• Journal of the Korea institute for structural maintenance and inspection
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• v.19 no.6
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• pp.63-71
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• 2015

The objective of the present study is to investigate how elevated temperature ranging from $100^{\circ}C$ to $800^{\circ}C$ as well as room temperature affects the variation of mechanical properties of high strength concrete ($over\;f_{ck}=60MPa\;grade$). In this experiment, specimens were exposed for a period of $2^{\circ}C/min$ to temperatures of $20^{\circ}C$, $100^{\circ}C$, $200^{\circ}C$, $300^{\circ}C$ $400^{\circ}C$, $500^{\circ}C$, $600^{\circ}C$, $700^{\circ}C$ and $800^{\circ}C$, respectively. Accordingly, the study investigated the fire resistance performance of high strength concrete mixed with composite fibers which composed with hybrid fibers and steel fibers. After cooling down to ambient temperature, the following basic mechanical properties were then evaluated and compared with reference values obtained prior to thermal exposure: (i) compressive strength in room temperature; (ii) residual compressive strength; (iii) Poisson's ratio; (iv) weight change; (v) SEM analysis & XRD analysis In addition, XRD and SEM Images analyses were performed to investigate chemical and physical characteristics of high strength concrete with composite fibers according to high temperature.

• Journal of Environmental Science International
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• v.26 no.12
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• pp.1333-1339
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• 2017

Coal-fired power plants emit various Particulate Matter(PM) at coal storage pile and ash landfill as well as the stack, and affect the surrounding environment. Field Emission Scanning Electron Microscopy and Energy Dispersive X-ray analyzer(FE-SEM/EDX) were used to develop identification factor and the physico-chemical analysis of PM emitted from a power plant. In this study, three samples of pulverized coal, bottom ash, and fly ash were analyzed. The pulverized coal was spherical particles in shape and the chemical composition of C-O-Si-Al and C/Si and C/Al ratios were 200~300 on average. The bottom ash was spherical or non-spherical particles in shape, chemical composition was O-C-Si-Al-Fe-Ca and C/Si and C/Al ratios were $4.3{\pm}4.6$ and $8.8{\pm}10.0$. The fly ash was spherical particles in shape, chemical composition was O-Si-Ai-C-Fe-Ca and C/Si and C/Al ratios were $0.5{\pm}0.2$ and $0.8{\pm}0.5$.

• The Korean Journal of Food And Nutrition
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• v.24 no.1
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• pp.71-78
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• 2011

Peeled chestnuts were stored at different temperatures($-10^{\circ}C$ and $-20^{\circ}C$) and for different times(0, 10, and 20 min at $90^{\circ}C$) for blanching over a 6 month period. Analyses were conducted for moisture content, total sugar content, browning index, polyphenol compounds, PPO activity, and SEM. Moisture content and PPO activity were increased by storage time. The increments for the samples stored at $-20^{\circ}C$ were lower that for the samples stored at $-10^{\circ}C$. The Browning index was increased by storage time, and increments for the samples stored at $-20^{\circ}C$ were lower that for the samples stored at $-10^{\circ}C$. Scanning electronic microscopy(SEM) studies were performed on peeled chestnuts. Results showed that the wrinkle structure of the cell wall was enhanced by storage time, and the level of enhancement was higher at $-10^{\circ}C$ than at $-20^{\circ}C$.

• Journal of Conservation Science
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• v.16 s.16
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• pp.64-76
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• 2004

This study was performed by chemical analysis and metallographic observation. Chemical properties were analized by ICP, XRD and SEM-EDS and slag structures were observed by microscope and SEM. Total Fe amounts in A, C area of slag can be observed $39\~45\%$ by chemical analysis results. It was average of acient times. CaO was $3\~8\%$. It's not plentiful but we think that was artificial. Ti was found in A area a little, and Ti, V were found in C area so much. The compounds, as if Fayalite, Wustite, Magnetite, Ilmenite, Pseudo-brookite, Ulvospinel, Forsterite, Fephroite, Olivine were observed in the result XRD. These structures were also observed in microscope and SEM image. Therefore, The furnance of A area usually used an iron mine, An Iron furnance of C area considered it which refined using a raw iron mine and a raw iron sand.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2010.06a
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• pp.323-323
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• 2010

PNN-PZT계 세라믹스를 $Pb(Ni_{1/3}Nb_{2/3})_{0.4}(Zr_{0.48}Ti_{0.52})_{0.6}O_3$ 조성으로 설계하고, 이에 낮은 융점의 NiO를 1wt% 첨가하여 저온소결 특성을 평가하였다. 일반적인 세라믹 분말 소결법을 이용하여 시편을 제작하였으며, 이때의 소결온도는 $850{\sim}105^{\circ}C$ 범위에서 변화시켰다. 소결체의 압전 및 유전적 특성을 평가를 하고. SEM 및 XRD를 이용한 미세구조 및 상 분석도 수행하였다. 이러한 실험 결과, PNN-PZT 세라믹은 NiO의 첨가로 $1000^{\circ}C$ 정도에서도 저온소결이 가능한 것을 확인하였다.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2005.07a
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• pp.236-237
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• 2005

To measure surface roughness and smoothness of semiconducting materials in power cable, we have investigated the formation and growth process of carbon black showed by changing the content of carbon black. The specimens were primarily kneaded in material samples of pellet form for 5 minutes on rollers ranging between 70[$^{\circ}C$] and 100[$^{\circ}C$]. Then they were produced as sheets after pressing for 20 minutes at 180[$^{\circ}C$] with a pressure of 200[kg/cm]. The contents of conductive carbon black were the variable, and their contents were 20, 30 and 40[wt%], respectively. The surface roughness and smoothness of specimens were measured by SEM and AFM. From SEM experimental result, carbon black in specimens formed matrix as a particles. Also we showed growth process of carbon black according to an increment of the content of carbon black. From AFM experimental result, surface roughness of specimens decreased according to an increment of the content of carbon black.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2006.06a
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• pp.276-277
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• 2006

1mm-thick BLT ceramics were sintered in accordance with a bulk ceramic fabrication process. AII XRD peaks detected in the sintered ceramics were indexed as the Bi-layered perovskite structure without secondary phases. Density was increased with increasing the sintering temperature up to $1050^{\circ}C$ and the maximum value was about 98% of the theoretical density. The remanent polarization (2Pr) value of BLT ceramic sintered at $1050^{\circ}C$ was approximately $6.5\;{\mu}C/cm^2$ at the applied voltage of 4.5 kV. The calculated electromechanical coupling factor ($k_t$) of it was about 5% and the mechanical quality factor (Qm) was about 2200. From these results, a BLT ceramic target for pulsed laser deposition (PLD) system was successfully fabricated.

• Journal of the Korean Wood Science and Technology
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• v.35 no.1
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• pp.36-43
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• 2007

Elemental analysis, SEM-EDX, X-ray diffraction (XRD) and IR analysis were adopted to examine the quality of charred woods excavated from the underground of the Daewoongjeon Hall of Youngguksa Temple, Youngdong-gun, Chungbuk, Korea. A large amount of calcium was detected in SEM-EDX analysis. The analyses of chemical elements suggested that completely charred wood was carbonized at about $500^{\circ}C$. The XRD results indicated the destruction of cellulose crystalline region. The IR analysis exhibited that thermal degradation of wood component was different depending upon the carbonization temperature. It can be suggested from the results that PEG with different molecular weights should be used for the conservation of excavated charred woods.

• Analytical Science and Technology
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• v.21 no.3
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• pp.229-236
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• 2008

$C/TiO_2$ composites were prepared with surface modified MWCNT sequentially after HCl treatment and TNB as titanium source. There is a single crystal structure which is anatase in all of the samples from the data of XRD. The SEM microphotographs of $C/TiO_2$ composites show that the $TiO_2$ particles were well mixed with the CNT. There are C, O and Al with strong Ti peaks in all samples from EDX results, and it also shows that the sample CT has much more amount of C and Ti content than that of sample HCT. Finally, the photocatalytic activities for the $C/TiO_2$ composites have more effective than that of pristine $TiO_2$.

• Korean Journal of Food Science and Technology
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• v.22 no.3
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• pp.300-306
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• 1990

The microstrutural changes of mayonnaise during storage were examined by light microscopy (LM) and scanning electron microscopy (SEM). Fresh mayonnaise was composed of heterogenous population of dispersed spherical oil droplets and droplet size was normally distributed with one mode. During storage at $60^{\circ}C\;and\;-10^{\circ}C$, a shift in droplet size distribution toward larger droplets was observed, as a result of coalescence of lipid droplets. Turbidimetric study also confirmed that coalescence was occurring during this accelerated aging treatments. Measurements obtained from SEM microgrphs provided better determination of smaller droplets and resulted in lower mean diameter of droplets than those obtained from LM. From these results, SEM was found to be an advantageous method of examining emulsion products as compared to LM, providing a better resolution of small droplets and a more representative view of droplet distribution, as dilution of the sample was avoided.