• Journal of Welding and Joining
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• 제32권5호
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• pp.7-12
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• 2014

In this study, API-X100 steel pipes were welded with various kinds of welding wires in the laser-arc hybrid welding process. 10kW fiber laser source was combined to MIG arc welding process. API X-100 steel of base metal was of 16.9mm thickness, and butt welding applied. After welding, full penetration weld was acquired by 1-pass welding. A root porosity and the lack of fusion was observed in some welding conditions. By the mixing the melted wire, acicular ferrite, polygonal ferrite, pro-eutectoid, aligned side plate, and bainite structures were observed at the weld metal. From the observation of hybrid weld, unmixed zone had more Ni and Cr. The unmixed zone was a 1/3 area of the weld metal. As the mechanical test of the hybrid welding, tensile test and impact test applied. From the tensile test, all of the welding except SM70S was fractured at the base metal. The result of the impact test at -30 degree C led 60J~320J of the absorbed energy. The result of the low-absorbed energy might be from the coarse equiaxed structures of the weld metal.

• Steel and Composite Structures
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• 제25권5호
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• pp.571-579
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• 2017

The grid structure with bolt-sphere joints is widely adopted by industrial plants with suspending crane. The alternating reciprocating action of the suspending crane will cause fatigue problems of the grid structure with bolt-sphere joints with respect to the rod, the cone, the sealing plate, the bolt ball and the high strength bolt; while the fatigue of the high strength bolt is the key issue of fatigue failure. Based on efficient and smooth loading equipment with the AMSLER fatigue testing machine, this paper conducted a constant amplitude fatigue test on 18 M20 and 14 M30 high strength bolts with 40Cr material, and obtained 19 valid failure points, 9 unspoiled points with more than 2 million cycles, and 4 abnormal failure points. In addition, it established the constant amplitude fatigue design method, ${[{\Delta}{\sigma}]_{{2{\times}10}}{^6=58.91MPa}$, and analyzed the stress concentration and the fatigue fracture of high strength bolts. It can be explained that the geometrical stress concentration of high-strength bolt caused by spiral burr is severe.

• Applied Microscopy
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• 제1권1호
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• pp.11-17
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• 1969

Conidio spores of Aspergillus niger (strain No. NRRL 330) cultured on potato dextrose agar media were studied by electron microscopy, using the thin sectioning techniques. Conidio spores to be sectioned were fixed by triple methods with $K_2Cr_2O_7$, Glutaraldehyde and $OsO_4$. After dehydrated with alcohol, the specimens were embedded in metacrylate and epon resin media, and thinly sectioned by Porter-Blum MT-2. After sectioned these specimens were negative-stained with uranyl acetate and observed. by Hitachi HS-6 electron microscope. The results of this experiment were summarized as follows. 1. The structures of spore ,wall system seem to be formed 4 layers; exosporium, basal layer, spore coat and unit cell membrane. The protuberance of spore surface that was looked like hair appears to be protrusived from the basal layer. 2. The 3 layers of unit cell membrane was constituted outer layer membrane, inner layer membrane and inter-mediate light layer. 3. The structures of intra cytoplasmic membrane appear as spiral form which was consisted of 3 layers membrane system; outer membrane, inner membrane, and intermediate layer, which has pits. 4. The cement substance of spore coat and cortex may be changed quantitatively by physiological state in cell. 5. In some cases, we observed that the ribosome was transformed into poly ribosome group, and the storage materials and the protein crystals were changed variously. It. has been suggested that the morphological change of some cytoplasmic materials may be caused by some specialized function of the physiological stage.

• Steel and Composite Structures
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• 제33권3호
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• pp.433-444
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• 2019

Fatigue failure of a grid structure using bolt-sphere joints is liable to occur in a high-strength bolt due to the alternating and reciprocal actions of a suspension crane. In this study, variable amplitude fatigue tests were carried out on 20 40 Cr steel alloy M30 high-strength bolts using an MTS fatigue testing machine, and four cyclic stress amplitude loading patterns, Low-High, High-Low, Low-High-Low, and High-Low-High, were tested. The scanning electron microscope images of bolt fatigue failure due to variable amplitude stress were obtained, and the fractographic analysis of fatigue fractures was performed to investigate the fatigue failure mechanisms. Based on the available data from the constant amplitude fatigue tests, the variable amplitude fatigue life of an M30 high-strength bolt in a bolt-sphere joint was estimated using both Miner's rule and the Corten-Dolan model. Since both cumulative damage models gave similar predictions, Miner's rule is suggested for estimating the variable-amplitude fatigue life of M30 high-strength bolts in a grid structure with bolt-sphere joints; the S-N fatigue curve of the M30 high-strength bolts under variable amplitude loading was derived using equivalent stress amplitude as a design parameter.

• 청정기술
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• 제17권4호
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• pp.314-324
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• 2011

아마이드 유도체는 방청성능 및 윤활성능이 우수하여 금속가공유 및 유압작동유등의 첨가제로 많이 사용되고 있다. 본 연구에서는 광유계 윤활기유의 방청제로 사용하기 위하여 알킬 무수 숙신산과 여러 가지 아민과의 링개환 반응을 행하여 카르복실 그룹과 아마이드 그룹을 동시에 포함하는 숙신산 알킬 하프-아마이드 유도체들을 97% 이상의 수율로 합성하였으며 합성구조에 따라 1 중량% 농도범위에서 광유계 오일에 용해되었다. 합성 유도체의 구조는 $^1H$-NMR 및 FT-IR 스펙트럼으로 행하였으며 GC 크로마토그램을 통하여 화합물의 순도를 확인하였다. 또한, 합성 유도체의 해수에 대한 방청성능을 ASTM D665 표준방법과 무게 중량법으로 평가한 결과, 합성 유도체의 농도가 증가하고 알킬기의 사슬이 짧고 2차 아민으로 합성한 숙신산 알킬 하프-아마이드의 방청성능이 1차 아민으로 합성한 유도체보다 상대적으로 방청성능이 우수하였다. 무게 중량법으로 평가한 방청효율% (IE%)는 알킬기의 사슬이 짧을수록 우수한 방청효율을 나타내었으며 구조에 따라 방청효율에 차이를 나타내었다. 40 ppm 농도를 첨가한 오일의 IE%는 최고 93% 이상이었다. 또한, 발청속도(Corrosion Rate, CR)는 알킬기의 사슬이 짧을수록 낮은 값을 나타내어 합성 유도체 40 ppm 농도를 첨가한 오일의 CR 값은 최고 0.5 mm/year 이하로 나타났다.

• 콘크리트학회논문집
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• 제23권3호
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• pp.265-272
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• 2011

콘크리트는 건축물을 구성하는 가장 중요한 재료이지만, 단순한 색상에 의해서 도시 경관을 손상시키는 주요 요인으로 인식되어 왔다. 콘크리트의 이러한 제한점을 개선하기 위하여 안료를 사용하거나 페인팅의 방법에 의해 다양한 색상을 구현하고 있지만, 안료의 사용은 비용 상승을 유발하고 페인트의 경우에는 내구적인 피막을 얻는 것이 어렵다. 최근 콘크리트의 컬러화 방안으로서 착색용 산화제를 사용하는 것이 제안되고 있지만, 사용한 경험이 부족하여 안정적 사용을 위한 체계적인 연구가 필요한 실정이다. 착색용 산화제는 금속이온을 함유한 산성계열의 용액으로 콘크리트 부재에 도포하여 색상을 구현한다. 용액은 Cl성분을 바탕으로 갈색은 Fe, 흑색은 Mn과 Cr, 녹색은 Cu, 적색은 Fe와 Cr이 함유되어 있다. 착색용 산화제는 일시적인 도포로 매우 얇은 착색층을 형성시켜 컬러를 구현하는 것으로, 비교적 용이하게 색상을 구현하는 것이 가능하다. 이 연구는 착색용 산화제를 모르타르 표면에 도포하여 구현된 색상의 특성과 색상을 나타내는 피막의 미세 구조 및 화학적 조성을 검토하였다. 색상은 자연스러운 얼룩의 형태이다. 표면의 변화는 육안으로 확인할 수 없었지만, 미세 구조는 거칠어 졌으며 수화 생성물의 결정인 수산화칼슘과 C-S-H 겔을 관찰할 수 있었다. 표면 거칠기는 산술 평균 거칠기와 단면 굴곡 모두 동일하게 증가하였다. 표면경도는 도포하지 않은 경우와 비교하여 유사하거나 높다. pH는 모르타르에 대해 약 10% 저하된다. 화학적 구성은 모르타르의 원소인 Ca, Si, Al은 감소하고, 시멘트에 함유되어 있지 않는 Mn, Cr, Cu가 생성되고, Fe와 알칼리 원소인 K 및 Na는 증가하는 것으로 나타났다.

• 한국해양공학회지
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• 제35권5호
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• pp.327-335
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• 2021

Microcracks can rapidly grow and develop in high-strength steels used in offshore structures. It is important to render these microcracks harmless to ensure the safety and reliability of offshore structures. Here, the dependence of the aspect ratio (As) of the maximum depth of harmless crack (a_hlm) was evaluated under three different conditions considering the threshold stress intensity factor (Δk_th) and residual stress of offshore structural steel F690. The threshold stress intensity factor and fatigue limit of fatigue crack propagation, dependent on crack dimensions, were evaluated using Ando's equation, which considers the plastic behavior of fatigue and the stress ratio. a_hlm by peening was analyzed using the relationship between Δk_th obtained by Ando's equation and Δk_th obtained by the sum of applied stress and residual stress. The plate specimen had a width 2W = 12 mm and thickness t = 20 mm, and four value of As were considered: 1.0, 0.6, 0.3, and 0.1. The a_hlm was larger as the compressive residual stress distribution increased. Additionally, an increase in the values of As and Δk_th(l) led to a larger a_hlm. With a safety factor (N) of 2.0, the long-term safety and reliability of structures constructed using F690 can be secured with needle peening. It is necessary to apply a more sensitive non-destructive inspection technique as a non-destructive inspection method for crack detection could not be used to observe fatigue cracks that reduced the fatigue limit of smooth specimens by 50% in the three types of residual stresses considered. The usefulness of non-destructive inspection and non-damaging techniques was reviewed based on the relationship between a_hlm, a_NDI (minimum crack depth detectable in non-destructive inspection), a_{cr N} (crack depth that reduces the fatigue limit to 1/N), and As.

• 제어로봇시스템학회논문지
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• 제10권7호
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• pp.604-610
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• 2004

Ultraviolet-nanoimprint lithography (UV-NIL) is a promising method for cost-effectively defining nanoscale structures at room temperature and low pressure. Since the resolution of transferred nanostructures depends strongly upon that of nanostamps, the nanostamp fabrication technology is a key technology to UV-NIL. In this paper, a $5\times5\times0.09$ in. quartz stamp whose critical dimension is 377 nm was fabricated using the etching process in which a Cr film was employed as a hard mask for transferring nanostructures onto the quartz plate. To effectively apply the fabricated 5-in. stamp to UV-NIL on a 4-in. Si wafer, we have proposed a new UV-NIL process using a multi-dispensing method as a way to supply resist on a wafer. Experiments have shown that the multi-dispensing method can enable UV-NIL using a large-area stamp.

• 천문학회지
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• 제37권5호
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• pp.601-603
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• 2004

We present the results of the linear analysis for the Parker-Jeans instability in the magnetized gas disks including the effect of cosmic-ray diffusion along the magnetic field lines. We adopted an uni-formly rotating two temperature layered disk with a horizontal magnetic fields and solved the perturbed equations numerically. Fragmentation of gases takes place and filamentary structures are formed by the growth of the instability. Nagai et al. (1998) showed that the direction of filaments being formed by the Parker-Jeans instability depends on the strength of pressure outside the unperturbed gas disk. We found that at some range of external pressures the direction of filaments is also governed by the value of the diffusion coefficient of CR along the magnetic field lines k.

• Journal of Welding and Joining
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• 제21권1호
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• pp.99-106
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• 2003

This research was aimed to evaluate the material degradation with various microstructures of X20CrMoV121 steel weldment by Advanced Small Punch(ASP) test. Due to the regional limitation on constitutive structures, the minimized loading ball(${\varphi}1.5mm$) and bore diameter of lower die(${\varphi}3mm$) were designed for the ASP test. The micro-hardness test was also performed to assess the mechanical properties with artificial aging heat treatment. Material degradation was estimated by ductile-brittle transition temperature(DBTT). The results obtained from the ASP test were compared with those from conventional small punch(CSP) test and CVN impact test for several weldment microstructures. It was found that the ASP test clearly showed the microstructural dependance on the material degradation in the weldment.