• 제목/요약/키워드: Brewster angle

검색결과 41건 처리시간 0.019초

BAM(Brewster-Angle Microscope)으로 관측한 Langmuir막의 상전이에 관한 연구 (The Study on the Phase Transition of Langmuir Film by Brewster-Angle Microscope)

  • 조완제;송경호;박태곤;박근호
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2000년도 영호남학술대회 논문집
    • /
    • pp.323-326
    • /
    • 2000
  • In this study, we used Brewster-Angle Microscope(BAM) to study on the molecular orientation of monolayer on the water surface. The behaviors of molecules on three different subphase have been observed. Reproducible $\pi$-A isotherm have been obtained only on information about phase transition by molecular area. BAM facilitates the observation of morphology by optical anisotropy and thickness in monolayer and multilayers as BAM is shown to be sensitive to anisotropy of film. Every transition was found by BAM technique, either as a dramatic change in degree of contrast or as a sudden alteration of molecular action and $\pi$-A isotherm.

  • PDF

Brewster Angle Microscope를 이용한 액정 배향막 연구 (A Study of Liquid Crystal Alignment Layer Using Brewster Angle Microscope)

  • 정치섭
    • 한국전기전자재료학회논문지
    • /
    • 제12권1호
    • /
    • pp.81-87
    • /
    • 1999
  • The surface morphology of liquid crystal alignment layer has been investigated by using Brewster angle microscope(BAM) for the first time. The samples used in this work for liquid crystal alignment layer were mechanically rubbed polyimide films. The rubbing pattern on this layer has been analyzed with the terms of microgroove and rubbing induced optical birefringence. For the mechanically rubbed surface, the geometrical factors of microgroove play the major role for the formation of rubbing pattern. We propose that the BAM can be used as a powerful tool not only for observing the rubbing pattern, but also for inspecting the surface defects.

  • PDF

변위전류법과 BAM(BREWSTER-ANGLE MICROSCOPE)를 이용한 LANGMUIR막의 관찰 (Obervation of Langmuir Films Using Displacement Current Method and BAM (Brewster-Angle Microscope))

  • 송경호;박태곤;박근호
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2001년도 춘계학술대회 논문집 센서 박막재료
    • /
    • pp.38-42
    • /
    • 2001
  • To observe the Langmuir films, displacement current measuring system(Nippon Laser & Electronics), $\pi-A$ isotherms measuring device, and Brewster Angle Microscope(BAM) were used. As results, for 8A5H, big tilt angle changes of many molecules were detected before liquid expanded phase when the monolayer was compressed and expanded by barrier. Also many small and bright points were detected by BAM when the displacement current radically changed. In $\pi$-A isotherms, surface pressure of 8A5H was radically decreased between 35 and 40[mN/m] and monolayer was assumed to be collapsed in solid condensed phase, since large bright domain was observed without change of displacement current and this bright boundary was not classified part of domain in BAM image. If we observe behaviors of molecules on the water surface in these three measurement at the same time, we can get more precise informations on L films and it could be good data for fabricating LB films.

  • PDF

BAM(Brewster angle microscopy)을 이용한 PAAS(Polyamic Acid Alkylamine Salts)의 Langmuir막과 Langmuir-Blodgett막의 특성 연구 (A. Study on the PAAS(Polyamic Acid Alkylamine Salts) Langmuir Films and Langmuir-Blodgett Films using BAM(Brewster angle microscopy))

  • 이승엽;강도열;김태완
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 1996년도 추계학술대회 논문집
    • /
    • pp.147-151
    • /
    • 1996
  • Brewster angle microscopy(BAM) makes it possible to observe the monolayer states on the water subphase and the phase transitions from a gaseous phase via a expanded phase to a condensed phase. Also BAM can be used to observe the films on the solid substrate such as Langmuir-Blodgett(LB) films. In this Paper Polyamic Acid Alkylamine Salts(PAAS) was used for forming L films and LB films and $\pi$-A isotherm showed pressure of each phase. We obtained BAM images as surface pressure increased. Images of LB films were compared with data from ellipsometry which was used to measure the film thickness. Images of both L films and LB films were analyzed with computer in the point of brightness.

  • PDF

$Gd_{2}(MoO_{4})_{3}$ 단결정의 강탄성구역과 굴절률특성 (Ferroelastic Domain and Refractive Property of $Gd_{2}(MoO_{4})_{3}$ Single Crystal)

  • 손중윤;이찬구;이수대;김재형
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2002년도 춘계학술대회 논문집 센서 박막재료 반도체재료 기술교육
    • /
    • pp.98-102
    • /
    • 2002
  • We investigated domains and conoscope under the polarizing microscope and the index of refraction on the c-plate GMO which has the ferroelectric and ferroelastic phase at room temperature. To observed the change of refractive index in connection with domain, we developed an apparatus to obtain the refractive index by measuring the Brewster's angle. The resolution of the minimum rotation angle of this apparatus is $0.001^{\circ}$. To obtain the refractive index map on the sample, the moving distance of XY stage loaded sample holder is 60 mm and the minimum moving distance is 0.002 mm. Also, To obtain the indicatrix for single crystal, vertical turntable with sample holder and XY stage was loading on horizontal turntable. The minimum resolution angle of this vertical turntable is $0.001^{\circ}$. We measured the refractive index of transparent materials such as ferroelectrics. In the case of $Gd_{2}(MoO_{4})_{3}$, the Brewster angle is $62.11^{\circ}$ and then, the refractive index is 1.8895 by using He-Ne Laser. Also the refractive distribution of c-plate GMO was obtained with $400{\mu}m{\times}120{\mu}m$.

  • PDF

분광 타원해석기 입사각의 정밀 보정 (Precise calibration of the angle of ncidence in spectroscopic ellipsometer)

  • 김현종;김상열;이윤우;조현모;조용재;이인원
    • 한국광학회지
    • /
    • 제10권3호
    • /
    • pp.208-213
    • /
    • 1999
  • 반도체 및 박막의 두께 측정에 많이 이용되는 분광 타원해석기의 입사각을 정밀하게 보정하기 위한 방법을 제안하고 이를 실험적으로 확인하였다. 몇 종류의 광학유리를 이용하여 프리즘과 기판을 가공하였다. 프리즘의 꼭지각과 최소 벗어나 기각을 측정해 광학유리의 굴절률을 결정하였고 브루스터각(Brewster's angle)에서 측정한 유리기판의 타원해석 스펙트럼을 분석하기 위한 기준값으로 이 굴절률을 사용하여 분광 타원해석기의 입사각을 0.01도의 정밀도로 결정,보정하였다.

  • PDF

접힌 공진기 형태의 연속 발진 티타늄 사파이어 레이저의 발진 특성 (Characteristics of a CW Ti:sapphire Laser in a Folded Geometry)

  • 강영일;차용호;남창희
    • 한국광학회지
    • /
    • 제6권4호
    • /
    • pp.282-287
    • /
    • 1995
  • 발진 파장 영역이 매우 광범위한 티타늄 사파이어를 사용하여 접힌 공진기 형태의 레이저를 제작하고 연속 발진 특성을 조사하였다. 티타늄 사파이어 결정은 $Ti^{3+}$ 도핑율이 0.15wt.%이고 두께가 4.1mm이며 양면이 Brewster 각으로 되어 있는 것을 사용하였다. Brewster 면에서는 비점수차가 발생하므로 이를 보정하기 위하여 공진기의 접힌 각도를 $15.4^{\circ}$로 조정하였다. 펌핑 광원으로는 Ar-ion 레이저를 사용하였고, 반사율 90%의 출력경을 사용하여 2W 펌핑에서 레이저 발진이 시작되었으며, 5W 펌핑에서 450mW 이상의 츨력을 얻을 수 있었다. 또한 공진기의 두 오목거울 간의 거리에 따라 출력 변화를 조사하였다.

  • PDF

황산 겔 전해질을 사용한 차세대 대체에너지용 밀폐형 납축전지에 관한 연구 (A Study on the Valve Regulated Lead-Acid Battery using Sulfuric Acid Gel Electrolyte for New Generation Substitution Energy)

  • 박근호;주찬홍
    • 한국응용과학기술학회지
    • /
    • 제21권2호
    • /
    • pp.164-173
    • /
    • 2004
  • The capacity and long life of gel electrolyte batteries is connected with gas recombination producting $PbO_2$ and Pb electrode. We prepared with sulfuric acid gel electrolyte to know gel characteristics per density to assemble valve regulated lead-acid (VRLA) batteries. We studied on actions of sulphuric acid gel electrolyte by measuring electrolyte dispersion using Brewster-angle microscope (BAM), charge-discharge cycle, and electrode structure using scanning election microscope (SEM). Sulphuric acid density 1.210 showed excellent gel dispersion in sol condition, electrode condition after fifty cycles in this study.

인산 겔 전해질을 사용한 밀폐형 납축전지에 관한 연구 (A Study on the Valve Regulated Lead-Acid Battery using Phosphoric Acid Gel Electrolyte)

  • 주찬홍;박근호
    • 한국응용과학기술학회지
    • /
    • 제20권4호
    • /
    • pp.296-308
    • /
    • 2003
  • The capacity and long life of gel electrolyte batteries is connected with gas recombination producting $PbO_2$ and Pb electrode. We were prepared with phosphoric acid gel electrolyte to know gel characteristics per density to assemble VRLA batteries. We studied by measuring electrolyte dispersion using Brewster-angle microscope(BAM), charge-discharge cycle and electrode structure using scanning election microscope(SEM) per electrolyte density. As a results, phosphoric acid density 1.210 was excellent gel dispersion in sol condition, electrode condition after fifty cycles in this study.

네마틱 액정의 수면상 단분자막에서의 분자 배향 연구 (A Study on the Molecular Orientation of Nematic Liquid Crystal Monolayers on the water Surface)

  • 조완제;송경호;박근호;강영수;박태곤
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 1999년도 추계학술대회 논문집
    • /
    • pp.610-612
    • /
    • 1999
  • In this study, we used both displacement-current method and BAM(Brewster-Angle Microscope) to study on the molecular orientation of monolayer on the water surface. The displacement-current method measured behaviors of molecules by current and BAM was shown to be sensitive to film anisotropy even when the molecules were not tilted as long as the unit cell was anisotropic. Every transition was visible with BAM technique, either as a dramatic change in decree of contrast or as a sudden alteration of the mosaic domain texture.

  • PDF