• Title/Summary/Keyword: Brittle ceramics

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Contact fatigue and strength degradation in dental ceramics (치아용 세라믹스에서의 접촉피로 및 강도저하)

  • 정연길;이수영;최성철
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.5
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    • pp.527-533
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    • 1999
  • Hertzian indentation tests with spherical indenters in water were conducted to examine the contact fatigue in three dental ceramics, such as feldspathic porcelain, micaceous glass-ceramic (MGC) and glass-infiltrated alumina, which was used as dental restorations, and evaluated the effect of contact damage on strength. Initial damage was dependent of microstructure, showing cone cracks of brittle behavior in the feldspathic porcelain and deformation of quasi-plastic behavior in the MGC, with an intermediate case in the glass-infiltrated alumina. However, as increasing the number of cyclic loading (n=1~n =$10^6$)all materials showed an abrupt strength degradation, at which fracture was originated from damage in the contact fatigue. There were two strength degradation with increasing the number of cyclic loading in specific loads (200N, 500N, 1000N):first was from the cone cracks, and second was from the radial cracks created by cyclic loading. The radial cracks, once formed, led to rapid degradation in strength properties, Finally the material was failed at the high number of cyclic loading. Strength degradation with indentation load at fixed number of cyclic loading indicated that the feldspathic porcelain should be highly damage tolerant to the contact fatigue.

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Effects of the Brazing Bonding between Al2O3 and STS304 with an Ion Beams (이온빔을 이용한 STS304와 알루미나 브레이징 접합효과)

  • Park, Il-Soo
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.12
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    • pp.8679-8683
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    • 2015
  • Using a surface modification technique, ion beam assisted deposition (IBAD) of Ti thin film it becomes possible to prepare an active ceramic surface to braze $Al_2O_3$-STS304 with conventional Ag-Cu eutectic composition filler metal. Researches on bonding formations at interfaces of ceramic joints were mainly related on the development of filler metals to ceramic, the process parameters, and clarifications of reaction products. From the results, the reactive brazing is a very convenient technique compared to the conventional Mn-Mo method. However melting point of reactive filler is still higher than that of Ag-Cu eutectic and it forms the brittle inter metallic compound. Recently several new approaches are introduced to overcome the main shortcomings of the reactive metal brazing in ceramic-metal, metal vapor vacuum arc ion source was introduced to implant the reactive element directly into the ceramics surface, and sputter deposition with sputter etching for the deposition of active material.

Surface Smoothing of Blasted Glass Micro-Channels Using Abrasive Waterjet (워터젯을 이용한 블라스팅 유리 마이크로 채널의 표면거칠기 개선)

  • Son, Sung-Gyun;Han, Sol-Yi;Sung, In-Ha;Kim, Wook-Bae
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.37 no.12
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    • pp.1159-1165
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    • 2013
  • Powder blasting, which is an efficient micromachining method for glass, silicon, and ceramics, has a critical disadvantage in that the surface finish is poor owing to the brittle fracture of materials. Low-pressure waterjet machining can be applied to smoothen the rough surface inside the blasted structure. In this study, the surface roughness and sectional dimension of micro-channels are observed during the repetitive application of a waterjet to blasted micro-channels. The asperities and subsurface cracks created by blasting are removed by waterjet machining. Along with the surface roughness, it is found that the sectional dimension increases and the edges of the finished micro-channel become slightly round. Finally, a microfluidic chip is machined by the blasting-waterjet process and a transparent microfluidic channel is obtained efficiently.

Optimization of Crystallization Condition for Transparent LAS Glass-ceramic Via Differential Thermal Analysis (DTA를 통한 LAS계 투명 결정화 유리의 결정화 조건 최적화)

  • Moon, Yun-Gon;Lim, Tae-Young;Lee, Mijai;Kim, Jin-Ho;Jeon, Dae-Woo;Hwang, Jonghee
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.29 no.2
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    • pp.101-105
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    • 2016
  • The basic characteristics of glass are highly fragile and brittle consequences the ultimate purpose of glass manufacturing is to make a transparent glass with complex shape. In order to solve this problem, mechanical properties of glass can be increased by crystallization of its amorphous glass. However, glass-ceramics has become opaque through crystallization process due to the distracted interface of glass by precipitated particles. This study has been investigated thermal processing conditions of LAS transparent glass-ceramic by using DTA (differential thermal analysis), in order to control size of precipitated particle and then fabricate transparent glass-ceramic. DTA indicated that crystallization peak area was declined with increased nucleation temperature. Subsequently, we have been established optimum temperature for crystallization depending on the nucleation temperature. The transmission and thermal expansion were measured after crystallization, and the size of precipitated particle was identified in range of 20~100 nm by FE-SEM. In addition, by setting the optimized crystallization condition, with high transmission and low thermal expansion glass was synthesized through this experiment.

Influence of Sintering Additives and Temperature on Fabrication of LPS-SiC (액상소결법에 의한 탄화규소 제조시 소결조제와 온도의 영향)

  • JUNG HUN-CHAE;YOON HAN-KI
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2004.11a
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    • pp.266-270
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    • 2004
  • SiC materials have been extensively studied for high temperature components in advanced energy system and advanced gas turbine because it has excellent high temperature strength, low coefficient of thermal expansion, good resistance to oxidation and good thermal and chemical stability etc. However, the brittle characteristics of SiC such as low fracture toughness and low strain-to fracture still impose a severe limitation on practical applications of SiC materials. For these reasons, SiC/SiC composites can be considered as a promising for various structural materials, because of their good fracture toughness compared with monolithic SiC ceramics. But, high temperature and pressure lead to the degradation of the reinforcing jiber during the hot pressing. Therefore, reduction of sintering temperature and pressure is key requirements for the fabrication of SiC/SiC composites by hot pressing method. In the present work, monolithic Liquid Phase Sintered SiC (LPS-SiC) was fabricated by hot pressing method in Ar atmosphere at $1800^{\circ}C$ under 20MPa using $Al_2O_3,\;Y_2O_3\;and\;SiO_2$ as sintering additives in order to low sintering temperature and sintering pressure. The starting powder was high purity $\beta-SiC$ nano-powder with all average particle size of 30mm. The characterization of LPS-SiC was investigated by means of SEM and three point bending test. Base on the composition of sintering additives-, microstructure- and mechanical property correlation, tire compositions of sintering additives are discussed.

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Parallel Computing Strategies for High-Speed Impact into Ceramic/Metal Plates (세라믹/금속판재의 고속충돌 파괴 유한요소 병렬 해석기법)

  • Moon, Ji-Joong;Kim, Seung-Jo;Lee, Min-Hyung
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.22 no.6
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    • pp.527-532
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    • 2009
  • In this paper simulations for the impact into ceramics and/or metal materials have been discussed. To model discrete nature for fracture and damage of brittle materials, we implemented cohesive-law fracture model with a node separation algorithm for the tensile failure and Mohr-Coulomb model for the compressive loading. The drawback of this scheme is that it requires a heavy computational time. This is because new nodes are generated continuously whenever a new crack surface is created. In order to reduce the amount of calculation, parallelization with MPI library has been implemented. For the high-speed impact problems, the mesh configuration and contact calculation changes continuously as time step advances and it causes unbalance of computational load of each processor. Dynamic load balancing technique which re-allocates the loading dynamically is used to achieve good parallel performance. Some impact problems have been simulated and the parallel performance and accuracy of the solutions are discussed.

FEA estimates of margin design in all ceramic crowns (완전 도재관을 위한 지대치 형성시 변연 형태에 따른 응력 분포의 유한요소법적 비교)

  • Han, Sang-Hyun;Cho, Jung-Hyeon;Lee, En-Jung;Jeong, Suk-In;Oh, Nam-Sik
    • The Journal of Korean Academy of Prosthodontics
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    • v.46 no.1
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    • pp.1-11
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    • 2008
  • Statement of problem: Over the past decade, increased demand for esthetically pleasing restorations has led to the development of all-ceramic systems. Recent reports suggest that the all-ceramic crowns have excellent physical properties, wear resistance, and color stability. In addition, numerous ceramics have excellent biocompatibility, a natural appearance, and improved physical bonding with resin composite luting agents. However, the brittle nature of ceramics has been a major factor in their restriction for universal usage. Functional occlusal loading can generate stress in the luting agent, and the stress distribution may be affected by the marginal geometry at the finish line. Tooth preparation for fixed prosthodontics requires a decision regarding the marginal configuration. The design dictates the shape and bulk of the all ceramic crowns and influences the fit at the margin. Purpose: The purpose of this study was to evaluate the stress distribution within marginal configurations of all- ceramic crowns (90-degree shoulder, 110-degree shoulder, 135-degree shoulder). Material and methods: The force is applied from a direction of 45 degrees to the vertical tooth axis. Three-dimensional finite element analysis was selected to determine stress levels and distributions. Results and conclusion: The result of stress level for the shoulder marginal configuration was more effective on stress distribution at 135-degree shoulder margin. But the stresses concentrated around at 135-degree shoulder margin. The stress decreased apically at the surface between cements and alumina core, and increased apically at the surface between alumina core and veneering porcelain.