• 제목/요약/키워드: Bath temperature

검색결과 581건 처리시간 0.033초

경질용 3가 크롬전착에 미치는 전해조건의 영향 (Effect of Electrolysis Conditions on Hard Chromium Deposition from Trivalent Chromium Bath)

  • 김대영;박상언;김만;권식철;최주원;최용
    • 한국표면공학회지
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    • 제36권2호
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    • pp.155-160
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    • 2003
  • The effect of the temperature, current density and deposit time on hard chromium deposition in trivalent chromium bath was investigated. Cathode current efficiency increased with increasing current density. Increasing bath temperature from $20^{\circ}C$ to $50^{\circ}C$, chromium deposits were produced in higher current density and the maximum current efficiency was increased. At the plating conditions of $40^{\circ}C$, $30A/dm\m^2$, the deposition thickness increased in proportion to increasing electrolysis time The rate is$ 90\mu\textrm{m}$/hrs. for 2 hours. Microhardness of chromium deposits increased with increasing bath temperature and decreasing current density, and it was constant with electrolysis time. All of bath conditions, microstructure of chromium deposits has nodular structure with some cracking pattern and nodule size increased with increasing deposit thickness.

무전해도금에 의한 코발트- 인 박막의 자성에 미치는 도금조건의 영향 (Influences of Plating Conditions on Magnetic Properties of Co-P Thin Films by Electroless Plating)

  • 최병익;여운관;이주성
    • 한국표면공학회지
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    • 제19권1호
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    • pp.3-12
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    • 1986
  • Influences of pH, temperature, and composition of bath on the deposition rate and the magnetic properties were studied for two kinds of electroless Co-P plating bath. The results obtained are as follows. Ammonia alkaline citrate bath was more stable than ammonia alkaline tartrate bath, and the film deposited from citrate bath gave a higher squareness. The magnetic properties of the film obtained from citrate bath greatly depended upon pH. Under the optimum conditions, the film deposited from citrate bath had coercive force of 330 Oe and squareness of 0.67. However the films deposited from tartrate bath had coercive force of 300 Oe and squareness of 0.58.

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관절 질환의 통증과 가동력에 파라핀 치료가 미치는 효과 (The Effect of Paraffin Therapy on Release of pain and Range of motion with Joint Disease Patients)

  • 이석민;권기자
    • 대한물리치료과학회지
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    • 제10권1호
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    • pp.130-139
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    • 2003
  • This study was conducted in order to determine the effect of Paraffin Therapy on release of pain, skin temperature and range of motion with joint diseases. This study was performed on 42 patients with general joint diseases and 21 patients with degenerative joint diseases. All the subjects were randomly assigned to three groups with 21 each. The experiment had been done from June, 1. 2002 to September, 30. 2002, in two general hospitals and a social welfare center using Digital Thermometer Kane-May KM330 and VAS(visual analogue scale). Each pint was measured in terms of skin temperature, pain scale and ROM(range of motion). The results of the experiment are as follows : 1. In application of three different heat modalities (Paraffin bath, Infra red, Hydro pack) on the Knee, Ankle, Elbow pints of the subjects for 30 minutes, the elevation of skin temperature and the reduction of pain scale were found to be significantly different. When checked right after the 30 minutes' application, the Infra red resulted in a higher degree elevation of skin temperature than two other modalities, while Paraffin bath resulted in the highest degree of the elevation of skin temperature when it was checked one hour after the application was over. It means that Paraffin bath lasted longer than the other two modalities(F=14.691, p<.000). 2. With Paraffin bath application, pint pain was reduced significantly both in 30 minutes and one hour checks(F=20.675, p<.001). 3. In terms of ROM(range of motion) increase, didn't seem to have any significant differences in 30 minutes and one hour. The results suggest that Paraffin therapy be helpful in maximizing th effects on pint diseases. I strongly suggest that further studies be done on other pints and muscle diseases using Paraffin bath in different methods of applying the therapy.

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Chemical Bath Deposition으로 성장한 CdS 박막의 반응온도에 대한 특성 (Dependence of reaction temperature on the properties of CdS thin films grown by Chemical Bath Deposition)

  • 이가연;유현민;이재형
    • 한국정보통신학회:학술대회논문집
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    • 한국해양정보통신학회 2010년도 춘계학술대회
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    • pp.805-808
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    • 2010
  • 본 연구에서는 CdTe 및 $CuInSe_2$ 태양전지의 광투과층으로 사용되는 CdS 박막을 chemical bath deposition으로 제조하고, 반응용액의 온도에 따른 미세구조의 변화를 조사하였다. CdS 박막의 결정구조와 미세구조는 기판의 종류에 큰 변화 없이 $85^{\circ}C$ 까지는 반응용액의 온도가 증가함에 따라 기판에서의 ion-by-ion 성장이 촉진되어 CdS 박막의 성장률이 증가하며, 결정성이 향상되고 continuous하면서 매우 조밀한 미세구조를 가졌다. 그러나 온도가 $55^{\circ}C$ 이하의 경우 CdS 형성에 필요한 Cd2+ 이온의 공급이 느려져 온도에 따라 증착률이 감소하였다. 또한 핵생성 위치 수가 감소하여 입자의 크기가 증가하였고, 박막 내부에는 void가 형성되어 균일하지 못한 미세구조를 나타내었다.

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冷間壓廷鋼板의 Aluminizing에 對한 速度論的인 硏究 (A Study on the kinetics of Aluminizing of Cold rolled Steel Sheets)

  • 윤병하;김영기
    • 한국표면공학회지
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    • 제12권2호
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    • pp.75-83
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    • 1979
  • The Rates of formation and heats of activation for the intermatallic Compound Layers between Cold rolled sheet and molten aluminium &ath (adding small amounts of silicon) has been determined by Continous aluminizing method in the temperature range of 680$^{\circ}$ to 760$^{\circ}C$ and with immerssion time. The structure of the intermetallic Compound Layers was the shape of "Tongues" in pure Al-Bath and Al-Bath Containing 1% Si, But in Al-5% Si Bath was "Band" the Composition of the intermetallic Compound Layers were checked by microhardness measurements and X-Ray probe micro analyzer. FeAl intermetallic Compound layer was found to be uniform in pure Al-Bath and Al-5% Si Bath, But Fe Al intermetallic Compound Layer was shown in Al-1% Si Bath. The growth Rates of the intermetallic Compound Layers was most rapidly increased at Temperatures from 720$^{\circ}$ to 760$^{\circ}C$, at the immorsion time above 60 Second in pure Al-Bath, But in Al-1% Si Bath was solwly increased for the same conditions, and then in Al-5% Si Bath was hardly effected by these experimental condition. Heasts of activation of 29, 46 Kcal per mole which calculuted from Layer growth experiments were found in pure Al-Bath, Al-1% Si Bath respectively.

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Cellulose acetate membrane preparation by phase inversion to estimate optimized parameters and its performance study

  • Katariya, Heena N;Patel, Tejal M
    • Membrane and Water Treatment
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    • 제13권3호
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    • pp.139-145
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    • 2022
  • Development in advanced separation processes leads to the significant advancement in polymeric membrane preparation methodology. Therefore, present research investigated the preparation and characterization of cellulose acetate membrane by phase inversion separation method to determine optimized operating parameters. Prepared CA membrane's performance was been analyzed in terms of % rejection and flux. Investigation was conducted to study effect of different parameters such as polymer concentration, evaporation rate, thickness of film, coagulation bath properties, temperature of polymer solution and of the coagulation bath etc. CA membrane was fabricated by taking polymer concentration 10wt% and 11wt% with zero second evaporation time and varying film thickness over non-woven polyester fabric. Effect of coagulation bath temperature (CBT) and casting solution temperature were also been studied. The experimental results from SEM showed that the surface morphology had been changed with polymer r concentration, coagulation bath and casting solution temperature, etc. Lower polymer concentration leads to lower precipitation time giving porous membrane. The prepared membrane was tested for advanced waste water treatment of relevant effluent stream in pilot plant to study flux and rejection behavior of the membrane.

Effect of bath conditions and pulse parameters on tin surface finish for microelectronic packaging applications

  • Sharma, Ashutosh;Jung, Do-hyun;Jung, Jae-pil
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2015년도 추계학술대회 논문집
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    • pp.232-233
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    • 2015
  • The effects of various bath conditions such as surfactant concentration, bath pH, bath temperature, agitation of bath; as well as pulse parameters such as cathodic current density, pulse duty cycle and frequency, on the grain size, surface finish, and appearance of the tin plated coatings have been investigated. The plating bath under investigation is an aqueous acidic solution composed of a mixture of $SnSO_4$, $H_2SO_4$, and a surfactant. The bath conductivity and pH are measured by a glass pH electrode. The microstructure of the coatings produced is characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and surface profilometry. XRD analysis shows that the deposits consist of tetragonal ${\beta}$-Sn crystal structure irrespective of plating conditions. The mechanism involved in the morphology evolution in response to various parameters and conditions has also been discussed.

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공랭식 변유량 냉매 냉동기를 적용한 수조 온도의 정밀 제어 (Precision Control of Water Bath Temperature using Air Cooled Variable Refrigerant Flow Chiller)

  • 정광주;김영일
    • 한국지열·수열에너지학회논문집
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    • 제14권4호
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    • pp.27-34
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    • 2018
  • This study compared constant water bath performances of conventional water-cooled refrigerator and electric heater with an air-cooled VRF chiller and electric heater equipped with optimal control algorithm. In heating mode, the air cooled VRF chiller and electric heater combination reduced the set temperature arrival time by an average of 42 minutes, and energy was also reduced by 18%. In cooling mode, the two systems took 70 minutes to reach the set temperature and showed no difference. Energy was reduced by 33.5% with the new system. For constant temperature maintaining experiment, after reaching the set temperature of $15^{\circ}C$, $20^{\circ}C$ and $22^{\circ}C$, temperature deviations were all in the range of $-0.2^{\circ}C$ to $+0.1^{\circ}C$. Energy was reduced by an average of 84.9%. Through this study, possibility of precise temperature control by an air cooled VRF chiller system was confirmed.

철강의 염산산세 폐액으로부터 전해철의 제조에 관한 연구 (Recovery of Pure Electrolytic Iron from Wasted Hydrochloric Pickling Solution of Steel)

  • 김기호;권오익;홍성규
    • 한국표면공학회지
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    • 제26권1호
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    • pp.23-30
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    • 1993
  • Iron component in wasted hydrochloric etching solutions from steel works were recovered by electrolysis. The electric conductances of the solutions, as the function of the bath temperature and the ferrousion concen-tration, were measured and the result of the original solution was K=(0.0012+0.0005$\times$10-3T-0.1160$\times$10-6T2)$\times$102S.m-1(T in $^{\circ}C$) The current efficiency was better for the bath using a soluble steel plate anode than for the bath using an insoluble platinized titanium one. Densed electrolytic iron having the purity of higher than 99.99% was ob-tained at the electrolysis conditions of the cathodic current density of 15A/dm2, the bath temperature of $70\pm$$5^{\circ}C$ and the ferrous ion concentration of about 100g/l. The morphologies of the deposited iron were observed by SEM.

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