• 한국재료학회지
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• 제11권12호
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• pp.1028-1034
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• 2001

The 2.5 vol% TiNi/6061Al composites were fabricated by permanent mold casting. The microstructures and tensile test for the cold rolled composites with maximum 50% reduction ratio were investigated. In the case of TiNi fiber with 2mm interval in preform, the interface bonding of fabricated composites were good, interface diffusion layer of this composites was made by the mutual diffusion. Transverse section of TiNi fiber was decreased with increasing reduction ratio and longitudinal section of TiNi fiber showed multiple wave phenomenon. And the tensile strength of composites at 38% reduction ratio was the most high. In the case of over 38% reduction ratio, the decrease of the tensile strength was due to TiNi fiber rupture by excess working. The fracture mode was appeared brittle fracture with increasing reduction ratio.

• 한국해양공학회지
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• 제31권3호
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• pp.241-247
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• 2017

Plywood, which is created by bonding an odd number of thin veneers perpendicular to the grain orientation of an adjacent layer, was developed to supplement the weak points such as contraction and expansion of conventional wood materials. With structural merits such as strength, durability, and good absorption against impact loads, plywood has been adopted as a structural material in the insulation system of a membrane type liquefied natural gas (LNG) carrier. In the present study, as an attempt to resolve recent failure problems with plywood in an LNG insulation system, conventional PF (phenolic-formaldehyde) resin plywood and its alternative MUF (melamine-urea-formaldehyde) resin bonded plywood were investigated by performing material bending tests at ambient ($20^{\circ}C$) and cryogenic ($-163^{\circ}C$) temperatures to understand the resin and grain effects on the mechanical behavior of the plywood. In addition, the failure characteristics of the plywood were investigated with regard to the grain orientation and testing temperature.

• The Journal of Advanced Prosthodontics
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• 제12권3호
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• pp.157-166
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• 2020

PURPOSE. The aim of this study was to evaluate the clinical performance and reliability of plasma sprayed nanostructured zirconia (NSZ) coating. MATERIALS AND METHODS. This study consisted of three areas of analysis: (1) Mechanical property: surface roughness of NSZ coating and bond strength between NSZ coating and titanium specimens were measured, and the microstructure of bonding interface was also observed by scanning election microscope (SEM). (2) Biocompatibility: hemolysis tests, cell proliferation tests, and rat subcutaneous implant test were conducted to evaluate the biocompatibility of NSZ coating. (3) Mechanical compatibility: fracture and artificial aging tests were performed to measure the mechanical compatibility of NSZ-coated titanium abutments. RESULTS. In the mechanical study, 400 ㎛ thick NSZ coatings had the highest bond strength (71.22 ± 1.02 MPa), and a compact transition layer could be observed. In addition, NSZ coating showed excellent biocompatibility in both hemolysis tests and cell proliferation tests. In subcutaneous implant test, NSZ-coated plates showed similar inflammation elimination and fibrous tissue formation processes with that of titanium specimens. Regarding fatigue tests, all NSZ-coated abutments survived in the five-year fatigue test and showed sufficient fracture strength (407.65-663.7 N) for incisor teeth. CONCLUSION. In this study, the plasmasprayed NSZ-coated titanium abutments presented sufficient fracture strength and biocompatibility, and it was demonstrated that plasma spray was a reliable method to prepare high-quality zirconia coating.

• Advanced Composite Materials
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• 제18권4호
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• pp.351-364
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• 2009

The thermal stability and elevated temperature mechanical properties of $SiC_P$/Al-11.7Fe-1.3V-1.7Si (Al-11.7Fe-1.3V-1.7Si reinforced with SiC particulates) composites sheets prepared by spray deposition (SD) $\rightarrow$ hot pressing $\rightarrow$ rolling process were investigated. The experimental results showed that the composite possessed high ${\sigma}_b$ (elevated temperature tensile strength), for instance, ${\sigma}_b$ was 315.8 MPa, which was tested at $315^{\circ}C$, meanwhile the figure was 232.6 MPa tested at $400^{\circ}C$, and the elongations were 2.5% and 1.4%, respectively. Furthermore, the composite sheets exhibited excellent thermal stability: the hardness showed no significant decline after annealing at $550^{\circ}C$ for 200 h or at $600^{\circ}C$ for 10 h. The good elevated temperature mechanical properties and excellent thermal stability should mainly be attributed to the formation of spherical ${\alpha}-Al_{12}(Fe,\;V)_3Si$ dispersed phase particulates in the aluminum matrix. Furthermore, the addition of SiC particles into the alloy is another important factor, which the following properties are responsible for. The resultant Si of the reaction between Al matrix and SiC particles diffused into Al matrix can stabilize ${\alpha}-Al_{12}(Fe,\;V)_3Si$ dispersed phase; in addition, the interface (Si layer) improved the wettability of Al/$SiC_P$, hence, elevated the bonding between them. Furthermore, the fine $Al_4C_3$ phase also strengthened the matrix as a dispersion-strengthened phase. Meanwhile, load is transferred from Al matrix to SiC particles, which increased the cooling rate of the melt droplets and improved the solution strengthening and dispersion strengthening.

• 한국진공학회지
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• 제10권3호
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• pp.321-327
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• 2001

Radio frequency magnetron sputtering방법으로 타켈의 Ti/si 조성과 $N_2$ 유량을 변화시켜 증착한 다양한 조성비의 Ti-Si-N 박막의 비저항 변화와 확산방지능력을 조사하였다. 높은 Si 함량을 포함한 Ti-Si-N박막내의 Si은 주로 비정질의 $Si_3N_4$ 형태로 존재하였으며 $N_2$의 양이 증가함에 따라 비저항도 증가하였다. 반면, 낮은 Si 함량을 포함한 Ti-Si-N박막은 낮은 $N_2$ 유량에서도 결정질의 TiN이 형성되었고 낮은 비저항을 나타내었다. 또한, 박막내의 N의 양이 증가함에 따라, 높은 박막의 밀도와 압축응력을 갖는 Ti-Si-N이 형성되었으며, 이는 박막 내의 N의 함량이 확산방지능력에 영향을 미치는 가장 중요한 요소 중 하나로 판단된다. 결과적으로, 29~49 at.%, Ti, 6~20 at.% Si, 45~55 at.% N 범위의 조성을 갖는 Ti-Si-N박막이 우수한 확산 억제 능력을 보유하면서 또한 낮은 비저항 특성을 나타내는데 적합한 조성 범위로 나타났다.

• 한국진공학회지
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• 제13권1호
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• pp.1-8
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• 2004

양성자 주입과 웨이퍼접합기술을 접목한 ion-cut기술로서 SOI 웨이퍼를 제조하는 기술을 개발하고자 하였다. TRIM 전산모사결과 표준 SOI 웨이퍼 (200 nm SOI, 400 nm BOX) 제조를 위해서는 65 keV의 양성자주입이 요구됨을 알 수 있었다. 웨이퍼분리를 위한 최적 공정조건을 얻기 위해 조사선량과 열처리조건(온도 및 시간)에 따른 표면변화를 조사하였다. 실험결과 유효선량범위는 6∼$9\times10^{16}$ $H^{+}/\textrm{cm}^2$이며, 최적 아닐링조건은 $550^{\circ}C$에서 30분 정도로 나타났다. 주입된 수소의 깊이분포는 ERD(Elastic Recoil Detection)와 SIMS(Secondary Ion Mass Spectrometry)측정에 의해 실험적으로 확인되었다. 아울러 상해층의 미세구조 형성기구를 X-TEM측정을 통해 조사하였다.

• 한국지반공학회논문집
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• 제20권5호
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• pp.49-58
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• 2004

시화지역 퇴적층의 퇴적환경을 분석하여 압밀특성을 연구하였다. 퇴적환경은 입도분석, 퇴적구조, 지화학특성, 간 극수 화학분석, 탄소동위원소분석을 통해 분석하였으며 조사지점에서 연속적으로 채취한 불교란 시료에 대해 압밀시험과 이방압밀삼축시험(CKoUC)을 수행하여 과압밀현상을 조사하였다. 퇴적환경 분석 결과 상부의 실트/점토 혼합층은 해성환경에서 퇴적되었으며 하부의 모래층과 점토층은 하성환경에서 퇴적된 것으로 밝혀졌다. 해성퇴적층에서는 실트와 점토의 수평층리에 의한 퇴적구조가 우세하게 나타난다. 해성퇴적층 내에서 지질학적 침식이 발생했다는 뚜렷한 증거가 없음에도 불구하고 상부 해성퇴적층의 과압밀비는 1보다 크게 나오고 있다. 상부 해성퇴적층은 삼축 응력경로에서 정규압밀 점토와 동일한 거동을 보이며, 응력상태선도에서도 지질학적 의미의 정규압밀 영역에 도시된다. 해성퇴적층의 이러한 겉보기 과압밀 현상은 퇴적속도의 차이에 의해 발생되는 연약층의 구조, 즉 입자간 화학적 결합력에 의해 발생된 것으로 설명할 수 있다.

• 대한치과교정학회지
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• 제44권5호
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• pp.246-253
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• 2014

Objective: To evaluate the bioactivity, and the biomechanical and bone-regenerative properties of Ti6Al4V miniscrews subjected to anodization, cyclic precalcification, and heat treatment (APH treatment) and their potential clinical use. Methods: The surfaces of Ti6Al4V alloys were modified by APH treatment. Bioactivity was assessed after immersion in simulated body fluid for 3 days. The hydrophilicity and the roughness of APH-treated surfaces were compared with those of untreated (UT) and anodized and heat-treated (AH) samples. For in vivo tests, 32 miniscrews (16 UT and 16 APH) were inserted into 16 Wistar rats, one UT and one APH-treated miniscrew in either tibia. The miniscrews were extracted after 3 and 6 weeks and their osseointegration (n = 8 for each time point and group) was investigated by surface and histological analyses and removal torque measurements. Results: APH treatment formed a dense surface array of nanotubular TiO2 layer covered with a compact apatite-like film. APH-treated samples showed better bioactivity and biocompatibility compared with UT and AH samples. In vivo, APH-treated miniscrews showed higher removal torque and bone-to-implant contact than did UT miniscrews, after both 3 and 6 weeks (p < 0.05). Also, early deposition of densely mineralized bone around APH-treated miniscrews was observed, implying good bonding to the treated surface. Conclusions: APH treatment enhanced the bioactivity, and the biomechanical and bone regenerative properties of the Ti6Al4V alloy miniscrews. The enhanced initial stability afforded should be valuable in orthodontic applications.

• 대한토목학회논문집
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• 제8권1호
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• pp.33-40
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• 1988

흙과 보강재 사이의 거동을 측정하는 수단으로서 hollow cylinder type의 샘플 내에 보강재를 인장방향으로 삽입하여 주위압력을 일정하게 유지한 가운데 축력(軸力)을 감소시키는 소위 삼축인장시험을 실시하였다. 인장특성(引張特性)(extensibility)이 상이(相異)한 3종류의 보강재를 사용한 결과 파괴변형율(failure strain), 최대강도후의 응력강소(loss of post-peak strength), 변형모양(deformation mode) 등이 보강재에 따라 각각 독특하였고, 파괴의 양상은 breakage 또는 pull-out 이 발생하였으며, 보강재단(補强材端)의 고정여부에 따라 보강효과가 영향을 받음이 확인되었다. 따라서 보강토해석 및 설계시 흙 및 보강재 자체의 강도(强度)와 더불어 보강재의 인장특성(引張特性)과 경계조건(境界條件)이 매우 중요한 고려요소임을 알 수 있었다.

• 한국정보통신학회논문지
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• 제16권4호
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• pp.759-764
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• 2012

고밀도집적을 위하여 전기도금과 무전해도금법을 적용하여 구리기둥주석범프(CPTB)를 제작하고, 그 특성을 분석하였다. CPTB는 ${\sim}100{\mu}m$의 피치를 갖도록 KM-1250 건식감광필름(DFR)을 사용하여 먼저 구리기둥범프(CPB)를 도금 전착시킨 다음, 구리의 산화억제를 위하여 그 위에 주석을 무전해 도금하였다. 열-압력에 따른 산화효과와 접합특성을 위하여 전기저항계수와 기계적 층밀림 전단강도를 측정하였다. 전기저항계수는 산화두께의 증가에 따라서 증가하였고, 전단강도는 $330^{\circ}C$에서 500 N의 열-압력일 때 최고치를 나타냈다. 시뮬레이션 결과에 따르면, CPTB는 시간이 경과됨에 따라 통전면적의 크기 감소의 결과를 나타냈으며, 그것은 구리의 산화에 의해 크게 영향을 받는 것으로 확인되었다.