• 제목/요약/키워드: Boiling method

검색결과 520건 처리시간 0.027초

CFC 113과 대체세정제의 세정성능 비교 (Comparison of Cleaning Performance of CFC 113 and the Alternatives)

  • 노경호;최대기;이윤용
    • 분석과학
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    • 제6권5호
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    • pp.521-530
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    • 1993
  • 몬트리올의정서에 의하여 오존층 파괴물질로 규정된 전자산업의 필수불가결한 세정제인 CFC 113(1,1,2-trichloro 1,2,2,-trifluoroethane)의 사용이 앞으로 규제가 됨에 따라서 대체세정제의 개발이 활발히 진행되고 있다. 따라서 현재 시판중인 세정제의 종류는 상당히 많다. 이 중에서 Axarel 32(DuPont), Cleanthru 750H(KAO Chemical), EC-Ultra(Petroferm)를 선정하여 CFC 113과 세정성능을 비교하였다. CFC 113과 대체세정제의 세정성능 검사방법은 기본적은 물성측정, 재질호환성에 대한 실험, 증발속도의 측정, 오염물질의 제거효율에 관한 실험으로 구성되어 있다. CFC 113과 대체세정제들의 기본적인 물성들은 서로 상이하였다. 대체세정제는 비점이 높고 표면장력과 점도가 CFC 113보다 큰 값을 가지고 있다. 전자산업에서의 로진계 flux를 오염물질로 하고 각기의 세정제와의 용해도를 비교한 결과 비극성 유기물질은 abietic acid에 대한 용해도는 서로 유사하였으나 대체세정제의 경우 극성 유기물질에 대한 용해도는 CFC 113에 비해서 월등히 좋았다. 또한 비점이 낮은 CFC 113의 건조성은 대체세정제와는 비교할 수 없을 정도로 우수하였고 특히 대체세정제 중에서 EC-Ultra는 건조성이 매우 낮았다. CFC 113과 대체세정제에서의 PCB의 구성 재질인 FR4와 Cu-coated FR4에 대한 재질호환성은 거의 비슷하였다. Abietic acid의 제거효율에 관한 실험에서는 초음파 세정에 의해서 우수한 세정효과를 보여 주었으며 침적에 의해 세정에서는 건조성이 좋은 세정제가 유리하지만 초음파 세정에 의해서 대체세정제간의 제거효율의 차이는 거의 없었다. CFC 113의 대체세정제로서 로진계 flux를 제거하는 대체세정제간의 세정성능은 큰 차이는 없으나 최종 세정제로 선정하기 위해서는 세정장치의 적용, 환경문제 및 경제성의 고려가 병행되어야 한다.

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담금 방법을 달리한 오이지의 숙성 중 특성 변화 (Changes of Physicochemical and Sensory Characteristics of Korean Pickled Cucumber with Different Preparation Methods)

  • 박미원;박용곤;장명숙
    • 한국식품영양과학회지
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    • 제23권4호
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    • pp.634-640
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    • 1994
  • 담금초기 소금물의 농도와 온도를 달리한 오이지의 숙성 중 품질요소인 pH, 산도, 색도, 조직감 등의 이화학적, 관능적 특성 변화를 조사하였다. 10% 소금물을 끓여 바로 부은 A처리구의 pH는 숙성 3일 경과시 3.30으로 급격히 감소하였고, 20% 소금물을 끓여 바로 부은 B처리구는 다른 처리구에 비해 숙성 40일 까지 pH가 4.16으로 완만하게 감소하였다. 산도는 모든 숙성 기간에서 A처리구가 가장 높은 값을 나타내었고, 소금 농도의 경우 숙성 3일 후 A처리구가 30%, B가 45%, C가 36%의 높은 소금침투율을 보였으나 숙성기간이 경과하면서 점차 증가속도가 완만하였다. 색도 변화에서 백색도는 모두 숙성 3일에 가장 높은 수치를 보인 후 감소하였고, 녹색도는 B처리구가 숙성 40일 까지 낮은 값을 보인 반면 황색도는 가장 높은 값을 나타내었다. 오이지의 절단강도는 숙성에 의해 생오이 보다 증가하였으나 담금초기 소금물의 농도와 온도의 상태에 따라 오이지의 부위에 각기 다른 특성을 나타내었고, 최대 절단력을 나타내는 숙성일수에 있어서도 차이가 있음을 알 수 있었다. 도한 오이지의 부위 중 밑부위가 가운데 또는 꼭지부위에 비해 최대 절단강도를 보이는 숙성일수가 짧았다. 오이지 담금시 B처리구는 빠른 숙성 시일내에 오이지를 얻을 수는 있으나 오이지의 풍미와 조직감 특성이 떨어지는 것으로 판명되었고, 20% 소금물을 가열, 냉각 후 첨가한 C처리구는 오이지의 색상이 지나치게 퇴색되는 것으로 나타나 본 실험에서 이용한 전통적인 오이지 담금방법 중에서는 10% 소금물을 가열한 후 바로 오이에 첨가하는 방법이 가장 좋은 오이지의 조직감 및 관능적 특성을 나타내었다.

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설비공학 분야의 최근 연구 동향: 2014년 학회지 논문에 대한 종합적 고찰 (Recent Progress in Air-Conditioning and Refrigeration Research: A Review of Papers Published in the Korean Journal of Air-Conditioning and Refrigeration Engineering in 2014)

  • 이대영;김사량;김현정;김동선;박준석;임병찬
    • 설비공학논문집
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    • 제27권7호
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    • pp.380-394
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    • 2015
  • This article reviews the papers published in the Korean Journal of Air-Conditioning and Refrigeration Engineering during 2014. It is intended to understand the status of current research in the areas of heating, cooling, ventilation, sanitation, and indoor environments of buildings and plant facilities. Conclusions are as follows. (1) The research works on the thermal and fluid engineering have been reviewed as groups of heat and mass transfer, cooling and heating, and air-conditioning, the flow inside building rooms, and smoke control on fire. Research issues dealing with duct and pipe were reduced, but flows inside building rooms, and smoke controls were newly added in thermal and fluid engineering research area. (2) Research works on heat transfer area have been reviewed in the categories of heat transfer characteristics, pool boiling and condensing heat transfer and industrial heat exchangers. Researches on heat transfer characteristics included the results for thermal contact resistance measurement of metal interface, a fan coil with an oval-type heat exchanger, fouling characteristics of plate heat exchangers, effect of rib pitch in a two wall divergent channel, semi-empirical analysis in vertical mesoscale tubes, an integrated drying machine, microscale surface wrinkles, brazed plate heat exchangers, numerical analysis in printed circuit heat exchanger. In the area of pool boiling and condensing, non-uniform air flow, PCM applied thermal storage wall system, a new wavy cylindrical shape capsule, and HFC32/HFC152a mixtures on enhanced tubes, were actively studied. In the area of industrial heat exchangers, researches on solar water storage tank, effective design on the inserting part of refrigerator door gasket, impact of different boundary conditions in generating g-function, various construction of SCW type ground heat exchanger and a heat pump for closed cooling water heat recovery were performed. (3) In the field of refrigeration, various studies were carried out in the categories of refrigeration cycle, alternative refrigeration and modelling and controls including energy recoveries from industrial boilers and vehicles, improvement of dehumidification systems, novel defrost systems, fault diagnosis and optimum controls for heat pump systems. It is particularly notable that a substantial number of studies were dedicated for the development of air-conditioning and power recovery systems for electric vehicles in this year. (4) In building mechanical system research fields, seventeen studies were reported for achieving effective design of the mechanical systems, and also for maximizing the energy efficiency of buildings. The topics of the studies included energy performance, HVAC system, ventilation, and renewable energies, piping in the buildings. Proposed designs, performance performance tests using numerical methods and experiments provide useful information and key data which can improve the energy efficiency of the buildings. (5) The field of architectural environment was mostly focused on indoor environment and building energy. The main researches of indoor environment were related to the evaluation of work noise in tunnel construction and the simulation and development of a light-shelf system. The subjects of building energy were worked on the energy saving of office building applied with window blind and phase change material(PCM), a method of existing building energy simulation using energy audit data, the estimation of thermal consumption unit of apartment building and its case studies, dynamic window performance, a writing method of energy consumption report and energy estimation of apartment building using district heating system. The remained studies were related to the improvement of architectural engineering education system for plant engineering industry, estimating cooling and heating degree days for variable base temperature, a prediction method of underground temperature, the comfort control algorithm of car air conditioner, the smoke control performance evaluation of high-rise building, evaluation of thermal energy systems of bio safety laboratory and a development of measuring device of solar heat gain coefficient of fenestration system.

장옹(腸癰)에 있어서 종양(腫瘍).농양(膿瘍).궤양(潰瘍)의 진단(診斷)과 치료(治療)에 관(關)한 고찰(考察) ('Studies on diagnosis and Treatment of tumor.abscess.ulcer in intestinal carbuncle')

  • 한규언;류봉하;박동원;류기원;장인규
    • 대한한방내과학회지
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    • 제11권1호
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    • pp.93-107
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    • 1990
  • Studies on diagnosis and treatment of tumor . abscess . ulcer in intestinal carbuncle were carried out. The result of studies were summerized as follows: 1. By Nai-Gyung carbuncle-tumor arose from disharmony between nutrient and defensive because of cold, abscess arose from fever victory between cold and fever, ulcer arose from decreasing function of Bi-Kam year. By latter literature Bi-Kam year could be interpreted that spleen stomach was invaded evil influence from unattainable vital force of the earth. 2. Sites of intestinal carbuncle were large intestine, small intestine, intestinal inside or outside between large and small intestine, Intestinal carbuncle was common name of a disease about large intestinal carbuncle, small intestinal carbuncle, pelvic intestinal carbuncle, shrink leg intestinal carbuncle etc.. Pain appeared Chunchu-Hyul in large intestinal carbuncle, and Gwanweon-Hyul in small intestinal carbuncle. 3. On abdominal diagnosis tumor had indistinct pain of Gwanweon Chunchu, edema and heary feeling in low abdomen, no excessive pain by hand press and intestinal boiling sound. In abscess pain descended from right side of low abdomen to huckle, and there was rejection against press, feeling about fever,water sound with flank movement. In ulcer hand approach was difficult since excessive pain diffuse to whole abdomen, and perforating ulcer sometimes caused a serious symptom of umbilical pus. 4. On fecal and urinary diagnosis in tumor urine was yellowish red pollakiuria like gonorrhoea and occasional constipation. In abscess uncomfortable rough pain short red early urine like gonorrhoea appeared during urination, and constipation with stinging pain appeared during defecation. In ulcer red rough pyuria appeared, and stinging and pain with puruloid blood appeared during defecation. 5. On treatment in tumor Daiwhang-Tang Daisenggi-Tang Dangui-Jun by dissipation method, calming down method, interior reliance maturation method, in abscess Mokdan-San Euiiin-Tang Jeokduiin-Tang by the method of water repelling pus discharge, acute breaking, in ulcer Takridanggui-Tang Paljin-Tang Bojungikki-Tang were each used by the method of interior reliance, virulence astriction, supplement vital force and blood, supplement spleen stomach. 6. On treatment patient may have to be careful of excessive moving and suprising anxiety. Abuse of acupuncture and moxibustion made patient worse, misuse of analgesics purgative intestinal irrigation etc. could provoke difficult diagnosis and perforation. So you must treat after exact diagnosis. 7. Prognosis of ease tumor ease abscess ease ulcer and ease astriction was good. If the intestinal carbuncle were not to promote to abscess and ulcer for a long time, its prognosis was bad and it could metastasize to cancer because of dark purple with hardness. So tumor abscess ulcer in intestinal carbuncle may be significant of precancerous lesion.

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Protein Quality Evaluation of Cooked Hagfish (Eptatretus burgeri) Meats

  • Hwang, Eun-Young;Lee, Jin-Hwa;Ryu, Hong-Soo;Park, Nam-Gyu;Chun, Soon-Sil
    • Preventive Nutrition and Food Science
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    • 제7권3호
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    • pp.287-292
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    • 2002
  • The effect of cooking methods on in vivo and in vivo indices of the protein quality of hagfish meat were investigated. In vivo protein digestibilities of cooked meats (81.3~83.5 %) were not significant different (p<0.05) from those of van meat (82.9%), with the exception of steamed (11$0^{\circ}C$, 15 min) meat (86.3 %). Convection oven cooking (22$0^{\circ}C$, IS min) resulted in a higher trypsin indigestible substrate (TIS, 49.2 mg/g solid) compared with that of raw meat (38.9 mg/g solid). free amino acid content of raw meat was decreased after boiling (10$0^{\circ}C$, 10min). Both convection oven and microwave cooking (2,450 MHz, 3 min) decreased available lysine from 4.9g/16g N to 3.8~4.1g/16g N. In vivo apparent protein digestibilites (AD) of hagfish meat were similar fur raw (92.4%) and cooked meats, but were somewhat lower than ANRC (Animal Nutrition Research Council) casein (945%). The PERs (3.7~4.1) and NPRs (3.7~4.9) of cooked meats were significantly higher (p<0.05) than those of raw meat (PER 3.3, NPR 3.6 and ANRC casein (PER 2.5, NPR 2.6), despite their lower in vivo protein digestibilities. These results demonstrate that cooking at optimal conditions resulted in remarkably positive effects on in vivo and in vivo protein qualities of hagfish meats. Therefore, steamed hagfish meat is an excellent source of high quality protein from seafood products.

콜타르 유분 중에 함유된 인돌의 고순도 정제 - 용액 결정화에 의한 인돌 유사 비점 혼합물의 분리 - (High-Purity Purification of Indole Contained in Coal Tar Fraction - Separation of Close Boiling Mixtures of Indole by Solute Crystallization -)

  • 김수진;강호철;정화진
    • 공업화학
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    • 제21권2호
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    • pp.238-241
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    • 2010
  • 콜타르 유분(유출온도범위: $240{\sim}265^{\circ}C$)으로부터 추출-증류의 조합에 의해 회수한 54.3 wt% 인돌 유출액(유출온도범위 $250{\sim}255^{\circ}C$)을 원료로 사용하여 용액 결정화 조작을 행해 인돌의 고순도 정제를 검토했다. 원료 유출액은 8성분(quinoline, iso-quinoline, indole, quinaldine, 1-methylnaphthalene, 2-methylnaphthalene, biphenyl, phenyl ether)으로 구성되어 있다. 결정화 조작의 용매로서는 노말헥산을, 냉매로서는 메탄올 수용액(50 : 50 vol%)을 각각 사용하였으며, 결정화 장치로서는 재킷이 부착된 pyrex제 유리 회분 교반기를 사용했다. 결정화 온도와 용매/원료의 초기 체적비의 증가는 인돌의 순도를 향상시켰으나, 역으로 수율을 저하시켰다. 석출된 결정의 세정조작 없이, 노말헥산을 용매로 사용한 용액 결정화 조작에 의해 고순도(99.3 wt%)의 인돌을 고수율(50%)로 회수할 수 있었다.

페인트 도장공사의 색관리에 관한 연구 (A study on the color controlled of painter's work)

  • 심명섭;이현정
    • 한국건축시공학회지
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    • 제3권1호
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    • pp.107-114
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    • 2003
  • This study aims to find methods that prevents aging of buildings paint coating and that limits defects in construction. Defects in painting can occur in four stages: pure paint, during painting, after the paint coating has dried, and after some period of time has passed after coating. Paint may become bad due to precipitation of pigments, formation of membranes, and seeding during manufacturing. Therefore, it is important that the paint is well mixed and kept airtight at a cool, dark place. Indents, paint brush strokes, orange peel, separation of colors, and paint running and spreading during the paint work process can be prevented by using high quality materials and applying a high-level of construction method. After the paint coating has dried, boiling, yellowing, poor drying, poor bonding, and/or glen deficiency may occur. These are influenced by the levels of cleanness of the dried product, drying temperature and hydration. Then, when the coating has been left dried for some period of time, cracking, peeling, scaling, swelling, discoloring, and/or rusting may develop due to the ultraviolet and contaminants in the air. Since these defects occur due to inappropriate construction schedule and/or hot and humid condition, one must use weatherproof materials. Furthermore, poor paint color may be caused by contamination in the sample plate, discoloration, and/or discrepancies in colors which are due to material differences, level of glossiness, degree of dispersion, dual color property of metallic colors, precipitation of pigments, etc. One should achieve reduction in construction cost and effectiveness in paint work by limiting contaminations in the construction site and strictly observing to construction regulations.

Effect of Do-In (Prunus persica L. BATSCH) Water Extract (PPE) on Concentration of Extracellular Acetylcholine in the Rat Hippocampus

  • Gong Dae-Jong;Kim Geun-Woo;Koo Byung-Soo
    • 대한한의학회지
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    • 제25권4호
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    • pp.1-7
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    • 2004
  • Objective : This study was designed to examine the effects of orally administered Prunus persica water extract (PPE), which is used as herbal medicine, for treatment of Yu Xue (stasis of blood) and tacrine on the basal concentration of extracellular acetylcholine in the hippocampus of rats. Methods: To investigate the effects of PPE and tacrine on concentration of extracellular acetylcholine in the hippocampus of rats, the microdialysis technique, under the same experimental conditions, was used. And we used male Wistar rats which were 7 weeks of age and 210-290 g. PPE was extracted with boiling water, and the rats were anesthetized with pentobarbital Na. Their skulls were exposed and a hole was drilled for implantation of a microdialysis probe. In order to increase the recovery of acetylcholine, a probe with a long membrane was used. One day after surgery, the microdialysis probe was perfused with Ringer's solution at a flow rate of 1.5 l/min. The acetylcholine concentration in dialysis samples was measured by high-performance liquid chromatography (HPLC) with electrochemical detection. AChE activity was measured using the radiometric method, as described by Sherman. Results : The comparative effects of PPE and tacrine on hippocampal extracellular acetylcholine concentration was that these cholinesterase inhibitors produced dose-dependent increases in the extracellular acetylcholine concentration. And the effect of PPE and tacrine on rat brain AChE activity was that PPE produced maximal inhibition at 1 h after administration, when AChE activity was 44% of the intact level. AChE activity gradually recovered thereafter, and reached 78% of the intact level at 12 h after administration. Conclusion : In this study, PPE has a potent activity and a long-lasting effect on the central cholinergic system, in terms of the basal concentration of extracellular acetylcholine in the hippocampus and the AChE activity in the brain of rats. And oral administration of PPE increased dose-dependently the basal concentration of extracellular acetylcholine in the hippocampus of rats. PPE may be one of the more useful cholinesterase inhibitors for the treatment of Alzheimer's disease.

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Production techniques to Improve the Quality of Steamed and Freeze-Dried Mature Silkworm Larval Powder

  • Ji, Sang-Deok;Son, Jong-Gon;Kim, Seong-wan;Kim, Nam-Suk;Kim, Kee-Young;Kweon, Hae-Yong;Seong, Gyu-Byeong;Koh, Young-Ho
    • International Journal of Industrial Entomology and Biomaterials
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    • 제34권2호
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    • pp.17-22
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    • 2017
  • Cooked mature silkworms have received increasing attention as a new source of income for sericultural farms. Quality improvement of these worms as the end-product requires prevention of the following: inclusion of unfertilized silkworm eggs, mixing with impurities, producing undercooked or overcooked mature larvae, and mixing spewed silk substance. Preventing unfertilized eggs and impurities and reducing undercooked or overcooked mature larvae can be achieved by sericultural farms. However, the prevention of spewed silk substance requires the development of new techniques. This study developed new techniques for optimum cold storage temperature, soaking, and hydro-thermal treatment to minimize the spewing of mature larvae prior to steaming: when larvae mature after 7 days on the $5^{th}$ instar, they should be soaked in water at room temperature of $25^{\circ}C$ immediately upon collection and stored at $8^{\circ}C$ for less than 3 days. They should be soaked in boiling water for approximately 10 s immediately before steaming to kill the larvae and cooked with steam. This method allows for the production of high-quality mature larvae without spewed silk substance. These new techniques will considerably improve the production of well-cooked quality mature larvae by minimizing silk substance spewed out from the larvae.

Quality Characteristics of Beef by Different Cooking Methods for Frozen Home Meal Replacements

  • Kim, Kwang-Il;Lee, Sang-Yoon;Hwang, In-Guk;Yoo, Seon-Mi;Min, Sang-Gi;Choi, Mi-Jung
    • 한국축산식품학회지
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    • 제35권4호
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    • pp.441-448
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    • 2015
  • Blanching beef for use in home meal replacements (HMR) is an important process that determines the final quality of the beef after the cooking process. Thermal pretreatment also minimizes the change in quality during the main cooking process or storage. In this study, beef samples were washed and sliced, then treated by immersion in boiling water (1-10 min), steaming (1-10 min), or pan-frying in oil (30-240 s). The color after each thermal treatment showed higher L* and b* values and lower a* values compared with the raw beef, except for the pan-frying thermal treatment. The total color difference (∆E) and pH value were significantly increased by panfrying (p<0.05). There was no significant difference in the shear force of the beef samples, except for the sample pan-fried for 210 s. The nutritional content of beef was measured as the moisture, protein, fat, and ash contents, which were 69.96, 16.64, 3.49, and 1.13%, respectively, in raw beef. After thermal treatment, the crude protein and fat contents were increased, whereas the moisture and ash contents decreased. The mineral content, including Na, Mg, Fe, and Ca was highest after pan-frying. The heat treatment decreased microorganisms in all the samples. The total bacteria count in raw beef was 4.5-4.7 Log CFU/g, whereas the bacteria count decreased to 2.2-2.8 Log CFU/g after blanching. Thermophilic bacteria, coliform, mold, and yeast not detected in any thermally treated sample.