• Title/Summary/Keyword: By-Product Materials

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Preparation and Sound Insulation Properties of Thermoplastic Elastomer Composites with CaCO3 Filler (탄산칼슘 분말을 충진시킨 열가소성 탄성체 복합재의 제조 및 차음 특성)

  • Choi, Jung-Woo;Hwang, Yeon
    • Korean Journal of Materials Research
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    • v.20 no.9
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    • pp.467-471
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    • 2010
  • Composites of ceramic powders and an elastomer-based matrix were prepared by mixing $CaCO_3$ powders with polyethylene and polypropylene elastomers, and their mechanical and sound insulation properties were measured. $CaCO_3$ powders with 0.7 ${\mu}m$ and 35 ${\mu}m$ particle size were added to elastomers up to 80 wt%. Scanning electron microscopy photographs showed uniform distribution of the $CaCO_3$ powders in the matrix. While density and surface hardness increased, melt index, tensile strength and elongation of the composites decreased as the amount of added $CaCO_3$ powders increased. As more $CaCO_3$ powders were added sound transmission loss of the composites increased owing to the increase of density. Addition of 0.7 ${\mu}m$ sized $CaCO_3$ powders resulted in a slightly higher transmission loss than the addition of 35 ${\mu}m$ sized powders because of the increased interface area between the elastomer matrix and the $CaCO_3$ powders. Composites with a polyethylene matrix showed higher transmission loss than those with a polypropylene matrix because the tensile strength and hardness of the polyethylene-based composites were low and their elongation was high.

Synthesis of β-SiC Powder using a Recycled Graphite Block as a Source (그라파이트 블록을 원료로써 재활용한 β-SiC 분말 합성)

  • Nguyen, Minh Dat;Bang, Jung Won;Kim, Soo-Ryoung;Kim, Younghee;Jung, Eunjin;Hwang, Kyu Hong;Kwon, Woo-Teck
    • Resources Recycling
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    • v.26 no.1
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    • pp.16-21
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    • 2017
  • This paper relates to the synthesis of a source powder for SiC crystal growth. ${\beta}-SiC$ powders are synthesized at high temperatures (>$1400^{\circ}C$) by a reaction between silicon powder and carbon powder. The reaction is carried out in a graphite crucible operating in a vacuum ambient (or Ar gas) over a period of time sufficient to cause the Si+C mixture to react and form poly-crystalline SiC powder. End-product characterizations are pursued with X-ray diffraction analysis, SEM/EDS, particle size analyzer and ICP-OES. The purity of the end-product was analyzed with the Korean Standard KS L 1612.

A Study on the Extru-Bending Process of the Angle Product with 'Λ' Section Using Two Extrusion Billets (두 개의 압출빌렛을 사용하는 'Λ' 단면 앵글 구조재의 압출굽힘가공에 관한 연구)

  • Lee K. K.;Jin I. T.
    • Transactions of Materials Processing
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    • v.14 no.2 s.74
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    • pp.160-167
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    • 2005
  • In the present study about extru-bending of angle product, the bending of extruded angle products with the $'\Lambda'$ section and 'ㄱ', section can be obtained using two extrusion billets by the hot metal extru-bending machine with the two punches moving in the different velocity. The bending curvature can be controlled by the different velocity of billets through the two-hole container. This paper describes simulations and experiments of extru-bending process that can make bending during extruding by the difference of stem velocities. And they are applied to two kinds of dies, that is, one of them is conical dies with symmetry $'\Lambda'$ section and the other one is conical dies with asymmetry 'ㄱ' section. The results of the forming simulation by $DEFORM^{TM}-3D$ and results of experiments show that the bending phenomenon at the die exit during extrusion can be obtained with two extrusion billet by the two stems moving in the different velocity. And it was known that it is possible to design the structure of conical cavity of extrusion dies and to control the curvature of product through the simulation and experiment of extru-bending process.

The Effect of Processing Variables and Composition on the Nitridation Behavior of Silicon Powder Compact

  • Park, Young-Jo;Lim, Hyung-Woo;Choi, Eugene;Kim, Hai-Doo
    • Journal of the Korean Ceramic Society
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    • v.43 no.8 s.291
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    • pp.472-478
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    • 2006
  • The effect of compositional and processing variables on a nitriding reaction of silicon powder compact and subsequent post sintering of RBSN (Reaction-Bonded Silicon Nitride) was investigated. The addition of a nitriding agent enhanced nitridation rate substantially at low temperatures, while the formation of a liquid phase between the nitriding agent and the sintering additives at a high temperature caused a negative catalyst effect resulting in a decreased nitridation rate. A liquid phase formed by solely an additive, however, was found to have no effect on nitridation for the additive amount used in this research. The original site of a decomposing pore former was loosely filled by a reaction product ($Si_3N_4$), which provided a specimen with nitriding gas passage. For SRBSN (Sintered RBSN) specimens of high porosity, only a marginal dimensional change was measured after post sintering. Its engineering implication for near-net shaping ability is discussed.

Experimental Study on Air Decomposition By-Product Under Creepage Discharge Fault and Their Impact on Insulating Materials

  • Javed, Hassan;LI, Kang;Zhang, Guoqiang;Plesca, Adrian Traian
    • Journal of Electrical Engineering and Technology
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    • v.13 no.6
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    • pp.2392-2401
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    • 2018
  • Creepage discharge faults in air on solid insulating material play a vital role in degradation and ageing of material which ultimately leads to breakdown of power equipment. And electric discharge decompose air in to its by-products such as Ozone and $NO_x$ gases. By analyzing air decomposition gases is a potential method for fault diagnostic in air. In this paper, experimental research has been conducted to study the effect of creepage discharge on rate of generation of air decomposition by-products using different insulating materials such as RTV, epoxy and fiberglass laminated sheet. Moreover XRF analysis has been done to analyze creepage discharge effect on these insulating materials. All experiments have been done in an open air test cell under constant temperature and pressure conditions. While analysis has been made for low and high humidity conditions. The results show that the overall concentration of air decomposition by-products under creepage discharge in low humidity is 4% higher than concentration measured in high humidity. Based on this study a mathematical relationship is also proposed for the rate of generation of air decomposition by-products under creepage discharge fault. This study leads to indirect way for diagnostic of creepage discharge propagation in air.

Improvement in Grade of Sericite Ore by Dry Beneficiation (건식정제에 의한 견운모광의 품위향상연구)

  • Cho, Keon-Joon;Kim, Yun-Jong;Park, Hyun-Hae;Cho, Sung-Baek
    • Korean Journal of Materials Research
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    • v.19 no.4
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    • pp.212-219
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    • 2009
  • A study on the dry beneficiation of sericite occurring in the Daehyun Mine of the Republic of Korea region as performed by applying selective grinding and air classification techniques. Quartz and sericite occurred in the raw ore as major components. The results of liberation using a ball mill and an impact mill showed that the contents of $R_2O$ were increased while $SiO_2$ was decreased in proportion to decreasing particle size. According to the XRD, XRF analysis and the EDS of SEM analysis, the ball mill gave a better grade product in $R_2O$ content than the impact mill when the particle size was the same. When the raw ore was ground by the impact mill with arotor speed 57.6 m/sec and then followed by 15,000rpm classification using an air classifier, the chemical composition of the over flowed product was 49.65wt% $SiO_2$, 32.15wt% $Al_2O_3$, 0.13wt% $Fe_2O_3$, 10.37wt% $K_2O$, and 0.14wt% $Na_2O$. This result indicates that the $R_2O$ contents were increased by 49.5% compared to that of the raw ore. From these results described above, it is suggested that hard mineral such as Quartz little ground by selective grinding using impact mill whereas soft mineral such as sericite easily ground to small size. As a result of that hard minerals can be easily removed from the finely ground sericite by air classification and the $R_2O$ grade of thus obtained concentrate was improved to higher than 10wt% which can be used for ceramics raw materials.

Microstructure Change of Large Cast-forged Product by Forging and Heat Treatment Conditions (단조/열처리 공정이 대형 주단조품의 조직변화에 미치는 영향)

  • Lee, M.W.;Lee, Y.S.;Lee, S.W.;Lee, D.H.;Kim, S.S.;Moon, Y.H.
    • Transactions of Materials Processing
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    • v.18 no.6
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    • pp.458-464
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    • 2009
  • Thermal energy control is a important factor to control properties of large sized product in ingot-forging. Good control of thermal energy helps to increase characteristics and eliminate defects of large cast-forged part, such as large sized forged shell. We have studied about not only large size ring forging process and after heat treatment process by FEM simulation. Changes of temperature and microstructure for forged shell were predicted according to different heat treatment conditions. Therefore, we can choose the proper heat treatment condition by FEA. The sectional properties confirmed by practical experiment and evaluation have presented possibilities of process design by computational analysis.

Study on Dormancy Mechanisms of American Ginseng Seed II - Germination Inhibition of Seed Coat

  • Huang, Yao-Ge;Li, Xiang-Gao;Cui, Shu-Yu;Yang, Ji-Xiang;Liu, Ren-Song;Kim, Hack-Seang
    • Natural Product Sciences
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    • v.2 no.2
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    • pp.137-142
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    • 1996
  • This paper gives a description about the germination inhibition of American ginseng (Panax quinquefolium L.) seed coat. The existence of seed coat is one of the inhibitory factors which inhibit the embryo growth, particularly during the morphological after-ripening stage. The seed coat can obstruct the water absorption at the beginning of seed stratification, but it can not threaten seed germination. The inhibition of seed coat is not caused by the mechanical fetter neither. However, before splitting the seed coat, the inhibition of seed coat comes from both air-tight character and inhibitors, and after splitting the seed coat, the inhibition may come mainly from the inhibitors.

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Comparison of analytical method of headspace and tenax analysis for residue of solvent amounts on plastic packaging materials (Headspace 방법과 tenax 방법을 이용한 잔존 용제 분석 방법의 비교)

  • An, Duek-Jun
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.10 no.1
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    • pp.63-68
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    • 2004
  • The regulations for migration amounts in USA, EU and Korea are investigated to compare the actual overall and specific migration date from plastic food packaging materials. Among the packaging materials regulated in above countries, printing ink solvents on packaging materials is used very widely and sometimes cause off-flavor in the food by migration of residual solvents. Even though migration of the residual solvents dose not generally cause safety problems in the contained food, it certainly can generate off-flavor and finally deteriorate quality of the finished product. Therefore regulation and development of analytical method for amount of residual ink solvents are very important issue in food industry. The headspace analytical method and tenax method for residual ink solvent on food packaging materials were evaluated from the accuracy, precise, swiftness and convenience of viewpoint. Headspace analytical method was selected and recommended for using in food industry field.

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Synthesis and Morphological Transformation of NaA Zeolite Crystals at High Temperature

  • Kim, Young-Mi;Kim, Ik-Jin
    • Journal of the Korean Ceramic Society
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    • v.43 no.1 s.284
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    • pp.1-3
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    • 2006
  • Well-shaped NaA zeolite cubic crystals of a large size of $5-7{\mu}m$ were synthesized by a hydrothermal method in a mother solution having a $3.55Na_2O:Al_2O_3:1.6SiO_2:593\~2000H_2O$ composition. Thermal treatment of NaA zeolite crystals resulted in the formation of a crystalline phase of $NaAlSiO_4-Camegeite$ between 800 and $900^{\circ}C$. Even at $1000^{\circ}C,\;NaAlSiO_4$ phase was found as a major product. Environmental Scanning Electron Microscopy (ESEM), High Resolution Transmission Electron Microscopy (HRTEM), X-Ray powder Diffraction (XRD), Fourier Transform Infrared (FT-IR) spectroscopy, and DTA/TGA and BET analyses were used to characterize the initial materials and the obtained products after various heat treatments.