback in this approach is, however, the lack of accuracy. Methods: This study discussed the calibration of a low-cost PM2.5-monitoring device (PMD) to improve the accuracy and reliability for practical use. The proposed method is based on construction of the PM2.5 sensor network using Message Queuing Telemetry Transport (MQTT) protocol and web query of reference measurement data available at government-authorized PM monitoring station (GAMS) in the republic of Korea. Four machine learning (ML) algorithms such as support vector machine, k-nearest neighbors, random forest, and extreme gradient boosting were used as regression models to calibrate the PMD measurements of PM2.5. Performance of each ML algorithm was evaluated using stratified K-fold cross-validation, and a linear regression model was used as a reference. Results: Based on the performance of ML algorithms used, regression of the output of the PMD to PM2.5 concentrations data available from the GAMS through web query was effective. The extreme gradient boosting algorithm showed the best performance with a mean coefficient of determination (R2) of 0.78 and standard error of 5.0 ㎍/㎥, corresponding to 8% increase in R2 and 12% decrease in root mean square error in comparison with the linear regression model. Minimum 100 hours of calibration period was found required to calibrate the PMD to its full capacity. Calibration method proposed poses a limitation on the location of the PMD being in the vicinity of the GAMS. As the number of the PMD participating in the sensor network increases, however, calibrated PMDs can be used as reference devices to nearby PMDs that require calibration, forming a calibration chain through MQTT protocol. Conclusions: Calibration of a low-cost PMD, which is based on construction of PM2.5 sensor network using MQTT protocol and web query of reference measurement data available at a GAMS, significantly improves the accuracy and reliability of a PMD, thereby making practical use of the low-cost PMD possible.

Safety factor calibration for bridge concrete girders

  • Silva, Rita C.;Cremona, Christian
    • Structural Engineering and Mechanics
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    • v.49 no.2
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    • pp.163-182
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    • 2014
  • Safety factors proposed in codes CEB, B.A.E.L 91 and EUROCODE 1 cover a great number of uncertainties; making them inadequate for the assessment of existing structures. Suitable safety factors are established using a probabilistic assessment, once real dimensions, materials strength and existing structures deterioration mechanisms are taken into account. This paper presents a calibration method for safety factors using a typical set of RC bridges in France. It considers the principal stages of corrosion provoked by $CO_2$ and $Cl^-$ penetration and threshold indexes (${\beta}_0$) for existing structures. Reliability indexes are determined by the FORM method in the calibration method.

Accurate Calibration of Odometry Errors for Wheeled Mobile Robots by using Experimental Orientation Errors (차륜형 이동로봇의 방향각오차를 이용한 오도메트리 정밀보정기법)

  • Jung, Changbae;Jung, Daun;Chung, Woojin
    • Journal of the Korean Society for Precision Engineering
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    • v.31 no.4
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    • pp.319-326
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    • 2014
  • Accurate estimation of the robot's position has an important role in autonomous navigation. Odometry is one of the most widely used techniques for mobile robot positioning. However, odometry has a well-known drawback that the position errors are accumulated when the travel distance increases. The UMBmark method is the conventional odometry calibration scheme for two wheel differential mobile robots. In the UMBmark method, the approximations for small angles are used in order to simplify the calculations. In this paper, we propose the new calibration scheme by using experimental orientation errors. Kinematic parameters can be calculated accurately without approximations by using experimental orientation errors. The numerical simulation and experimental results show that the odometry accuracy can be improved by the proposed method.

Auto Calibration and Simulation Method for a Strain Gage Type Transducer/Signal Conditioner (스트레인 게이지형 센서 신호조정기 자동교정 및 시뮬레이션 기법)

  • 유제택
    • Journal of Institute of Control, Robotics and Systems
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    • v.9 no.12
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    • pp.1019-1025
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    • 2003
  • We introduce a new auto-calibration/simulation method for a strain gage type transducer/signal-conditioner which guarantees the output linearity and compensates the error automatically. We design a micro voltage supply which is able to interface either AC or DC type excitation voltage. A new strain gage simulator is also designed. We make linearity output of the signal conditioner and can compensate error automatically with this new auto calibration/simulation method. The experimental results show that the error between the real value and the expected one is less than 1%.

FLUX CALIBRATION METHOD OF SLIT SPECTROMETER FOR EXTENDED SOURCES

  • Lee, Sung-Ho;Park, Soo-Jong
    • Journal of The Korean Astronomical Society
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    • v.39 no.4
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    • pp.151-155
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    • 2006
  • Long slit spectrometers are widely used in optical and infrared bands in astronomy. Absolute flux calibration for extended sources, however, is not straightforward, because a portion of the radiation energy from a flux calibration star is blocked by the narrow slit width. Assuming that the point spread function(PSF) of the star is circularly symmetric, we develop a robust method to extrapolate the detected stellar flux to the unobscured flux using the measured PSF along the slit-length direction. We apply this method to our long slit data and prove that the uncertainty of the absolute flux calibration is less than a few percents.

Semiquantitative Analysis of metal for Cigarette Product by Inductively Coupled Plasma Mass Spectrometry (유도결합 플라스마 질량분석기를 이용한 담배 제품의 무기물 반정량 분석)

  • Cho, Sung-Eel;Kim, Hyo-Keun;Hwang, Keon-Joong
    • Journal of the Korean Society of Tobacco Science
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    • v.31 no.2
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    • pp.95-106
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    • 2009
  • Semiquantitative analysis by ICP-MS has proven to be a powerful tool for fast screening, in addition, it does not require the element of interest to be present in the calibration standard, making it especially useful for the analysis of unknown samples. In this study, seven cigarette samples were analyzed by the rapid semi-quantitative analysis method based on the ICP-MS. For each cigarette sample, cut tobacco, cigarette paper, filter (before and after smoking), and smoke condensate were analyzed. The accuracy of the analysis technique was evaluated by comparing results obtained from Calibration Check Standard(CCS) and calibration method. Relative Percentage Error(RPE) value of all elements measured for three CCS showed a stable result of less than ${\pm}20%$. Compared to full quantitative analysis by calibration method, the results for cigarette samples showed average error within ${\pm}15%$.

The Structured Grid Calibration Based On Triangulation Method (삼각법을 기반으로 한 구조화된 격자 캘리브레이션)

  • KIM EUN-SEOK;JOO KI-SEE;WANG GI-NAM
    • Proceedings of the Korean Operations and Management Science Society Conference
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    • 2002.05a
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    • pp.248-252
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    • 2002
  • Many sensors such as a structured grid pattern generator, a laser, and CCD camera to information have been used, but most of algorithms for a calibration are inefficient memory and experiment data are required. In this paper, the calibration algorithm of a structured grid pattern based on triang is introduced to calculate 3D information in the real world. The beams generated from str pattern generator established horizontally with the CCD camera are projected on the calibn CCD camera observes the intersection plane of a light and an object plane. The 3D infon calculated using observed and calibration data. This proposed method in this paper has advantages such as a memory saving and an experimental data since the 3D information are obtained simply triangulation method.

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Study on Kinematic Calibration Method of Stewart Platforms (스튜어트 플랫폼의 기구학적 교정기법에 관한 연구)

  • Goo, Sang-Hwa;Son, Kwon
    • Journal of Institute of Control, Robotics and Systems
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    • v.7 no.2
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    • pp.168-172
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    • 2001
  • The accuracy problem of robot manipulators has long been one of the principal concerns in robot design and control. A practical and economical way of enhancing the manipulator accuracy, without affecting its hardware, is kinematic calibration. In this paper an effective and practical method is presented for kinematic calibration of Stewart platforms. In our method differential errors in kinematical parameters are linearly related to differential errors in the platform pose, expressed through the forward kinematics. The algorithm is tested using simulated measurement in which measurement noise is included.

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Real Time Relative Radiometric Calibration Processing of Short Wave Infra-Red Sensor for Hyper Spectral Imager

  • Yang, Jeong-Gyu;Park, Hee-Duk
    • Journal of the Korea Society of Computer and Information
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    • v.21 no.11
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    • pp.1-7
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    • 2016
  • In this paper, we proposed real-time relative radiometric calibration processing method for SWIR(Short Wavelength Infra-Red) sensor using 'Hyper-Spectral Imager'. Until now domestic research for Hyper-Spectral Imager has been performing with foreign sensor device. So we have been studying hyper spectral sensor device to meet domestic requirement, especially military purpose. To improve detection & identify capability in 'Hyper-Spectral Imager', it is necessary to expend sensing wavelength from visual and NIR(Near Infra-Red) to SWIR. We aimed to design real-time processor for SWIR sensor which can control the sensor ROIC(Read-Out IC) and process calibrate the image. To build Hyper-Spectral sensor device, we will review the SWIR sensor and its signal processing board. And we will analyze relative radiometric calibration processing method and result. We will explain several SWIR sensors, our target sensor and its control method, steps for acquisition of reference images and processing result.