• Proceedings of the KIEE Conference
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• 1989.07a
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• pp.287-290
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• 1989

Single-phase $YBa_2Cu_3O_{j-g}$ (YBC) ceramic samples were annealed at $700^{\circ}C$ under a flowing $O_2$ atmosphere for 0, 18, 36, 54 and 72. hours after sintering. The resistivities(p) and the critical current densities($J_c$) of the samples were measured in a temperature range 77 to 300 K by a four probe method, using silver paint contacts. The variations of the electrical properties with annealing time are explained in terms of flux pinning, percolation probability and randomness, and alignment of grains and twins.The anomalous increases in $J_c$ and $T_c$ observed in sample annealed for a relatively long time possibly due to alignment of grains and twins, may imply the occurrence of superconducting glass state in high-$T_c$ superconducting ceramic.

• 한국생물공학회:학술대회논문집
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• 2005.10a
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• pp.889-893
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• 2005

Cell lysis method is very important to study intracellular metabolites in microorganisms. In this study, various cell lysis methods were compared to find a good method analysing intracellular metabolites in P. pastoris. P. pastoris was cultivated in YPD medium at 30 $^{\circ}C$, 200 rpm for 24 hours and its morphology as well as the change in strain's shape were observed by microscopy. The UV/vis spectrophotometer was used to measure intracellular protein concentrations.

• Journal of the Korean Chemical Society
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• v.41 no.8
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• pp.392-398
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• 1997

A method of selective determination of inorganic and organic mercury compounds has been described. The $CHCl_3$ solution of a high molecular quaternary alkylammonium salt, Aliquat 336 was used for the simultaneous preconcentration of both inorganic, $Hg^{2+}$ as its thiocyanate complex, and organic mercury compounds, $CH_3HgCl$ and $C_2H_3O_2$ $HgC_6H_5$ by extraction from their aqueous solution. Selective separation of the inorganic mercury from the extract was followed by stripping with 3 M $HClO_4 $ solution for the subsequent determination by CVAAS. Organic mercury was also determined by CVAAS after removal of $CHCl_3solvent$ from the extract and decomposition of the residue with 4% $KMnO_4 $-1 MH_2$S0_4$. The mixtures of inorganic and organic mercury compounds contained 1.0 $\mug$ as Hg in 50 mL of sample solution(0.02 ${\mu}gHg/mL$) were analysed within ${\pm}6%$ by absolute errors.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2010.11a
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• pp.681-682
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• 2010

• The Transactions of the Korean Institute of Electrical Engineers D
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• v.49 no.2
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• pp.74-80
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• 2000

In this paper, we present a control method of mobile power assist systems. Most of mobile power assist systems have a heavy base for preventing easy tumbling, so continual movement of the base during operations causes high energy consumption and gives the high risk of human injury. Furthermore, the slow dynamics of the base limits the frequency bandwidth of the whole system. Thus we propose a cooperation control method of the mobile base and manipulator, which removes the unnecessary movements of the base. In our scheme, the mobile base does not move until the center of gravity(C.G) of the system goes outside a safety region. When C.G. reaches the boundary of the safety region, the base starts moving to recover the manipulator's initial configuration. By varying the parameters of a human impedance controller, the operator is warned by a force feedback that C.G. is on the marginal safety region. Our scheme is implemented by assigning a nonlinear mass-damper-spring impedance to the tip of the manipulator. Our scheme is implemented by a nonlinear mass-spring impedance to the tip of the manipulator. The experimental results show the efficacy of the proposed control method.

• Korean Chemical Engineering Research
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• v.53 no.5
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• pp.609-613
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• 2015

The onset of instability induced by impulsive spin-down of the rigid-body flow placed in the gap between two coaxial cylinders is analyzed by using the energy method. In the present stability analysis the growth rate of the kinetic energy of the base state and also that of disturbances are taken into consideration. In the present system the primary flow is a transient, laminar one. But for the Reynolds number equal or larger than a certain one, i.e. $Re{\geq}Re_G$ secondary motion sets in, starting at a certain time. For $Re{\geq}Re_G$ the dimensionless critical time to mark the onset of vortex instabilities, ${\tau}_c$, is here presented as a function of the Reynolds number Re and the radius ratio ${\eta}$. For the wide gap case of small ${\eta}$, the transient instability is possible in the range of $Re_G{\leq}Re{\leq}Re_S$. It is found that the predicted ${\tau}_c$-value is much smaller than experimental detection time of first observable secondary motion. It seems evident that small disturbances initiated at ${\tau}_c$ require some growth period until they are detected experimentally.

• Atmosphere
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• v.19 no.2
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• pp.107-125
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• 2009

Statistical downscaled surface temperature datasets by employing the cyclostationary empirical orthogonal function (CSEOF) analysis and multiple linear regression method are examined. For evaluating the efficiency of this statistical downscaling method, monthly surface temperature of the ECMWF has been downscaled into monthly temperature having a fine spatial scale of ~20km over the Korean peninsula for the 1973-2000 period. Monthly surface temperature of the ECHOG has also been downscaled into the same spatial scale data for the same period. Comparisons of temperatures between two datasets over the Korean peninsula show that annual mean temperature of the ECMWF is about $2^{\circ}C$ higher than that of the ECHOG. After applying to the statistical downscaling method, the difference of two annual mean temperatures reduces less than $1^{\circ}C$ and their spatial patterns become even close to each other. Future downscaled data shows that annual temperatures in the A1B scenario will increase by $3.5^{\circ}C$ by the late 21st century. The downscaled data are influenced by the ECHOG as well as observation data which includes effects of complicated topography and the heat island.

• Journal of the Korean Chemical Society
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• v.45 no.1
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• pp.7-13
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• 2001

The interaction of benzenesulfonate anion and its derivatives ($C_6H_5SO_3^-, p-$CH_3C_6H_4SO_3^-, and $p-C_2H_5C_6H_4SO_3^-$) with the micellar system of cationic surfactant TTAB(tetradecyltrimethylammonium bromide) was studied by UV/Vis spectrophotometric method. The solubilization constants($K_s$) of benzenesulfonate anions into the micellar phase of this surfactant have been measured with the change of temperature. The effects of additives(n-pentanol and NaBr) on the solubilization of benzenesulfonate anions by this surfactant system have been also measured. There was a great decrease on the values of $K_s$ and CMC simultaneously with these additives so that the measured values of ln$K_s$ were linear relationships with the values of lnCMC. For the thermodynamic study, various thermodynamic parameters(${\Delta}G^0_s$, ${\Delta}H^0_s$ and ${\Delta}S^0_s$) have been calculated and analyzed from the dependence of Ks values on temperature.

• Journal of the Korean Chemical Society
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• v.38 no.4
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• pp.283-287
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• 1994

The crystal stucture of bithional surfoxide, $C_{12}H_6Cl_4O_3S$, has been determined from 2295 independent reflections collected on an automated CAD-4 diffractometer with a graphite-monochromated $Mo-K\alpha$ radiation. The crystal belongs to the monoclinic, space group P2$_1$/n, with a unit cell dimensions a = 12.448(4), b = 9.740(1), c = $11.815(2)\AA$, $\beta$ = $100.06^{\circ}$, $\mu$ = 9.02 cm$^{-1}$, Dm = 1.76 g/cm$^3$, Dc = 1.75 g/cm$^3$, F(000) = 744, and Z = 4. The structure was solved by the direct method and refined by the least-squares method. The final R values was 0.037 for 2295 independent reflections. Overall conformation of the molecule is folded with respect to central surfur atom. Comparing with the molecular conformation of bithional, one of phenyl rings was swinged with about $180^{\circ}.$ This conformational change in the molecule results in the existance of intramolecular-hydrogen bond of S-O(3)---H-O(1) type and its steric hindrance between this moiety and the other phenyl ring. The two best planes of the phenyl rings have a maximum deviation of 0.009 $\AA$ for C(1) atom. The dihedral angle between two phenyl rings is $99.22^{\circ}.$ In the crystal structure, the molecules are packed with intermolecular-hydrogen bond of O(3)---H-O(2).

• Proceedings of the Korean Nuclear Society Conference
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• 2004.10a
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• pp.933-934
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• 2004