• YAKHAK HOEJI
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• v.60 no.3
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• pp.112-117
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• 2016

A liquid chromatography-tandem mass spectrometry (LC-MS/MS) method was developed and validated for the determination of caffeine in forensic aqueous sample. The centrifuged sample ($100{\mu}l$) was diluted 50-fold with distilled water. The diluted sample ($400{\mu}l$) was then diluted further with $200{\mu}l$ of 0.1% formic acid solution and $400{\mu}l$ of acetonitrile containing 500 ng of caffeine-(3-methyl-$^{13}C_3$) prior to LC-MS/MS analysis. The mobile phase was composed of 0.1% formic acid in distilled water (A) and acetonitrile (B). Chromatographic separation was performed by using a Zorbax SB-C18 ($100mm{\times}2.1mm$ i.d., $3.5{\mu}m$) column and caffeine was eluted within 1.1 min. Linear least-squares regression with a 1/x weighting factor was used to generate a calibration curve with the coefficients of determination ($r^2=0.9983$). The lower limit of quantification was $25ng/ml$ for the analyte. The process efficiency was 98.6~100.1%. Intra- and inter-day precisions were not more than 2.1% and 1.7%, while intra- and inter-day accuracies were ranged from -6.8 to 4.5%, respectively. The suitability of the method was examined by analyzing unknown forensic aqueous samples.

• The Bulletin of The Korean Astronomical Society
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• v.39 no.1
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• pp.54.2-54.2
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• 2014

IGRINS (Immersion GRating Infrared Spectrograph) is a high spectral resolution near-infrared spectrograph that has been developed in a collaboration between the Korea Astronomy & Space Science Institute and the University of Texas at Austin. By using a silicon immersion echelle grating, the size of the fore optics is reduced by a factor of three times and we can make a more compact instrument. One exposure covers the whole of the H- and K-band spectrum with R=40,000. While the operation of and data reduction for this instrument is relatively simple compared to other grating spectrographs, we still need to operate three infrared arrays, cryostat sensors, calibration lamp units, and the telescope during astronomical observations. The IGRINS Instrument Control Software consists of a Housekeeping Package (HKP), Slit Camera Package (SCP), Data Taking Package (DTP), and Quick Look Package (QLP). The SCP will do auto guiding using a center finding algorithm. The DTP will take the echellogram images of the H and K bands, and the QLP will confirm fast processing of data. We will have a commissioning observations in 2014 March. In this poster, we present the performance of the software during the test observations.

• Journal of the Korean GEO-environmental Society
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• v.13 no.6
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• pp.73-81
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• 2012

Safety issue for offshore wind-turbine foundation becomes a crucial factor as offshore wind turbines have been scaled up. Correspondingly, there is a demand to understand the effect of soil-structure interaction on to system behavior in geotechnical engineering point of view. The p-y curve method researched in past few decades is one of the most appropriate methodology to analyze the problem. In this study, recently proposed p-y curve models for various rocks are calibrated to analyze the engineering characteristics of seabed of Jeju Island where it is known to be most suitable area for offshore wind energy farm. Step by step calibration process for p-y models is presented. Analysis results show that subgrade reaction generally increases as closer to seabed. It is also shown that the behavioral characteristics of foundation reflect well rock properties in terms of resultant moment, shear force, etc.

• Journal of Ocean Engineering and Technology
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• v.29 no.2
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• pp.169-174
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• 2015

This paper addresses experimental methodologies to measure the temperature-dependent thermal conductivity of the insulation materials popularly used for LNG cargo containment systems. The measurement techniques considered in this paper are the guarded hot plate (GHP) method and heat flow method (HFM). The former is based on the power supplied to the hot plate to keep the temperature constant, and the latter is based on a direct heat flux measurement. In order to improve the accuracy of the HFM, the thermal conductivity obtained by GHP was cross-compared with the HFM results, and a calibration factor was derived. It was found that the thermal conductivities measured by the two methods corresponded well under room temperature, but the deviation tended to slightly increase as the temperature decreased. Because of the easy installation and operability of HFM, it can be used to measure thermal conductivity in a large scale mock-up test or unit insulation panel test, where the GHP method is difficult to apply.

• The KIPS Transactions:PartB
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• v.14B no.3 s.113
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• pp.163-170
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• 2007

In autonomous navigation of a mobile vehicle or a mobile robot, localization calculated from recognizing its environment is most important factor. Generally, we can determine position and pose of a camera equipped mobile vehicle or mobile robot using INS and GPS but, in this case, we must use enough known ground landmark for accurate localization. hi contrast with homography method to calculate position and pose of a camera by only using the relation of two dimensional feature point between two frames, in this paper, we propose a method to calculate the position and the pose of a camera using relation between the location to predict through perspective transform of 3D feature points obtained by overlaying 3D model with previous frame using GPS and INS input and the location of corresponding feature point calculated using KLT tracking method in current frame. For the purpose of the performance evaluation, we use wireless-controlled vehicle mounted CCD camera, GPS and INS, and performed the test to calculate the location and the rotation angle of the camera with the video sequence stream obtained at 15Hz frame rate.

• Journal of the HCI Society of Korea
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• v.13 no.3
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• pp.65-73
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• 2018

Game balance settings are crucial to game design. Game balancing must take into account a large amount of numerical values, configuration data, and the relationship between elements. Once released and served, a game - even for a balanced game - often requires calibration according to the game player's preference. To achieve sustainability, game balance needs adjustment while allowing for small changes. In fact, from the producers' standpoint, game balance issue is a critical success factor in game production. Therefore, they often invest much time and capital in game design. However, if such a costly game cannot provide players with an appropriate level of difficulty, the game is more likely to fail. On the contrary, if the game successfully identifies the game players' propensity and performs self-balancing to provide appropriate difficulty levels, this will significantly reduce the likelihood of game failure, while at the same time increasing the lifecycle of the game. Accordingly, if a novel technology for game balancing is developed using artificial intelligence (AI) that offers personalized, intelligent, and customized service to individual game players, it would bring significant changes to the game production system.

• Analytical Science and Technology
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• v.13 no.1
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• pp.27-33
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• 2000

Simultaneous separation and analysis of Ni(II), Pd(II), Co(II), Cu(II) and Hg(II) in peperidinedithiocarbamate (PDTC) chelates were investigated by reversed phase liquid chromatography. The optimum conditions for the separation of PDTC metal chelates were examined with respect to the pH, extraction solvent, and mobile phase strength on Novapak $C_{18}$ column using methanol/water mixture as mobile phase. All metal PDTC chelates were eluted in an acceptable range of capacity factor value ($0{\leq}log\;k^{\prime}{\leq}1$). The linear calibration curves were obtained in the concentration range of $0{\sim}1.2{\mu}g/mL$ for five metal ions, and also good precision in the range of 1.96~3.41% RSD was obseved. Under the optimum conditions, trace metat ions in the composite water sample were successfully separated and determined with relative error of ${\pm}2.0%$.

• Analytical Science and Technology
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• v.17 no.1
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• pp.45-52
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• 2004

Determination of some PAHs in sediments at Ulsan bay has been carried out by extraction of the components into n-hexane followed by synchronous spectrofluorimetric technique. 11 PAHs, such as acenaphthene (Ace), anthracene (Anth), benz(a)anthracene (BaA), benzo(b)fluoranthene (BbFt), benzo(k)fluoranthene (BkFt) benzo(a)pyrene (BaP), chrysene (Chry), phenanthrene (Phen), fluoranthene(Ft), perlyrene (Per), and pyrene (Pyr) in sediment samples were able to determine separately by synchronous spectrofluorimetry. Calibration curves for those components were linear for the concentration range of 0.15~166 ppb PAHs with the correlation factor of 0.9985~0.9999. The total amount of PAHs in sediments varied from 68.8 to 324.4 ng/g. The PAHs concentration was shown a tendency to increase from the outer bay to the inner basin as well the predominant contributors to the aromatic ring groups of the PAHs was 4-ring group.

• Korean Journal of Pharmacognosy
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• v.46 no.2
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• pp.160-166
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• 2015

Yijung-tang (YJT) is a traditional herbal formula comprising 4 medicinal herbs. In the present study, we performed the simultaneous analysis for three compounds of YJT and examined anti-allergic effects in vitro. The column for separation of three compounds was used Gemini C18 column and maintained at 40$^{\circ}C$. The mobile phase for gradient elution consisted of two solvent systems. To evaluate Th2 chemokines, YJT was treated into tumor necrosis factor (TNF)-${\alpha}$ and interferon (IFN)-${\gamma}$-stimulated HaCaT cells, and performed ELISA for thymus and activation regulated chemokine (TARC) and regulated on activation, normal T-cell expressed and secreted (RANTES). To measure Th2 cytokines, YJT was added into primary mouse splenocytes, and performed ELISA for interleukin (IL)-4, 5, 13. Calibration curves were acquired with r² >0.9999. The contents of liquiritin, glycyrrhizin, and 6-gingerol in YJT were 4.50 mg/g, 11.10 mg/g, and 1.33 mg/g, respectively. YJT inhibited production of TARC and RANTES in TNF-${\alpha}$ and IFN-${\gamma}$-treated HaCaT cells. YJT also reduced production of IL-4, 5, and 13 in primary mouse splenocytes. In conclusion, our data will be a valuable information to improve quality control and anti-allergic effects of YJT.

• Journal of the Korean Society for Nondestructive Testing
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• v.24 no.4
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• pp.315-324
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• 2004

In eddy current testing(ECT), differential probes have been frequently used since they .an reduce the number of parameters that influence ECT signals. However, differential signal is actually the difference of the two coils' impedance so that signal prediction and interpretation are not easy, On the other hand, absolute coil signal is rather straightforward to predict and analyze. Therefore, combined use of the two types of signals would increase the test reliability. In this paper, absolute coil signals from Inconel plate and tubes are predicted by the finite element analysis and efforts of lift-off, fill-factor, conductivity, operating frequency, test specimen thickness, inner diameter defects, and outer diameter defects are investigated. As a result, various impedance plane diagrams are drawn and analyzed. Significant practical knowldege about absolute signals is accumulated and similar characteristics of the two types of signal could be understood. Finally, slope angle versus defect depth calibration corves are prepared for three different frequencies.