• 제목/요약/키워드: Boron analysis

검색결과 267건 처리시간 0.033초

상변태를 고려한 핫프레스포밍 공정의 유한요소해석 (FE Analysis of Hot Press Forming Process considering the Phase Transformation)

  • 강경필;이경훈
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2008년도 추계학술대회 논문집
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    • pp.226-229
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    • 2008
  • Hot press forming is an advanced forming technology fur manufacturing of complex and crash-resistant automotive parts using ultra high strength steels. The 3-dimensional FE analysis of hot press forming process, in which process the deformation, heat transfer and phase transformation behavior are fully coupled, is carried out. The vast amount of material properties for the FE analysis is obtained from material properties calculation software which is based on thermodynamic calculations. The overall methodology for the FE analysis of HPF process and the analysis results are discussed here.

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Effects of Molding Pressure and Sintering Temperature on Properties of Foamed Glass without Blowing Agent

  • Kim, EunSeok;Kim, Kwangbae;Lee, Hyeryeong;Kim, Ikgyu;Song, Ohsung
    • 한국세라믹학회지
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    • 제56권2호
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    • pp.178-183
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    • 2019
  • A process of fabricating the foamed glass that has closed pores with 8 ~ 580 ㎛ sizes without a blowing agent by sintering 10 ㎛ boron-free glass powder composed of CaO, MgO, SO3, Al2O3-83 wt% SiO2 at a molding pressure of 0 ~ 120 MPa and a sintering temperature of 750 ~ 1000℃ was investigated. To analyze the glass transition temperature of glass powder, thermogravimetric analysis-differential thermal analysis (TGA-DTA) method were used. The microstructure and pore size of foamed glass were examined using the optical microscopy and field emission scanning electron microscopy (FE-SEM). For the thermal diffusivity and color of the fabricated samples, a heat flow meter and ultraviolet-visible-near-infrared (UV-VIS-NIR)-colormetry were used, respectively. In the TGA-DTA result, the glass transition temperature of glass powder was confirmed to be 626℃. In the microstructure result, closed pores of 7 ~ 20 ㎛ were formed at 750 ~ 900℃, and they were not affected by the molding pressure and sintering temperature. However, at 1,000℃, when there was 0 MPa molding pressure, closed pores of 580 ㎛ were confirmed, and the pore size decreased as the molding pressure increased. Moreover, at a molding pressure of 30 MPa or higher, closed pores of approximately 400 ㎛ were formed. The porosity showed an increasing trend of smaller molding pressure and larger sintering temperature, and it was controllable in the range of 5.69 ~ 68.45%. In the thermal diffusivity result, there was no change according to the molding pressure, and, by increasing the sintering temperature, up to 0.115 W/m·K could be obtained. The Lab color index (CIE-Lab) results all showed a similar translucent white color regardless of molding pressure and sintering temperature. Therefore, based on the foamed glass without boron and blowing agent, it was confirmed that white foamed glass, which has closed pores of 8 ~ 580 ㎛ and a thermal diffusivity characteristic of 0.115 W/m·K, can be fabricated by changing the molding pressure and sintering temperature.

Boron-doped Diamond 전극을 이용한 Rhodamine B와 N, N-Dimethyl-4-nitrosoanilin의 전기화학적 분해에 반응표면분석법의 적용과 공정 최적화 (Application of the Response Surface Methodology and Process Optimization to the Electrochemical Degradation of Rhodamine B and N, N-Dimethyl-4-nitrosoanilin Using a Boron-doped Diamond Electrode)

  • 김동석;박영식
    • 한국환경보건학회지
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    • 제36권4호
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    • pp.313-322
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    • 2010
  • The aim of this research was to apply experimental design methodology to optimization of conditions of electrochemical oxidation of Rhodamine B (RhB) and N, N-Dimethyl-4-nitrosoaniline (RNO, indicative of the OH radical). The reactions of electrochemical oxidation of RhB degradation were mathematically described as a function of the parameters of current ($X_1$), NaCl dosage ($X_2$) and pH ($X_3$) and modeled by the use of the central composite design. The application of response surface methodology (RSM) yielded the following regression equation, which is an empirical relationship between the removal efficiency of RhB and RNO and test variables in a coded unit: RhB removal efficiency (%) = $94.21+7.02X_1+10.94X_2-16.06X_3+3.70X_1X_3+9.05X_2X_3-{3.46X_1}^2-{4.67X_2}^2-{7.09X_3}^2$; RNO removal efficiency (%) = $54.78+13.33X_1+14.93X_2- 16.90X_3$. The model predictions agreed well with the experimentally observed result. Graphical response surface and contour plots were used to locate the optimum point. The estimated ridge of maximum response and optimal conditions for the RhB degradation using canonical analysis was 100.0%(current, 0.80 A; NaCl dosage, 2.97% and pH 6.37).

고 에너지 (1.5 MeV) Boron 이온 주입과 초기 산소농도 조건이 깊은 준위에 미치는 영향에 관한 연구 (The Effects of high Energy(1.5MeV) B+ ion Implantation and Initial Oxygen Concentration Upon Deep Level in CZ Silicon Wafer)

  • 송영민;문영희;김종오
    • 한국재료학회지
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    • 제11권1호
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    • pp.55-60
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    • 2001
  • 고 에너지 (1.5 MeV) 이온 주입된 Boron의 농도와 silicon 기판의 초기 산소 농도의 변화에 따라 silicon기판에 형성된 결정 결함 및 금속 불순물의 Gettering 효율에 대하여 DLTS(Deep Level Transient Spectroscopy), SIMS(Secondary ion Mass Spectroscopy), BMD(Bulk Micro-Defect) analysis 및 TEM (Transmission Electron Microscopy)을 이용하여 연구하였다. 이온 주입 전후의 DLTS 결과를 확산로 및 RTA를 이용한 열처리 전후의 DLTS 결과와 비교할 때 이온 주입 전 시편에서 볼 수 있는 공공에 의한 깊은 준위는 열처리 온도의 증가에 따라 금속 불순물과 관련된 깊은 준위로 천이함을 알 수 있다. 또한 고온 열처리의 경우, 초기 산소 농도가 높을수록 깊은 준위의 농도가 감소함을 볼 때 초기 산소 농도가 높을 수록 gettering 효율 측면에서 유리한 것으로 사료된다

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열간성형공법으로 제작된 현가부품의 피로특성 연구 (Study on Fatigue Characteristic of Suspension Part Using Hot Forming)

  • 서창희;박명규;박종규;김영석
    • 대한기계학회논문집A
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    • 제37권3호
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    • pp.339-344
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    • 2013
  • 보론강을 사용하는 열간성형은 경량화된 자동차 차체부품의 생산을 위해서 최근에 널리 사용되고 있으며, 열간성형 후 약 1,500 MPa 정도의 고강도 특성을 얻을 수 있다. 그러나 열간성형이 현가부품에 사용되기 위해서는 고강도 특성보다 피로특성이 더 중요해진다. 따라서, 본 연구에서는 열간성형에 의해 제작된 자동차 현가부품의 일종인 튜블러 토션빔 액슬의 피로특성에 대하여 연구하였다. 냉각방식에 따른 보론강의 저주기 피로특성에 대하여 연구하였으며, 튜블러 토션빔 액슬의 피로수명을 예측하기 위해서 구조 및 피로해석이 수행되었다. 튜블러 토션빔 액슬의 토션빔 영역에서 응력집중이 발생하였으며, 열간성형에 의한 고강도화가 튜블러 토션빔 액슬의 수명향상에 큰 영향을 미쳤다.

PMD용 BKNO3 금속화약의 제조공정 및 특성분석 (The Manufacturing Process and Characteristic Analysis of BKNO3 Metal-Explosive for PMD)

  • 심정섭;김상백;안길환;김준형;류병태
    • 한국추진공학회지
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    • 제22권3호
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    • pp.90-96
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    • 2018
  • 고체 점화제 $BKNO_3$는 항공우주 및 유도탄 등의 점화제로 널리 적용되는데 본 연구에서는 $BKNO_3$의 제조공정과 특성평가를 수행하였다. 이 고체 점화제는 금속분말과 산화제 그리고 유기 고분자물질(결합재)로 구성된다. 증발법(evaporation process)을 사용하여 원료들을 균질하게 혼합하였다. CEA 프로그램을 사용하여 $BKNO_3$의 물질특성 및 열적 반응 해석을 통한 최적 조성비를 설계하였으며, 입도, 형상, 감도, 열량 분석 등의 특성 평가를 수행하여 결과를 분석하였다.

Plunger 타입 유량조절장치를 적용한 덕티드 로켓용 가스발생기 개발 및 성능분석 : Part I (Development and Performance Analysis of Gas Generator with Plunger-type Flow Control Valve for Ducted Rocket : Part I)

  • 이정표;한승주;조성봉;김경무;임재일;이기연
    • 항공우주시스템공학회지
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    • 제15권3호
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    • pp.79-86
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    • 2021
  • 추력조절이 가능한 가변유동형 덕티드 로켓(VFDR; Variable Flow Ducted Rocket)의 기초연구 목적으로 가스발생기와 유량조절장치를 개발하여 지상연소시험을 수행하였다. 연소시험을 통하여 본 개발에 대한 내열성, 연소시간, 압력 및 온도와 같은 성능 요구조건의 충족 여부를 확인하였으며 Boron/MgAl/AP 등을 혼합한 연료농후 고체추진제의 연소특성을 분석하였다. 유량조절장치는 Plunger 타입으로 개발하여 토출면적 조절로 유량 및 압력을 제어할 수 있음을 확인하였다. 그러나 토출 유로 내 연소 생성물 부착으로 인한 토출면적 감소에 따라 압력 안정화 구간 없이 연소압력이 증가하는 경향을 나타내었다. 토출면적 감소로 인한 압력증가의 연소특성 분석은 본 논문의 Part 2에서 다루어진다.

Analysis of the Nuclear Subcriticality for the High Density Spent Fuel Storage at PWR Plants

  • Koh, Duck-Joon;Yang, Ho-Yeon;Kim, Byung-Tae;Jo, Chang-Keun;Hokyu Ryu;Cho, Nam-Zin
    • 한국원자력학회:학술대회논문집
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    • 한국원자력학회 1998년도 춘계학술발표회논문집(2)
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    • pp.470-475
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    • 1998
  • The marginal nuclear criticality analysis for the high density spent fuel storage at a PWR plant was carried out by using the HELIOS and CASMO-3 codes. More than 20 % of the calculated reactivity saving effect is observed in this analysis. This mainly comes from the adoption of some important fission products and B-10 in the criticality analysis. By taking burnup and boron credits, the high capacity of the spent fuel storage rack can be more fully utilized, reducing the space of storage. Larger storage for a given inventory of spent fuel should result in remarkable cost savings and mort importantly reduce the risks to the public and occupational workers.

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핫스탬핑강의 너트 프로젝션 용접시 너트 재질이 용접부 파단모드 변화에 미치는 영향 (Effect of Chemical Composition of Nut Material on the Fracture Behavior in Nut Projection Welding of Hot-Stamped Steel Sheet)

  • 임성상;김영태;천은준;남기성;박영환;김재완;이선영;최일동;박영도
    • Journal of Welding and Joining
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    • 제34권2호
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    • pp.1-10
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    • 2016
  • The use of materials for modern lightweight auto-bodies is becoming more complex than hitherto assemblies. The high strength materials nowadays frequently used for more specific fields such as the front and rear sub frames, seat belts and seats are mounted to the assembled body structure using bolt joints. It is desirable to use nuts attached to the assembled sheets by projection welding to decrease the number of loose parts which improves the quality. In this study, nut projection welding was carried out between a nut of both boron steel and carbon steel and ultra-high strength hot-stamped steel sheets. Then, the joints were characterized by optical and scanning electron microscope. The mechanical properties of the joints were evaluated by microhardness measurements and pullout tests. An indigenously designed sample fixture set-up was used for the pull-out tests to induce a tensile load in the weld. The fractography analysis revealed the dominant interfacial fracture between boron steel nut weld which is related to the shrinkage cavity and small size fusion zone. A non-interfacial fracture was observed in carbon steel nut weld, the lower hardness of HAZ caused the initiation of failure and allowed the pull-out failure which have higher in tensile strengths and superior weldability. Hence, the fracture load and failure mode characteristics can be considered as an indication of the weldability of materials in nut projection welding.

Coating Layer Behavior Analysis of Al-Si Coated Boron Steel in Hot Bending Process

  • 이양;강충길
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2009년도 추계학술대회 논문집
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    • pp.307-310
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    • 2009
  • Nowadays, the usage of high strength steel has been growing in automobile industry mainly as structural parts since for its lightweight and high strength properties the oil crisis happened. Owing to poor formability, complex-shaped high-strength steel components are invariably produced through hot press forming. The high-strength steel sheets are in so me instances used with an Al-Si-coating with a view to prevent scaling of components during hot press forming. How ever, friction and fracture characteristics of Al-Si-coated high-strength steel during hot press forming process have not yet been investigated. In this paper, the formed parts which were formed in hot bending process were investigated by using EDS. SEM and nano indenter in order to analysis the coating layer behavior.

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