• 한국고분자학회:학술대회논문집
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• 한국고분자학회 2006년도 IUPAC International Symposium on Advanced Polymers for Emerging Technologies
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• pp.179-179
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• 2006

PLGA/HA composite scaffold fabricated by GF/PL method showed enhanced mechanical property, hydrophilicity and osteoconductivity compared with the SC/PL scaffolds, and this enhancement was most likely due to a higher extent of exposure of HA particles to the scaffold surface. The biodegradable polymer/bioceramic composite scaffolds fabricated by the GF/PL method could enhance bone regeneration efficacy for the treatment of bone defects compared with conventional composite scaffolds.

• 한국세라믹학회지
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• 제27권6호
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• pp.721-728
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• 1990

Hydroxyapatite powders were synthesized with Ca/P=1.67 and pH=11 by precipitaton method, after characterization of these specimen, behavior in Ringer's solution and biocompatibility of hydroxyapatite, such as cytotoxity test and implantation test, were investigated. The hydroxyapatite ceramics had structural stability in Ringer's solution, and hydroxyapatite ceramics did not prevent cell growing and exhibit any cytotoxic effects. In implantation of hydroxyapatite ceramics into muscle under abdome of guinea pig, hydroxyapatite ceramics did not show any symptom of rejection for cellular texture.

• The Journal of Advanced Prosthodontics
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• 제9권3호
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• pp.200-207
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• 2017

PURPOSE. In this study, three bioceramic materials, [IPS Empress CAD (Ivoclar), IPS e.max CAD (Ivoclar), and Lava Ultimate CAD (3M ESPE)] were treated with three commercial mouthrinses [Listerine, Tantum Verde, and Klorhex]; and changes in colour reflectance and surface roughness values were then quantitatively assessed. MATERIALS AND METHODS. One hundred and twenty ceramic samples, with dimensions of $2{\times}12{\times}14mm$, were prepared and divided into nine sample groups, except three control samples. The samples were immersed in the mouthrinse solutions for 120 hrs, and changes in colour reflectance and surface roughness values were measured by UV light spectrophotometry (Vita Easyshade; VITA Zahnfabrik) and by profilometer device (MitutoyoSurftest SJ-301), respectively. The change of surface roughness was inspected by Scanning Electron Microscopy (SEM) and Atomic Force Microscopy (AFM). RESULTS. There was a positive correlation between the ${\Delta}E$ and increase in the surface roughness. Two of the ceramic materials, IPS Empress and Lava Ultimate, were affected significantly by the treatment of the mouthrinse solutions (P<.05). The most affecting solution was Tantum Verde and the most affected material was Lava Ultimate. As expected, the most resistant material to ${\Delta}E$ and chemical corrosion was IPS e max CAD among the materials used. CONCLUSION. This work implied that mouthrinse with lower alcohol content had less deteriorating effect on colour and on the surface morphology of the bioceramic materials.

• 한국토양환경학회지
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• 제5권2호
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• pp.99-105
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• 2000

본 연구는 Pb으로 오염된 토양을 Biofilter에 의한 적용가능성을 판단하고 충전물질, bed수 그리고 미생물 접종에 따른 Pb의 이동억제효과의 변화를 Pilot plants의 실험을 하였으며 토양의 분해정도를 CODcr/TOC ratio로써 안정화 지표에 대한 변화를 검토하였다. 생물여과는 오염된 물질을 생물여과상를 통과시켜 충전물질표면에 부착되어있는 생물막의 각종미생물들에 의한 경계면을 통하여 물질의 상호교환 및 전환이 생기며 생물막내에 흡수된 물질을 생물학적으로 처리하는 방법의 일종이다. 본 연구는 오염된 토양에 lead nitrate를 첨가시켜 납을 1,000㎎/kg dry soil로 인공적으로 조제한후 충전물질로는 퇴비, 바이오세라믹 그리고 퇴비와 바이오세라믹을 중량비로 7:3으로 하였고, 1단, 2단, 3단으로 하고 이에따라 생물흡착제로 'Aspergillus niger'를 이용하며 납의 이동억제효과의 변화를 검토하였다.

• 대한기계학회논문집A
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• 제38권11호
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• pp.1273-1281
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• 2014

조직공학은 손상된 골 조직 및 장기를 복원, 재생, 그리고 복구할 수 있는 잠재력을 가진 새로운 학문 분야이다. 인산칼슘계 세라믹스인 삼인산칼슘과 수산회인회석은 골 조직 재생을 위해 골전도성과 생체적합성의 특성을 가진 우수한 재료로 알려져 있다. 본 연구에서, 혼합 용액 구조물은 적층 및 히터장치를 기반으로 한 압출 적층 조형 시스템을 이용하여 제작되었다. 바이오 세라믹 인공지지체는 $1,300^{\circ}C$의 고온에서 소결되었고, 또한 형태학적인 특성은 주사전자현미경을 통해 분석되었다. 게다가, TCP/HA 의 혼합비율에 따른 미세구조물과 수축률에 대한 효과는 연구되었다. 인공지지체의 기계적 특성은 1 mm/min 의 크로스헤드 속도로 압축 시험기를 통해 측정되었고, 인공지지체의 세포 증식평가를 위해 MG-63 세포를 이용하였다. 본 연구의 결과는 혼합된 TCP(75 wt%)/HA(25 wt%) 인공지지체가 골 조직 재생을 위해 적합한 인공지지체라는 것을 제안한다.

• Restorative Dentistry and Endodontics
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• 제45권2호
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• pp.19.1-19.8
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• 2020

Objective: This study aimed to evaluate the effect of ultrasonic cleaning of the intracanal post space on the bond strength of fiber posts in oval canals filled with a premixed bioceramic (Bio-C Sealer [BIOC]) root canal sealer. Materials and Methods: Fifty premolars were endodontically prepared and divided into 5 groups (n = 10), based on the type of root canal filling material used and the post space cleaning protocol. A1: gutta-percha + AH Plus (AHP) and post space preparation with ultrasonic cleaning, A2: gutta-percha + BIOC and post space preparation with ultrasonic cleaning, B1: gutta-percha + AHP and post space preparation, B2: gutta-percha + BIOC and post space preparation, C: control group. Fiber posts were cemented with a self-adhesive luting material, and 1 mm thick slices were sectioned from the middle and cervical third to evaluate the remaining filling material microscopically. The samples were subjected to a push-out test to analyze the bond strength of the fiber post, and the results were analyzed with the Shapiro-Wilk, Bonferroni, Kruskal-Wallis, and Mann-Whitney tests (p < 0.05). Failure modes were evaluated using optical microscopy. Results: The results showed that the fiber posts cemented in canals sealed with BIOC had lower bond strength than those sealed with AHP. The ultrasonic cleaning of the post space improved the bond strength of fiber posts in canals sealed with AHP, but not with BIOC. Conclusions: BIOC decreased the bond strength of fiber posts in oval canals, regardless of ultrasonic cleaning.

• 태양에너지
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• 제15권2호
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• pp.13-24
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• 1995

국내의 주택난방은 온수 순환 파이프를 매설한 시멘트 온돌이 대부분을 차지하고 있으며, 현재와 같은 형태의 파이프 매설식 온돌은 열매자체의 축열성이 없기 때문에 빈번한 난방열의 공급으로 인하여 경제성과 쾌적도의 측면에서 불리하고, 또한 매설식이기 때문에 고장시의 수리가 불편하다는 문제점을 안고 있다. 따라서 축열형 조립식 형태의 온돌에 관한 연구가 최근에 이루어 지고 있으나, 실용화를 저해서는 보다 더 조직적이며 체계적인 연구가 이루어져야 할 것으로 판단된다. 현재 이용되고 있는 매설식 온수 순환 온돌의 단점을 개선하기 위하여 본 연구에서는 잠열축열재와 바이오세라믹을 이용한 조립식 온돌을 설계 제작하였으며, 온돌을 설치한 난방공간의 열전달 특성을 열평형 이론을 적용하여 해석하였다.

• Restorative Dentistry and Endodontics
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• 제44권2호
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• pp.18.1-18.9
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• 2019

Objective: This study evaluated the presence of residual root canal filling material after retreatment using micro-computed tomography (micro-CT). Materials and Methods: Extracted human teeth (single- and double-rooted, n = 21/each; C-shaped, n = 15) were prepared with ProFile and randomly assigned to three subgroups for obturation with gutta-percha and three different sealers (EndoSeal MTA, EndoSequence BC sealer, and AH Plus). After 10 days, the filling material was removed and the root canals were instrumented one size up from the previous master apical file size. The teeth were scanned using micro-CT before and after retreatment. The percentage of remaining filling material after retreatment was calculated at the coronal, middle, and apical thirds. Data were analyzed using the Kruskal-Wallis test and Mann-Whitney U test with Bonferroni post hoc correction. Results: The tested sealers showed no significant differences in the percentage of remaining filling material in single- and double-rooted teeth, although EndoSeal MTA showed the highest value in C-shaped roots (p < 0.05). The percentage of remaining filling material of AH Plus and EndoSeal MTA was significantly higher in C-shaped roots than in single- or double-roots (p < 0.05), while that of BC sealer was similar across all root types. EndoSeal MTA showed the highest values at the apical thirds of single- and double-roots (p < 0.05); otherwise, no significant differences were observed among the coronal, middle, and apical thirds. Conclusions: Within the limitations of this study, a large amount of EndoSeal MTA remained after retreatment, especially in C-shaped root canals.

• Restorative Dentistry and Endodontics
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• 제48권1호
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• pp.8.1-8.8
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• 2023

Objectives: This study was designed to evaluate the parameters of bonding performance to root dentin, including push-out bond strength and dentinal tubular biomineralization, of a hydraulic bioceramic root-end filling material premixed with dimethyl sulfoxide (Endocem MTA Premixed) in comparison to a conventional powder-liquid-type cement (ProRoot MTA). Materials and Methods: The root canal of a single-rooted premolar was filled with either ProRoot MTA or Endocem MTA Premixed (n = 15). A slice of dentin was obtained from each root. Using the sliced specimen, the push-out bond strength was measured, and the failure pattern was observed under a stereomicroscope. The apical segment was divided into halves; the split surface was observed under a scanning electron microscope, and intratubular biomineralization was examined by observing the precipitates formed in the dentinal tubule. Then, the chemical characteristics of the precipitates were evaluated with energy-dispersive X-ray spectroscopic (EDS) analysis. The data were analyzed using the Student's t-test followed by the Mann-Whitney U test (p < 0.05). Results: No significant difference was found between the 2 tested groups in push-out bond strength, and cohesive failure was the predominant failure type. In both groups, flake-shaped precipitates were observed along dentinal tubules. The EDS analysis indicated that the mass percentage of calcium and phosphorus in the precipitate was similar to that found in hydroxyapatite. Conclusions: Regarding bonding to root dentin, Endocem MTA Premixed may have potential for use as an acceptable root-end filling material.

• 한국축산식품학회지
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• 제24권4호
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• pp.329-334
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• 2004

본 연구의 목적은 한방 부산물 및 바이오 세라믹(약돌) 혼합물의 급여가 비육돈의 성장 및 육질 특성에 미치는 영향을 평가하기 위하여 실시하였다. 3원 교잡종(Landrace${\times}$York-shire${\times}$Duroc) 비육돈 72두를 공시하였으며 시험개시시의 체중은 78.98kg이었다. 시험설계는 옥수수-대두박 위주의 사료인 대조구(Cotrol: 기초사료), 대조구 사료 내 한방부산물 및 바이오 세라믹 혼합물 0.1%[HBC 0.1 기초사료 + 0.1%한방 부산물 및 바이오 세라믹(약돌) 혼합물], 0.2% 첨가한 구 [HBC 0.2$.$ 기초사료 +0.2% 한방 부산물 및 바이오 세라믹(약돌) 혼합물]로 3처리를 하여 처리당 6반복, 반복당 4마리씩 완전임의 배치하였다. 전체 시험기간 동안, 일당 증체량은 대조구와 한방 부산물 및 바이오 세라믹(약돌) 혼합물을 첨가한 처리구 사이에서 대조구가 높았으나 유의적인 차이는 없었다(p>0.05). 등지방 두께는 한방 부산물 및 바이오 세라믹(약돌) 혼합물 0.2%를 첨가한 처리구가 얇아졌으나 유의적인 차이는 없었다(p>0.05). 총 콜레스테롤, LDL 콜레스테롤과 LDL + VLDL 콜레스테롤은 HBC 0.2 처리구가 낮게 나타났으나 유의적인 차이는 없었다(p>0.05). 동맥경화지수에 있어서는 한방 부산물 및 바이오 세라믹(약돌) 첨가 수준에 따라 낮게 나타났지만 유의적인 차이는 없었다(p>0.05). 또한, 도축한 돈육의 등심부위 육색에 있어서 L$^{*}$ -, a$^{*}$ -, b$^{*}$ -값에 있어서도 유의적인 차이를 보이지 않았다(p>0.05). pH는 등심부위에서 한방 부산물과 바이오 세라믹(약돌) 0.2% 첨가한 처리구가 낮게 나타났다(p<0.05). 결론적으로 비육돈 사료내 한방 부산물 및 바이오 세라믹(약돌) 혼합물 급여가 비육돈의 성장 및 육질 특성에는 영향을 미치지 않는 것으로 판단된다.