• Title/Summary/Keyword: Bonding layer

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SEM AND CONFOCAL LASER SCANNING MICROSCOPIC STUDY ON THE CORROSION OF DENTAL RESTORATIVE RESINS (주사전자현미경과 공촛점 레이저 주사현미경을 이용한 치과용 수복레진의 부식에 관한 연구)

  • Yang, Kuy-Ho;Park, Eun-Hae;Jeong, Byung-Cho
    • Journal of the korean academy of Pediatric Dentistry
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    • v.29 no.3
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    • pp.430-438
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    • 2002
  • The aim of this study was to evaluate the resistance to degradation of four commercial composite resins-Prodigy(Kerr, USA), Vitalescence(Ultradent, USA), Z 250(3M, USA), Filtek flow(3M, USA)- in an alkaline solution. Resistance to degradation was evaluated on the basis of following parameters: (a) mass loss(%), (b) Si loss(ppm), (c) degradation depth($\mu}m$). The results were as follows: 1. There was no significant difference between Prodigy and Vitalescence, also Z 250 and Filtek flow. But, there was significant difference between former group and latter group. 2. The sequence of the degree of degradation layer depth was in descending order by Z 250, Filtek flow, Prodigy, Vitalescence. There was significant difference among the materials. 3. The sequence of the Si loss was in descending order by Filtek flow, Z 250, Prodigy, Vitalescence. There was significant difference among the materials. 4. The correlation coefficient between mass loss and degradation layer depth(r=0.714, p<0.05), mass loss and Si loss(r=0.770, p<0.05), and degradation layer depth and Si loss(r=0.930, p<0.05) were relatively high. 5. When observed with SEM, destruction of bonding was observed between resin matrix and filler. 6. When observed with CLSM, degradation layer depth of composite resin surface was observed.

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Interfacial and Tensile Properties of TiNi Shape Memory Alloy reinforced 6061 Al Smart Composites by vacuum casting (진공주조법에 의한 TiNi 형상기억합금 강화 6061Al 지적 복합재료의 계면 및 인장 특성)

  • Park, Gwang-Hun;Park, Seong-Gi;Sin, Sun-Gi;Park, Yeong-Cheol;Lee, Gyu-Chang;Lee, Jun-Hui
    • Korean Journal of Materials Research
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    • v.11 no.12
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    • pp.1057-1062
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    • 2001
  • We investigated the change of mechanical properties for TiNi shape memory alloy by heat treatment. 6061Al matrix composites with TiNi shape memory alloy as reinforcement were fabricated by vacuum casting. TiNi alloy has the maximum tensile strength at 673K treated and there is no change of tensile strength and hardness at 448K treated. The composites, prepared by vacuum casting, showed good interface bonding by vacuum casting. It was about 3$\mu\textrm{m}$ of thickness of the diffusion layer. Tensile strength of the composite was in higher than that of 6061Al alloy as increased value of about 70MPa at room temperature and about 110MPa at 363K. We thought that the increase of the tensile strength at 363K was due to reverse transformation of the TiNi shape memory alloy.

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Design Optimization of Dental Implants Using Finite Element Analysis for Injecting Bioactive Materials

  • Lee, Kang-Soo;Lee, Yong-Keun
    • Korean Journal of Materials Research
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    • v.22 no.6
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    • pp.292-297
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    • 2012
  • In order to improve osseointegration of dental implants with bone we studied an implant with holes inside its body to deliver bioactive materials based on a proposed patent. Bioactive materials can be selectively applied through holes to a patient according to diagnosis and the integration progress. After the bioactive material is applied, bone can grow into the holes to increase implant bonding and also enhance surface integration. In order to improve the concept and study the effect of bioactive material injection on implant integration, design optimization and integration research were undertaken utilizing the finite element method. A 2-dimensional simulation study showed that when bone grew into the holes after the bioactive material was injected, stress vertically distributed in the upper part of the implant was relieved and mild stress appeared at the opening of the injection holes. This confirmed the effect of the bioactive material and the contribution of the injection holes, but the maximum stress increased ten-fold at the opening. In order to reduce the maximum stress, the size, location, and the number of holes were varied and the effects were studied. When bioactive materials formed an interface layer between the implant and the mandible and four holes were filled with cortical and cancellous bones all the stress concentrated opposite to the loading side without holes disappeared. The stresses at the four outlets of the holes was mildly elevated but the maximum stress value was ten-fold greater compared to the case without the bioactive material.

Analysis of stress and stress intensity factor in bonded dissimilar materials by boundary element method (경계요소법을 이용한 이종재료 접착.접합재의 응력 및 응력세기계수 해석)

  • Yi, W.;Chung, N.Y.;Yu, Y.C.;Jeong, E.S.
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.21 no.9
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    • pp.1357-1363
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    • 1997
  • Currently it is increasing to use th bonded dissimilar materials in the various field of advanced engineering such as the highly rigid and lighter vehicle, plastic molding LSI package and metal/ceramic bonded joint. In spite of such a wide application of the bonded dissimilar materials, the evaluation method of the bonding strength has not been established yet. Therefore in this paper we analyze the interface crack problem by introducing fracture mechanics parameters as the basic research about estimating of the strength of adhesive joints. The variation of stress intensity factor according to the elastic modulus of adherend and thickness of bonded layer are investigated. Numerical results are based on the results of boundary element analysis of four different type butt joints subjected to uniaxial tension loading.

Bondline Strength Evaluation of Honeycomb Sandwich Panel For Cure Process and Moisture Absorption (경화공정 및 수분흡수에 따른 복합재료 하니콤 샌드위치 판넬의 접합강도특성 연구)

  • Choe, Heung-Seop;Jeon, Heung-Jae;Nam, Jae-Do
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.1
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    • pp.115-126
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    • 2001
  • In this paper, through a series of comparative experiments, effects of two different cure processing methods, cocure and precure, on the mechanical properties of honeycomb core materials for aircraft applications are considered. Mass of moisture accumulated into the closed cells of the sandwich panel specimen from the measured mass of moisture diffused to the full saturation state into the elements(skin, adhesive layer, Nomex honeycomb), consisting the honeycomb sandwich specimen has been calculated. Water reservoir of 70$\^{C}$ was used to have specimens absorb moisture to see the influence of moisture absorbed into sandwich panel on its mechanical properties. For the repair condition holding for 2 hours at 177$\^{C}$(350℉) temperature, a pressure due to the vapor expansion in each cell of the sandwich panel, which may result in the local separation of the interface between laminated skin and the surface of the honeycomb, has been estimated by vapor pressure-temperature relation from the thermodynamic steam table and compared to the pressure from the ideal gas state equation. The bonding strengths of the laminated skins on the flat surface of the Nomex honeycomb have been compared by the flatwise tension test and climbing drum peel test performed at room temperature for dry, wet and wet-repair specimens, respectively.

Design of Moving Coil Type Optical Pickup Actuator for Flexible Disk (유연디스크용 가동 코일형 광 픽업 엑추에이터 개발)

  • Kim, Yoon-Ki;Song, Myeong-Gyu;Lee, Dong-Ju;Park, No-Cheol;Park, Young-Pil
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2006.11a
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    • pp.479-483
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    • 2006
  • As high-definition television(HDTV) broadcasting were generalized, there have been many researches and developments about large storage capacity and fast data transfer rate in optical disk drives(ODD). Pickup actuators must have high flexible mode frequencies and gain margins. Flexible modes are caused by the flexibility of moving parts in the actuator and a servo bandwidth is limited by them. As a result, the system becomes unstable for high-speed operations in high density reading and recording. In this paper, we suggest improved modeling method that considers the bonding layer. And, flexible mode frequency of actuator is improved by Design of Experiment of lens holder. Magnet circuit is designed considering the relation with moving part. Through improving yoke design, the magnetic flux is changed and DC tilt is reduced. Consequently, we designed actuator which has high flexible mode frequency and gain margins.

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The Crystal and Molecular Structure of Fluocinolone Acetorlide $(C_{24}H_{30}F_2O_8)$ (FloucinoloneAcetonide의 결정 및 분자구조)

  • Jeong, Jong-Sun;Jo, Seong-Il;Jeong, Yong-Je
    • Korean Journal of Crystallography
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    • v.3 no.1
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    • pp.31-36
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    • 1992
  • 6, 9-Difluoro-11, 21-dihydroxyl-16, 17-[(1methylehtylidene)bis(oxy)]-pregna-1, 4-diene-3, 20-dione (fluorocinolone acetonide) , C24H3OF106, trigonal, R3 (defined as a hexagonal lattice), a =b = 17.896 k, c: 18.365 k, V=5094.3 A', Z=9, 1 (MoK a) =0.7107 A, D=1.31 g/cm3, D.: 1.328 g/cm3 T=298 K, final R=0.050 for 1101 unique observed reflections. The molecule has conformational features in common with other corticosteroids. Three molecules related by 3-fold symmetry are involved in hydrogen bonding, forming a layer of molecules perpendicular to the c-axis.

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Method of Solving Oxidation Problem in Copper Pillar Bump Packaging Technology of High Density IC (고집적 소자용 구리기둥범프 패키징에서 산화문제를 해결하기 위한 방법에 대한 연구)

  • Jung, One-Chul;Hong, Sang-Jeen;Soh, Dae-Wha;Hwang, Jae-Ryong;Cho, Il-Hwan
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.23 no.12
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    • pp.919-923
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    • 2010
  • Copper pillar tin bump (CPTB) was developed for high density chip interconnect technology. Copper pillar tin bumps that have $100{\mu}m$ pitch were introduced with fabrication process using a KM -1250 dry film photoresist (DFR), copper electroplating method and Sn electro-less plating method. Mechanical shear strength measurements were introduced to characterize the bonding process as a function of thermo-compression. Shear strength has maximum value with $330^{\circ}C$ and 500 N thenno-compression process. Through the simulation work, it was proved that when the copper pillar tin bump decreased in its size, it was largely affected by the copper oxidation.

A Study on the Etching Characteristics of $CeO_2$ Thin Films using inductively coulped $Cl_2/Ar$ Plasma (유도 결합 플라즈마($Cl_2/Ar$)를 이용한 $CeO_2$ 박막의 식각 특성 연구)

  • 오창석;김창일;권광호
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • 2000.11a
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    • pp.29-32
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    • 2000
  • Cerium oxide thin film has been proposed as a buffer layer between the ferroelectric film and the Si substrate in Metal-Ferroelectric-Insulator-Silicon (MFIS ) structures for ferroelectric random access memory (FRAM) applications. In this study, CeO$_2$thin films were etched with Cl$_2$/Ar gas combination in an inductively coupled plasma (ICP). The highest etch rate of CeO$_2$film is 230 $\AA$/min at Cl$_2$/(Cl$_2$+Ar) gas mixing ratio of 0.2. This result confirms that CeO$_2$thin film is dominantly etched by Ar ions bombardment and is assisted by chemical reaction of Cl radicals. The selectivity of CeO$_2$to YMnO$_3$was 1.83. As a XPS analysis, the surface of etched CeO$_2$thin films was existed in Ce-Cl bond by chemical reaction between Ce and Cl. The results of XPS analysis were confirmed by SIMS analysis. The existence of Ce-Cl bonding was proven at 176.15 (a.m.u.).

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Flexural performance of wooden beams strengthened by composite plate

  • Tahar, Hassaine Daouadji;Abderezak, Rabahi;Rabia, Benferhat
    • Structural Monitoring and Maintenance
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    • v.7 no.3
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    • pp.233-259
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    • 2020
  • Using bonded fiber-reinforced polymer laminates for strengthening wooden structural members has been shown to be an effective and economical method. In this research, properties of suitable composite materials (sika wrap), adhesives and two ways of strengthening beams exposed to bending moment are presented. Passive or slack reinforcement is one way of strengthening. The most effective way of such a strengthening was to place reinforcement laminates in the stretched part of the wooden beam (lower part in our case), in order to investigate the effectiveness of externally bonding FRP to their soffits. The model is based on equilibrium and deformations compatibility requirements in and all parts of the strengthened beam, i.e., the wooden beam, the sika wrap composite plate and the adhesive layer. The theoretical predictions are compared with other existing solutions. This research is helpful for the understanding on mechanical behaviour of the interface and design of the composite-wooden hybrid structures. The results showed that the use of the new strengthening system enhances the performance of the wooden beam when compared with the traditional strengthening system.